4.1 Split disk and ring segment tensile tests, properly interpreted, provide reasonably accurate information with regard to the apparent tensile strength of plastic pipe when employed under conditions approximating those under which the tests are made.4.2 Ring tensile tests may provide data for research and development, engineering design, quality control, acceptance or rejection under specifications, and for special purposes. The test cannot be considered significant for applications differing widely from the load-time scale of the standard test.NOTE 1: Procedure C has been used on polyethylene and polybutylene pipe to produce results equivalent to Quick Burst results (Test Method D1599) for 4 in. to 8 in. pipes.1.1 This test method covers the determination of the comparative apparent tensile strength of most plastic products utilizing a split disk or ring segment test fixture, when tested under defined conditions of pretreatment, temperature, humidity, and test machine speed. This test method is applicable to reinforced-thermosetting resin pipe regardless of fabrication method. This test method also is applicable to extruded and molded thermoplastic pipe.Procedure A is used for reinforced-thermosetting resin pipe; Procedure B is used for thermoplastic pipe of any size; Procedure C is used for thermoplastic pipe with nominal diameter of 41/2 in. (110 mm) and greater. Procedure D is used for polyethylene pipe with a nominal diameter of 14 in. (350 mm) and greater and preferably having wall thickness 1 in. (25 mm) and greater. Procedure E is used for polyvinyl chloride (PVC) pipe with a nominal diameter of 14 in. (350 mm) and greater and having wall thickness 0.5 in. (12.7 mm) and greater.1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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5.1 The vapor pressure of a substance as determined by measurement of evaporation reflects a property of the bulk sample. Little weight is given by the procedure to the presence of low concentrations of volatile impurities.5.2 Vapor pressure, per se, is a thermodynamic property that is dependent only upon composition and temperature for stable systems. In the present method, composition changes occur during the course of the test so that the contribution of minor amounts of volatile impurities is minimized.1.1 This test method covers a calculation procedure for converting data obtained by Test Method D972 to apparent vapor pressures and molecular weights. It has been demonstrated to be applicable to petroleum-based and synthetic ester lubricating oils,2 at temperatures of 395 K to 535 K (250 °F to 500 °F). However, its applicability to lubricating greases has not been established.NOTE 1: Most lubricants boil over a fairly wide temperature range, a fact recognized in discussion of their vapor pressures. For example, the apparent vapor pressure over the range 0 % to 0.1 % evaporated may be as much as 100 times that over the range 4.9 % to 5.0 % evaporated.1.2 The values stated in SI units are to be regarded as the standard. In cases in which materials, products, or equipment are available in inch-pound units only, SI units are omitted.1.3 WARNING—Mercury has been designated by many regulatory agencies as a hazardous substance that can cause serious medical issues. Mercury, or its vapor, has been demonstrated to be hazardous to health and corrosive to materials. Use caution when handling mercury and mercury-containing products. See the applicable product Safety Data Sheet (SDS) for additional information. The potential exists that selling mercury or mercury-containing products, or both, is prohibited by local or national law. Users must determine legality of sales in their location.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability or regulatory limitations prior to use. For specific warning statements, see 6.2, 7.1, 8.2, and Annex A2.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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4.1 The suitability of a dispersion resin for any given application is dependent upon its viscosity characteristics.4.2 The extrusion viscosity defines the flow behavior of a plastisol or organosol under high shear. This viscosity relates to the conditions encountered in mixing, pumping, knife coating, roller coating, and spraying processes.1.1 This test method covers the measurement of plastisol and organosol viscosity at high shear rates by means of an extrusion viscometer.1.2 Apparent viscosity at low shear rates is covered in Test Method D1824.1.3 The values stated in SI units are to be regarded as standard. The values in parentheses are given for information only.1.4 This standard does not purport to address the safety concerns associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.NOTE 1: This standard and ISO 4575-2007 address the same subject matter, but differ in technical content.
