4.1 The presence of trace amounts of hydrogen, oxygen, and carbon monoxide can have deleterious effects in certain processes using hydrocarbon products as feed stock. This test method is suitable for setting specifications, for use as an internal quality control tool and for use in development or research work.1.1 This test method covers the determination of hydrogen, nitrogen, oxygen, and carbon monoxide in the parts per million volume (ppmv) range in C2 and lighter hydrocarbon products. This test method should be applicable to light hydrocarbons other than ethylene, but the test program did not include them.1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For some specific hazard statements, see the Annex A1.

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1.1 This specification applies to the maximum content of eight PAHs (PAH8) in materials used as synthetic turf infill.1.2 This specification outlines a test method for sample preparation and the method for analyzing the content of the eight PAHs in synthetic turf infill.1.3 This specification provides guidelines for reporting the content of the eight PAHs in the synthetic turf infill.1.4 This specification is applicable to any infill material used in synthetic turf.1.5 The values stated in SI units are to be regarded as standard. No other units are included in this standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价： 515元 / 折扣价： 438 元 加购物车

1.1 This specification covers high-boiling hydrocarbon solvent for preparing solutions of oil-borne preservatives such as pentachlorophenol and copper naphthenate, and which shall be composed of petroleum distillates and cosolvents, provided that the blended solvent meets the requirements of Section 3.

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5.1 These test methods are intended to provide a basis for evaluating the time period during which a beam, girder, column, or similar structural assembly, or a nonbearing wall, will continue to perform its intended function when subjected to a controlled, standardized fire exposure.5.1.1 In particular, the selected standard exposure condition simulates the condition of total continuous engulfment of a member or assembly in the luminous flame (fire plume) area of a large free-burning-fluid-hydrocarbon pool fire. The standard fire exposure is basically defined in terms of the total flux incident on the test specimen together with appropriate temperature conditions. Quantitative measurements of the thermal exposure (total heat flux) are required during both furnace calibration and actual testing.5.1.2 It is recognized that the thermodynamic properties of free-burning, hydrocarbon fluid pool fires have not been completely characterized and are variable depending on the size of the fire, the fuel, environmental factors (such as wind conditions), the physical relationship of the structural member to the exposing fire, and other factors. As a result, the exposure specified in these test methods is not necessarily representative of all the conditions that exist in large hydrocarbon pool fires. The specified standard exposure is based upon the best available information and testing technology. It provides a basis for comparing the relative performance of different assemblies under controlled conditions.5.1.3 Any variation to construction or conditions (that is, size, method of assembly, and materials) from that of the tested assembly is capable of substantially changing the performance characteristics of the assembly.5.2 Separate procedures are specified for testing column specimens with and without an applied superimposed load.5.2.1 The procedures for testing loaded columns stipulate that the load shall be applied axially. The applied load is to be the maximum load condition allowed under nationally recognized structural design criteria unless limited design criteria are specified and a corresponding reduced load applied.5.2.2 The procedure for testing unloaded steel column specimens includes temperature limits. These limits are intended to define the temperature above which a steel column with an axially applied design allowable load would fail structurally.5.2.3 The procedure for unloaded specimens also provides for the testing of other than steel columns provided that appropriate acceptance criteria have been established.5.3 Separate procedures are also specified for testing beam assemblies with and without an applied superimposed load.5.3.1 The procedure for testing loaded specimens stipulates that the beam shall be simply supported. Application of restraint against longitudinal thermal expansion depends on the intended use, as specified by the customer. The applied load is intended to be the allowable design load permitted for the beam as determined in accordance with accepted engineering practice.5.3.2 The procedure for testing unloaded beams includes temperature limits for steel. These limits are to define the temperature above which a simply supported, unrestrained beam would fail structurally if subjected to the allowable design load. The procedure for unloaded specimens also provides for the testing of other than steel and reinforced concrete beams provided that appropriate acceptance