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ASTM C1342-96 Standard Practice for Flux Fusion Sample Distribution (Withdrawn 2001) Withdrawn, No replacement 发布日期 :  实施日期 : 

1.1 This practice covers flux fusion sample decomposition and dissolution for the determination of SiO2 as well as many other oxides in glasses, ceramics, and raw materials. The solutions are analyzed by atomic spectroscopy methods. Analyte concentrations ranging from trace to major levels can be measured in these solutions, depending on the sample weights and dilution volumes used during preparation.1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 8.

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4.1 This guide defines a procedure for testing components being considered for installation into a high-purity gas distribution system. Application of this guide is expected to yield comparable data among components tested for purposes of qualification for this installation.4.2 This guide establishes a procedure for determining the elemental composition and metallurgical characteristics of metal used to fabricate components for high purity gas distribution systems in the semiconductor industry. The composition and metallurgy of stainless steel may be expected to affect properties of importance to this application, including surface roughness, incidence of surface defects, passivation, corrosion resistance, and welding.1.1 This guide covers corrosion resistant metallic alloys of the general class stainless steel, containing chromium, nickel, manganese, and silicon as major alloying additions and possibly molybdenum, that are qualified or specified for the materials of components used in high-purity gas supply systems for the semiconductor industry. This guide is primarily intended for testing to determine conformance to applicable composition and metallurgical specifications as stated in supplier product specifications or customer purchase specifications, or both.1.2 Elements analyzed and reported in this guide are as follows:1.2.1 The alloying additions chromium, nickel, and molybdenum (if specified in alloy, as in type 316L),1.2.2 The minor elements and residuals manganese, silicon, copper, cobalt, and stabilizers such as titanium and columbium (niobium), if present,1.2.3 Carbon, sulfur and phosphorus,1.2.4 Nitrogen and oxygen gases,1.2.5 Any additional minor element additions that may be made as part of the melting and casting practice, such as aluminum and calcium,1.2.6 Available standard analytical and reporting techniques are described for these elements.1.3 Metallurgical characteristics to be analyzed and reported are inclusion contents, grain structure, mechanical properties, and intergranular corrosion susceptibility.1.4 Limitations: 1.4.1 This guide is limited to corrosion resistant metal alloys of the general class stated in the .1.4.2 The test methods cited in this guide are not intended to preclude the use of other generally accepted techniques of demonstrated equivalent or superior precision and bias.1.4.3 Inclusion of testing and analysis procedures for any given element or metallurgical characteristic in this guide is not to be construed as being a requirement for incorporation of that element or metallurgical characteristic into any specifications.1.5 The values stated in SI units are to be regarded as the standard. The inch-pound units given in parentheses are for information only.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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The determination of the boiling range distribution of gasoline by GC distillation provides an insight into the composition of the components from which the gasoline has been blended. This insight also provides essential data necessary to calculate the vapor pressure of gasoline, which has been traditionally determined by Test Method D 323. In addition, the Test Method D 86 distillation curve can be predicted using GCD data. See Annex A1.The GCD method facilitates online controls at the refinery, and its results offer improved means of describing several car performance parameters. These parameters include: (1) car-starting index, (2) vapor-lock index or vapor-liquid ratio, and (3) warm-up index. The car-starting and vapor-lock indexes have been found to be mostly affected by the front end of the Test Method D 86 distillation curve (up to about 200°F (93°C)). The warm-up index is affected by the middle and to a lesser extent by the back end of the Test Method D 86 curve, that is, the temperatures corresponding to the 50 to 90 % off range. Since the boiling range distribution provides fundamental information on composition, an improved expression for the above performance parameters may be worked out, even when the boiling range distribution curve is not smooth. Currently, car performance cannot be assessed accurately under such conditions.1.1 This test method covers the determination of the boiling range distribution of gasoline and gasoline components. This test method is applicable to petroleum products and fractions with a final boiling point of 500°F (260°C) or lower as measured by this test method.1.2 This test method is designed to measure the entire boiling range of gasoline and gasoline components with either high or low Reid vapor pressure and is commonly referred to as gas chromatography (GC) distillation (GCD).1.3 This test method has not been validated for gasolines containing oxygenated compounds (for example, alcohols or ethers).1.4 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Note 9 and 7.2.

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1.1 This test method can be used to determine the fiber length and length distribution of staple fibers of 100 mm (4 in.) or less, using the Fiber Length Measuring Unit AL-101. It includes determination of the fiber length parameters for loose fibers, carded slivers, drawn slivers, finisher slivers, combed slivers, and roving. 1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only. 1.3 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific precautionary statements, see 8.1.

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3.1 The purpose of this test method is to define a procedure for testing components being considered for installation into a high-purity gas distribution system. Application of this test method is expected to yield comparable data among components tested for the purposes of qualification for this installation.1.1 This test method covers testing components for total moisture contribution to a gas distribution system at ambient temperature. In addition, the test method allows testing at elevated ambient temperatures as high as 70°C and of the component moisture capacity and recovery.1.2 This test method applies to in-line components containing electronics grade materials such as those used in semiconductor gas distribution systems.1.3 Limitations: 1.3.1 This test method is limited by the sensitivity of current instrumentation, as well as by the response time of the instrumentation. This test method is not intended to be used for test components larger than 12.7-mm (1/2-in.) outside diameter nominal size. This test method could be applied to larger components; however, the stated volumetric flow rate may not provide adequate mixing to ensure a representative sample. Higher flow rates may improve the mixing but excessively dilute the sample.1.3.2 This test method is written with the assumption that the operator understands the use of the apparatus at a level equivalent to six months of experience.1.4 The values stated in SI units are to be regarded as the standard. The inch-pound units given in parentheses are for information only.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in Section 5.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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