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5.1 When an engine oil is cooled, the rate and duration of cooling can affect its yield stress and viscosity. In this laboratory test, a fresh engine oil is slowly cooled through a temperature range where wax crystallization is known to occur, followed by relatively rapid cooling to the final test temperature. These laboratory test results have predicted as failures the known engine oils that have failed in the field because of lack of oil pumpability.4 These documented field failing oils all consisted of oils normally tested at –25 °C. These field failures are believed to be the result of the oil forming a gel structure that results in either excessive yield stress or viscosity of the engine oil, or both.5.2 Cooling Profiles: 5.2.1 For oils to be tested at −20 °C or colder, Table X1.1 applies. The cooling profile described in Table X1.1 is based on the viscosity properties of the ASTM Pumpability Reference Oils (PRO). This series of oils includes oils with normal low-temperature flow properties and oils that have been associated with low-temperature pumpability problems (1-5).5 Significance for the −35 °C and −40 °C temperature profiles is based on the data collected from the “Cold Starting and Pumpability Studies in Modern Engines” conducted by ASTM (6, 7).5.2.2 For oils to be tested at −15 °C or −10 °C, Table X1.2 applies. No significance has been determined for this temperature profile because of the absence of appropriate reference oils. Similarly, precision of the test method using this profile for the −10 °C test temperature is unknown. The temperature profile of Table X1.2 is derived from the one in Table X1.1 and has been moved up in temperature, relative to Table X1.1, in consideration of the expected higher cloud points of the viscous oils tested at −15 °C and −10 °C.1.1 This test method covers the measurement of the yield stress and viscosity of engine oils after cooling at controlled rates over a period exceeding 45 h to a final test temperature between –10 °C and –40 °C. The precision is stated for test temperatures from –40 °C to –15 °C. The viscosity measurements are made at a shear stress of 525 Pa over a shear rate of 0.4 s–1 to 15 s–1. The viscosity as measured at this shear stress was found to produce the best correlation between the temperature at which the viscosity reached a critical value and borderline pumping failure temperature in engines.1.2 This test method contain two procedures: Procedure A incorporates several equipment and procedural modifications from Test Method D4684–02 that have shown to improve the precision of the test, while Procedure B is unchanged from Test Method D4684–02. Additionally, Procedure A applies to those instruments that utilize thermoelectric cooling technology or direct refrigeration technology of recent manufacture for instrument temperature control. Procedure B can use the same instruments used in Procedure A or those cooled by circulating methanol.1.3 Procedure A of this test method has precision stated for a yield range from less than 35 Pa to 210 Pa and apparent viscosity range from 4300 mPa·s to 270 000 mPa·s. The test procedure can determine higher yield stress and viscosity levels.1.4 This test method is applicable for unused oils, sometimes referred to as fresh oils, designed for both light duty and heavy duty engine applications. It also has been shown to be suitable for used diesel and gasoline engine oils. The applicability to petroleum products other than engine oils has not been determined.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5.1 Exception—This test method uses the SI based unit of milliPascal second (mPa·s) for viscosity which is equivalent to, centiPoise (cP).1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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This test method deals with the standards for the measurement of apparent viscosity of roofing bitumen by mean of a parallel plate plastometer. This method involves measuring viscosity using pre-determined arbitrary shear stress levels. The method involves molding the sample into a disc of specified dimensions, heating it to a selected temperature and placing it between the plates of a pre-heated apparatus and pressing under the standard conditions for a measured time.1.1 This test method covers the measurement of apparent viscosity of roofing bitumen by means of a parallel plate plastometer. This test method is applicable for a viscosity range from 102 to 109 Pa·s [103 to 1010 poises]. See Note 1.NOTE 1: This relatively simple test method of measuring viscosity uses predetermined, arbitrary shear stress levels. Since roofing bitumens are non-Newtonian, other viscosity test methods may give different results.1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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5.1 The apparent density is an important measure of a material characteristic of the powder that is useful to the powder producers and powder users in determining quality and lot to lot consistency.5.2 This test method is applicable to free-flowing and non-free-flowing metal powders, lubricated powder mixtures and metal compounds.5.3 The apparent density of a lubricated metal powder mixture may be different when a quantity settles after falling into the die cavity during automated compacting compared with the value obtained from a measurement taken in the laboratory under controlled test conditions.5.4 This test method simulates the action of the feed shoe on a powder compacting press and gives an apparent density value that closely approximates the apparent density of the powder in the die cavity after the production filling operation.5.5 Knowledge of this apparent density value for the final lubricated production powder mixture is very helpful to the powder metallurgy (PM) parts fabricator to set the compression ratios for fixed fill die cavity tooling.5.6 The values of apparent density obtained on metal powders with this test method are approximately 0.2 