criteria have been established.5.3.3 It is recognized that beam assemblies that are tested without load will not deflect to the same extent as an identical assembly tested with load. As a result, tests conducted in accordance with the unloaded beam procedure are not intended to reflect the effects of crack formation, dislodgement of applied fire protection materials, and other factors that are influenced by the deflection of the assembly.5.4 A separate procedure is specified for testing the fire-containment capability of a wall/bulkhead/partition, etc. Acceptance criteria include temperature rise of nonfire exposed surface, plus the ability of the wall to prohibit passage of flames or hot gases, or both.5.5 In most cases, the structural assemblies that will be evaluated in accordance with these test methods will be located outdoors and subjected to varying weather conditions that are capable of adversely affecting the fire endurance of the assembly. A program of accelerated weathering followed by fire exposure is described to simulate such exposure.5.6 These test methods provide for quantitative heat flux measurements to support the development of design fires and the use of fire safety engineering models to predict thermal exposure and material performance in a wide range of fire scenarios.1.1 The test methods described in this fire-test-response standard are used for determining the fire-test response of columns, girders, beams or similar structural members, and fire-containment walls, of either homogeneous or composite construction, that are employed in HPI or other facilities subject to large hydrocarbon pool fires.1.2 It is the intent that tests conducted in accordance with these test methods will indicate whether structural members of assemblies, or fire-containment wall assemblies, will continue to perform their intended function during the period of fire exposure. These tests shall not be construed as having determined suitability for use after fire exposure.1.3 These test methods prescribe a standard fire exposure for comparing the relative performance of different structural and fire-containment wall assemblies under controlled laboratory conditions. The application of these test results to predict the performance of actual assemblies when exposed to large pool fires requires a careful engineering evaluation.1.4 These test methods provide for quantitative heat flux measurements during both the control calibration and the actual test. These heat flux measurements are being made to support the development of design fires and the use of fire safety engineering models to predict thermal exposure and material performance in a wide range of fire scenarios.1.5 These test methods are useful for testing other items such as piping, electrical circuits in conduit, floors or decks, and cable trays. Testing of these types of items requires development of appropriate specimen details and end-point or failure criteria. Such failure criteria and test specimen descriptions are not provided in these test methods.1.6 Limitations—These test methods do not provide the following:1.6.1 Full information on the performance of assemblies constructed with components or of dimensions other than those tested.1.6.2 An evaluation of the degree to which the assembly contributes to the fire hazard through the generation of smoke, toxic gases, or other products of combustion.1.6.3 Simulation of fire behavior of joints or connections between structural elements such as beam-to-column connections.1.6.4 Measurement of flame spread over the surface of the test assembly.1.6.5 Procedures for measuring the test performance of other structural shapes (such as vessel skirts), equipment (such as electrical cables, motor-operated valves, etc.), or items subject to large hydrocarbon pool fires, other than those described in 1.1.1.6.6 The erosive effect that the velocities or turbulence, or both, generated in large pool fires has on some fire protection materials.1.6.7 Full information on the performance of assemblies at times less than 5 min because the rise time called out in Section 5 is longer than that of a real fire.1.7 These test methods do not preclude the use of a real fire or any other method of evaluating the performance of structural members and assemblies in simulated fire conditions. Any test method that is demonstrated to comply with Section 5 is acceptable.1.8 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.9 This standard is used to measure and describe the response of materials, products, or assemblies to heat and flame under controlled conditions, but does not by itself incorporate all factors required for fire hazard or fire risk assessment of the materials, products, or assemblies under actual fire conditions.1.10 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.11 The text of this standard references notes and footnotes which provide explanatory information. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.1.12 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 These methods are to be used as a basis for comparison of absorbents in a consistent manner.5.2 These tests are not appropriate for adsorbent materials which are covered in Test Method F726.5.3 These methods are not useful for a comparison of absorbents with adsorbents, even though all absorbents exhibit adsorbent properties. Both types of materials have prime areas of utility.5.4 These methods may not list all the safety and disposal options necessary for safe ultimate disposal of used sorbent material into the environment. Federal, state, and local regulatory rules must be followed.1.1 These test methods cover the development of laboratory test data that describe the performance of absorbent materials (and their retention ability) for use on chemical and light hydrocarbon spills.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. (For a specific warning statement see 10.4.)1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价： 590元 / 折扣价： 502 元 加购物车

