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3.1 An indication of the susceptibility to initiation of localized corrosion in this test method is given by the potential at which the anodic current increases rapidly. The more noble this potential, obtained at a fixed scan rate in this test, the less susceptible is the alloy to initiation of localized corrosion. The results of this test are not intended to correlate in a quantitative manner with the rate of propagation that one might observe in service when localized corrosion occurs.3.2 In general, once initiated, localized corrosion can propagate at some potential more electropositive than that at which the hysteresis loop is completed. In this test method, the potential at which the hysteresis loop is completed is determined at a fixed scan rate. In these cases, the more electropositive the potential at which the hysteresis loop is completed the less likely it is that localized corrosion will occur.3.3 If followed, this test method will provide cyclic potentiodynamic anodic polarization measurements that will reproduce data developed at other times in other laboratories using this test method for the two specified alloys discussed in 3.4. The procedure is used for iron-, nickel-, or cobalt-based alloys in a chloride environment.3.4 A standard potentiodynamic polarization plot is included. These reference data are based on the results from five different laboratories that followed the standard procedure, using specific alloys of Type 304 stainless steel, UNS S30400 and Alloy C-276, UNS N10276.3 Curves are included which have been constructed using statistical analysis to indicate the acceptable range of polarization curves.3.5 The availability of a standard test method, standard material, and standard plots should make it easy for an investigator to check his techniques to evaluate susceptibility to localized corrosion.1.1 This test method covers a procedure for conducting cyclic potentiodynamic polarization measurements to determine relative susceptibility to localized corrosion (pitting and crevice corrosion) for iron-, nickel-, or cobalt-based alloys in a chloride environment. This test method also describes an experimental procedure which can be used to check one's experimental technique and instrumentation.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This practice provides procedures to generate and document QC data for ensuring that an XRF is operating within acceptable tolerances throughout the testing period when being used to collect lead results during a lead-based paint (LBP) inspection for the purposes of generating lead classification results.5.2 This practice is intended to supplement XRF instrument manufacturer protocols and PCSs4 through the use of QA and QC procedures to provide uniform lead testing practices among the wide variety of available field-portable XRF instruments.NOTE 1: In the United States, an XRF used to perform a lead-based paint inspection shall be utilized according to the PCS for the particular instrument model in use.5.3 While the QC results collected using this practice can provide assurances that an XRF instrument is operating within acceptable tolerances, this practice does not determine an actual level of confidence for a classification result obtained from an XRF measurement.5.4 This practice does not address selection of test locations or representative sampling for leaded paint. Additional information on conducting measurements of lead in leaded paint or other coatings may be found in Guide E2115 and the HUD Guidelines, Chapter 7.5.5 This practice involves the use of field-portable XRF instruments that may contain radioactive materials that emit X-rays and gamma rays. These instruments are intended for use only by qualified, trained personnel.5.6 The use of field-portable XRF instruments for measurement of lead may not accurately reveal low but still potentially hazardous levels of lead.1.1 This practice covers the collection and documentation of quality control (QC) measurements for determining acceptable levels of instrumental performance when using field-portable energy-dispersive X-ray fluorescence spectrometry devices (XRFs) for the purposes of generating lead classification results from measurements on paint and other coating films within buildings and related structures.1.1.1 This practice is not designed to determine the presence of a hazard as defined by authorities having jurisdiction in the United States or other jurisdictions. See Guide E2115 and the HUD Guidelines for more information.1.2 QC procedures covered in this provisional practice include the performance of calibration checks, substrate bias checks, and specific instructions for documenting the collected data for later use in reporting the results.1.3 No detailed operating instructions are provided because of differences among the various makes and models of suitable instruments. Instead, the analyst is to follow the instructions provided by the manufacturer of the particular XRF device or other relevant sources of information on XRF operation.1.4 This practice contains notes which are explanatory and are not part of the mandatory requirements of this provisional practice.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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