g/cm3 higher than those obtained using the Hall Funnel, Test Method B212, the Carney Funnel, Test Method B417; or the Scott Volumeter, Test Method B329.5.7 This test method may be part of a purchase agreement between the powder producer and PM parts producer, or it may be an internal quality control test for either party.1.1 This test method covers a quantitative laboratory procedure for determining the apparent density of both free-flowing and non-free-flowing metal powders, lubricated metal powder mixtures, and powder compounds.1.2 Units—With the exception of the values for mass, volume, and density, for which the use of the gram and the cubic centimetre units is the long-standing industry practice, the values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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5.1 This test method is applicable to cementitious mixtures that have not been exposed to external chloride ions, other than the negligible quantity of chloride ion exposure from sample preparation using potable water, prior to the test.5.2 The calculation procedure described in this test method is applicable only to laboratory test specimens exposed to a sodium chloride solution as described in this test method. This calculation procedure is not applicable to specimens exposed to chloride ions during cyclic wetting and drying.NOTE 1: The diffusion of ionic species in concrete occurs within the fluid-filled pores, cracks and void spaces. The concentration and valence of other ionic species in the pore fluid also influence the rate of chloride diffusion, and therefore, the apparent diffusion coefficient as determined by this test procedure.5.3 In most cases, the value of the apparent chloride diffusion coefficient for cementitious mixtures changes over time (see Note 2). Therefore, apparent diffusion coefficients obtained at early ages may not be representative of performance in service.NOTE 2: The rate of change of the apparent diffusion coefficient for cementitious mixtures containing pozzolans or blast-furnace slag is typically different than that for mixtures containing only portland cement.5.4 The apparent chloride diffusion coefficient is used in Fick's second law of diffusion to estimate chloride penetration into cementitious mixtures that are in a saturated condition.5.5 The apparent chloride diffusion coefficient is commonly used in chloride ingress models based on Fick's second law of diffusion. The apparent diffusion coefficient determined by this method includes bound chloride, so proper use of the apparent chloride diffusion coefficient to predict chloride ingress requires consideration of chloride binding.5.6 The resistance to chloride penetration is affected by such factors as the environment, finishing, mixture composition, workmanship, curing, and age.1.1 This test method covers the laboratory determination of the apparent chloride diffusion coefficient for hardened cementitious mixtures.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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5.1 When an engine oil is cooled, the rate and duration of cooling can affect its yield stress and viscosity. In this laboratory test, used engine oil is slowly cooled through a temperature range where wax crystallization is known to occur, followed by relatively rapid cooling to the final test temperature. As in other low temperature rheological tests such as Test Methods D3829, D4684, and D5133, a preheating condition is required to ensure that all residual waxes are solubilized in the oil prior to the cooldown (that is, remove thermal memory). However, it is also known that highly sooted used diesel engine oils can experience a soot agglomerization phenomenon when heated under quiescent conditions. The current method uses a separate preheat and agitation step to break up any soot agglomerization that may have occurred prior to cooldown. The viscosity of highly sooted diesel engine oils as measured in this test method have been correlated to pressurization times in a motored engine test (1).45.2 Cooling Profiles: 5.2.1 For oils to be tested at –20 °C and –25 °C, Table X1.1 applies. The cooling profile described in Table X1.1 is based on the viscosity properties of the ASTM Pumpability Reference Oils (PRO). This series of oils includes oils with normal low-temperature flow properties and oils that have been associated with low-temperature pumpability problems (2-7).1.1 This test method covers the measurement of the yield stress and viscosity of engine oils after cooling at controlled rates over a period of 43 h or 45 h to a final test temperature of –20 °C or –25 °C. The precision is stated for test temperatures –20 °C and –25 °C. The viscosity measurements are made at a shear stress of 525 Pa over a shear rate of 0.4 s-1 to 15 s-1. This test method is suitable for measurement of viscosities ranging from 4000 mPa·s to >400 000 mPa·s, and is suitable for yield stress measurements of 7 Pa to >350 Pa.1.2 This test method is applicable for used diesel oils. The applicability and precision to other used or unused engine oils or to petroleum products other than engine oils has not been determined.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3.1 Exception—This test method uses the SI based unit of milliPascal second (mPa·s) for viscosity which is equivalent to centiPoise (cP).1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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