1.1 This test method covers the determination of the solubility of pentachlorophenol wood preservative in heavy hydrocarbon solvent. 1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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5.1 Low operating temperature fuel cells such as proton exchange membrane fuel cells (PEM-FC) require high purity hydrogen for maximum material performance and lifetime. Analysis to 0.1 part per million (ppm(v)) concentration of THCs (measured as CH4) in hydrogen is necessary for ensuring a feed gas of sufficient purity to satisfy fuel cell system needs as defined in SAE J2719 or as specified in regulatory codes.5.2 Dynamic dilution techniques using highly accurate mass flow controllers can be used with test samples that have THC content exceeding the upper limit of the instrument’s linear range, without the need to recalibrate the instrument using higher levels of calibration standards. The sample can be diluted with a high purity grade of hydrogen (99.999 %, so long as it contains < 0.1 ppm(v) THCs) to achieve a result of the THC content by applying the appropriate dilution factor to the result. Samples that contain THC concentrations greater than 1000 ppm(v) may be determined, although results will likey be achieved with reduced precision and should be analyzed by the dilution method.5.3 Although not intended for application to gases other than hydrogen, techniques within this test method can be applied to other non-hydrocarbon gas samples requiring THC content determination. This can be achieved by using a zero gas and a calibration gas that consist of the same background gas as the actual sample. As an example, for the THC determination of nitrogen, the instrument zero point must be determined with a high purity grade of nitrogen (99.999 % and < 0.1 ppm(v) THCs) and the instrument calibration must be done with a certified standard of CH4 in nitrogen in the appropriate range. This will correct for any interferences caused by the background gas.1.1 This test method describes a procedure for total hydrocarbons (THC’s) measurement in hydrogen intended as a fuel on a methane (C1) basis. The determination of THC on a C1 basis is an analytical technique where all the hydrocarbons are assumed to have the same response as methane (CH4). Sensitivity from 0.1 parts per million by volume (ppm(v), µmol/mol) up to 1000 ppm(v) concentration is achievable. Higher concentrations can be analyzed using appropriate dilution techniques. This test method can be applied to other gaseous samples requiring analysis of trace constituents provided an assessment of potential interferences has been accomplished.1.2 This test method is a Flame Ionization Detector-based (FID-based) hydrocarbon analysis method without the use of separation columns. Therefore, this method does not provide speciation of individual hydrocarbons. Several varieties of instruments are manufactured and can be used for this method.1.2.1 This method provides a measure of THC “as CH4,” because all hydrocarbon species are quantified the same as CH4 response, which is the sole species used for calibration. Magnitude of the FID response to an atom of carbon is dependent on the chemical environment of this atom in the molecule. This method provides the THC result as if all carbon atoms are from aliphatic, aromatic, olefinic, or acetylenic compounds, where the detector response caused by these atoms is approximately relative to the number of carbon atoms present in the molecule. Other types of molecules, including those containing oxygen or chlorine atoms, will respond differently and usually much lower than the corresponding aliphatic hydrocarbon. Therefore, other methods (Test Methods D7653, D7892, or equivalent) must be utilized to determine the exact constituents of the THC response determined by this method.1.3 The proper handling of compressed gas cylinders containing air, nitrogen, hydrogen, or helium requires the use of gas regulators to preclude over-pressurization of any instrument component1.4 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价： 590元 / 折扣价： 502 元 加购物车

5.1 The aromatic hydrocarbon content of motor diesel fuel is a factor that can affect exhaust emissions and fuel combustion characteristics, as measured by cetane number.5.2 The United States Environmental Protection Agency (US EPA) regulates the aromatic content of diesel fuels. California Air Resources Board (CARB) regulations place limits on the total aromatics content and polynuclear aromatic hydrocarbon content of motor diesel fuel, thus requiring an appropriate analytical determination to ensure compliance with the regulations.5.3 This test method is applicable to materials in the same boiling range as motor diesel fuels and is unaffected by fuel coloration. Test Method D1319, which has been mandated by the US EPA for the determination of aromatics in motor diesel fuel, excludes materials with final boiling points greater than 315 °C (600 °F) from its scope. Test Method D2425 is applicable to the determination of both total aromatics and polynuclear aromatic hydrocarbons in diesel fuel, but is much more costly and time consuming to perform. Test Method D5186, currently specified by CARB, is also applicable to the determination of both total aromatics and polynuclear aromatic hydrocarbons in diesel fuel. Test Method D5186, however, specifies the use of supercritical fluid chromatography equipment that may not be readily available.NOTE 2: Test Method D5186 was previously specified by CARB as an alternative to Test Method D1319.1.1 This test method covers a high performance liquid chromatographic test method for the determination of mono-aromatic, di-aromatic, tri+-aromatic, and polycyclic aromatic hydrocarbon contents in diesel fuels and petroleum distillates boiling in the range from 150 °C to 400 °C. The total aromatic content in % m/m is calculated from the sum of the corresponding individual aromatic hydrocarbon types.NOTE 1: Aviation fuels and petroleum distillates with a boiling point range from 50 °C to 300 °C are not determined by this test method and should be analyzed by Test Method D6379 or other suitable equivalent test methods.1.2 The precision of this test method has been established for diesel fuels and their blending components, containing from 4 % to 40 % (m/m) mono-aromatic hydrocarbons, 0 % to 20 % (m/m) di-aromatic hydrocarbons, 0 % to 6 % (m/m) tri+-aromatic hydrocarbons, 0 % to 26 % (m/m) polycyclic aromatic hydrocarbons, and 4 % to 65 % (m/m) total aromatic hydrocarbons.1.3 Compounds containing sulfur, nitrogen, and oxygen are possible interferents. Mono-alkenes do not interfere, but conjugated di- and poly-alkenes, if present, are possible interferents.1.4 By convention, this standard defines the aromatic hydrocarbon types on the basis of their elution characteristics from the specified liquid chromatography column relative to model aromatic compounds. Quantification is by external calibration using a single aromatic compound, which may or may not be representative of the aromatics in the sample, for each aromatic hydrocarbon type. Alternative techniques and methods may classify and quantify individual aromatic hydrocarbon types differently.1.5 Fatty Acid Methyl Esters (FAME), if present, interfere with tri+-aromatic hydrocarbons. If this method is used for diesel containing FAME, the amount of tri+-aromatics will be over estimated.1.6 This test method includes a Relative Bias section for Test Method D6591 versus Test Method D1319 and Test Method D5186 versus Test Method D6591 for diesel fuels only. The applicable concentration ranges of the correlations are presented in the Relative Bias section. The correlations are applicable only in the stated ranges.1.7 This test method and correlations were developed for diesel samples not containing biodiesel; the presence of biodiesel will interfere with the results. The correlation equations are only applicable between these concentration ranges and to diesel fuels that do not contain biodiesel.1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价： 590元 / 折扣价： 502 元 加购物车

5.1 Ampulization is desirable in order to minimize variability and maximize the integrity of calibration standards or RMs, or both, being used in calibration of analytical instruments and in validation of analytical test methods in round-robin or interlaboratory cross-check programs. This practice is intended to be used when the highest degree of confidence in integrity of a material is desired.5.2 This practice is intended to be used when it is desirable to maintain the long term storage of gasoline and related liquid hydrocarbon RMs, controls, or calibration standards for retain or repository purposes.5.3 This practice may not be applicable to materials that contain high percentages of dissolved gases, or to highly viscous materials, due to the difficulty involved in transferring such materials without encountering losses of components or ensuring sample homogeneity.1.1 This practice covers a general guide for the ampulization and storage of gasoline and related hydrocarbon mixtures that are to be used as calibration standards or reference materials. This practice addresses materials, solutions, or mixtures, which may contain volatile components. This practice is not intended to address the ampulization of highly viscous liquids, materials that are solid at room temperature, or materials that have high percentages of dissolved gases that cannot be handled under reasonable cooling temperatures and at normal atmospheric pressure without losses of these volatile components.1.2 This practice is applicable to automated ampule filling and sealing machines as well as to manual ampule filling devices, such as pipettes and hand-operated liquid dispensers.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价： 590元 / 折扣价： 502 元 加购物车

This specification covers formulating requirements for purchases of a UL100 unleaded aviation gasoline test fuel under contract and is intended solely for use by purchasing agencies for testing purposes. It prescribes the required properties of unleaded D7960 fuel at the time and place of delivery. The suitability of this fuel for use on any specific aircraft, aircraft engine, or ground-based fuel handling equipment should be evaluated before use on that equipment.Included in this specification are requirements for the manufacture of D7960 fuel and additives; workmanship, finish, and appearance; sampling; and the type and number of reports to ensure conformance with the requirements of this specification. Products shall conform to the requirements that shall be determined in accordance with ASTM test methods for knock value (lean rating), tetraethyl lead, density, distillation, vapor pressure, freezing point, sulfur, net heat of combustion, corrosion (copper strip), potential gum and visible lead precipitate, water reaction, and electrical conductivity.1.1 This specification covers formulating specifications for purchases of a UL102 unleaded aviation gasoline test fuel under contract and is intended solely for use by purchasing agencies for testing purposes.1.2 This specification defines a specific type of aviation gasoline for use as an aviation spark-ignition engine test fuel. It does not include all gasolines satisfactory for reciprocating aviation engines. Certain equipment or conditions of use may permit a wider, or require a narrower, range of characteristics than is shown by this specification.1.3 The D7960 test fuel defined by this specification may not exhibit identical performance to those leaded fuels with which the existing aircraft and ground-based fuel handling equipment have been designed to operate. Therefore, the suitability of this fuel for use on any specific aircraft, aircraft engine, or ground-based fuel handling equipment should be evaluated before use on that equipment.1.4 Issuance of this specification does not constitute approval to operate certificated aircraft with this fuel. Fuels used in certified engines and aircraft are ultimately approved by the certifying authority subsequent to formal submission of evidence to the authority as part of the certification program for that aircraft and engine model.1.5 This specification, unless otherwise provided, prescribes the required properties of unleaded D7960 test fuel at the time and place of delivery.1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价： 590元 / 折扣价： 502 元 加购物车

5.1 Aromatic content is a key characteristic of hydrocarbon oils and can affect a variety of properties of the oil including its boiling range, viscosity, stability, and compatibility of the oil with polymers.5.2 Existing methods for estimating aromatic contents use physical measurements, such as refractive index, density, and number average molecular weight (see Test Method D3238) or infrared absorbance4 and often depend on the availability of suitable standards. These NMR procedures do not require standards of known aromatic hydrogen or aromatic carbon contents and are applicable to a wide range of hydrocarbon oils that are completely soluble in chloroform at ambient temperature.5.3 The aromatic hydrogen and aromatic carbon contents determined by this test method can be used to evaluate changes in aromatic contents of hydrocarbon oils due to changes in processing conditions and to develop processing models in which the aromatic content of the hydrocarbon oil is a key processing indicator.1.1 This test method covers the determination of the aromatic hydrogen content (Procedures A and B) and aromatic carbon content (Procedure C) of hydrocarbon oils using high-resolution nuclear magnetic resonance (NMR) spectrometers. Applicable samples include kerosenes, gas oils, mineral oils, lubricating oils, coal liquids, and other distillates that are completely soluble in chloroform at ambient temperature. For pulse Fourier transform (FT) spectrometers, the detection limit is typically 0.1 mol % aromatic hydrogen atoms and 0.5 mol % aromatic carbon atoms. For continuous wave (CW) spectrometers, which are suitable for measuring aromatic hydrogen contents only, the detection limit is considerably higher and typically 0.5 mol % aromatic hydrogen atoms.1.2 The reported units are mole percent aromatic hydrogen atoms and mole percent aromatic carbon atoms.1.3 This test method is not applicable to samples containing more than 1 mass % olefinic or phenolic compounds.1.4 This test method does not cover the determination of the percentage mass of aromatic compounds in oils since NMR signals from both saturated hydrocarbons and aliphatic substituents on aromatic ring compounds appear in the same chemical shift region. For the determination of mass or volume percent aromatics in hydrocarbon oils, chromatographic, or mass spectrometry methods can be used.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in 7.2 and 7.3.

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5.1 The determination of oxygenates is important in the manufacture of ethene, propene, 1-3 butadiene, C4 hydrocarbons, and C5 hydrocarbons. Alcohols, ethers, aldehydes, and ketones are trace impurities in these hydrocarbons. Oxygenates decrease catalyst activity in downstream polymerization processes.1.1 This test method covers the gas chromatographic procedure for the quantitative determination of organic oxygenates in C2, C3, C4, and C5 matrices by multidimensional gas chromatography and flame ionization detection. This test method is applicable when the hydrocarbon matrices have a final boiling point not greater than 200 °C. Oxygenate compounds include, but are not limited to, those listed in Table 1. The linear working range for oxygenates is 0.50 mg/kg to 100 mg/kg.1.2 This test method is intended to determine the mass concentration of each oxygenate in the hydrocarbon matrix. Oxygenate compound identification is determined by reference standards and column elution retention order.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4.1 The user is advised to obtain LPG safety training for the safe operation of this test method procedure and related activities. The eLearning training course “Liquefied Petroleum Gases Sampling Safety” is available on the ASTM.org website.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价： 590元 / 折扣价： 502 元 加购物车

5.1 A knowledge of the hydrocarbon composition of the middle distillates, including the biodiesel blends is useful in following the effect of changes in process variables, diagnosing the source of plant upsets, and in evaluating the effect of changes in composition on product performance properties. The total aromatics content and polycyclic aromatics content are also important to evaluate the quality of diesel fuels/biodiesel blends. It requires an appropriate analytical method to make such determinations for diesel fuel/biodiesel blends production process and quality control.5.2 This test method provides a comprehensive analytical strategy for the determination of the total aromatics contents, polycyclic aromatics contents and the detail hydrocarbon composition of diesel fuel/biodiesel blends to ensure compliance with certain specifications or regulations.5.3 Test Method D2425 is applicable to the determination of the detailed hydrocarbon composition in middle distillates, however, the pre-separation procedure of elution chromatography is time-consuming and not eco-friendly. By combining with the separation procedures described in Test Method D8144, the dual column GC-MS system proposed in this method can determine the total aromatic hydrocarbon contents, polycyclic aromatic hydrocarbon contents and detailed hydrocarbon composition of diesel fuel/biodiesel blends simultaneously. The content of FAME in biodiesel blends can also be determined by GC. It is demonstrated to be time-saving and eco-friendly for the quality control of diesel fuel and biodiesel blends.1.1 This test method covers an analytical scheme using the gas chromatography/mass spectrometry (GC-MS) to determine the hydrocarbon types present in middle distillates 170 °C to 365 °C boiling range, 5 % to 95 % by volume as determined by Test Method D86, including biodiesel blends with up to 20 % by volume of fatty acid methyl ester (FAME). The detailed hydrocarbon composition, total aromatic hydrocarbon and polycyclic aromatic hydrocarbon contents can be determined. The hydrocarbon types include: paraffins, noncondensed cycloparaffins, condensed dicycloparaffins, condensed tricycloparaffins, alkylbenzenes, indans or tetralins, or both, CnH2n-10 (indenes, etc.), naphthalenes, CnH2n-14 (acenaphthenes, etc.), CnH2n-16 (acenaphthylenes, etc.), and tricyclic aromatics. The content of FAME in biodiesel blends can also be determined by GC.1.2 The values stated in acceptable SI units are to be regarded as the standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Performance testing of on-line analyzers is critical to their proper performance within predictable levels of precision and accuracy. This practice can affect production efficiency and certification of aromatic hydrocarbon materials.1.1 This practice serves as a practical guide for the performance testing of process stream analyzers specifically for measuring chemical or physical characteristics of liquid aromatic hydrocarbon materials for production or certification of these materials. The practice may be applicable to other hydrocarbon stream analyzers as well.1.2 Only external methods (complete substitution of the process stream with a standard) of control sample introduction are included. Internal methods are beyond the scope of this practice.1.3 Methods for resetting key operational parameters of analyzers to match predefined limits are provided by vendors and are not included in this practice.1.4 Analyzer validation procedures are covered in Practices D3764 and D6122, not in this practice.1.5 Procedures for statistically interpreting data from automatic sampling process stream analyzers are outlined.1.6 The implementation of this practice requires that the analyzer be installed according to APIRP-550 (1),2 and be in agreement with the analyzer supplier’s recommendations. Also, it assumes that the analyzer is designed to monitor the specific material parameter of interest, and that at the time of initial or periodic validation, the analyzer was operating at the conditions specified by the manufacturer and consistently with the primary test method.1.7 The units of measure used in this practice shall be the same as those applicable to the test primary method used for analyzer validation.1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices, and determine the applicability of regulatory limitations prior to use.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Thermal analysis provides a rapid method for determining transition temperatures in HC resins that possess them.5.2 This practice is useful for both quality assurance and research.1.1 This practice covers determination of glass transition temperatures of hydrocarbon (HC) resins by differential scanning calorimetry (DSC).1.2 This practice is applicable to HC resins as defined in Terminology D6640. The normal operating temperature range is from the cryogenic region to approximately 180 °C. The temperature range can be extended.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 Further discussion of glass transition can be found in Test Method D3418, and Test Method E1356.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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