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3.1 These test methods are designed to broaden the scope of the earlier editions of the test method by the inclusion of tall oil and tall oil derived products as test materials and will be referenced in Test Methods D803.3.2 The acid number is an important property of pine chemical products, such as tall oil, and the products obtained by the fractionation of tall oil. It is the test method widely used to determine the total free acid content of these products.3.3 The potentiometric test method should be used when the most reproducible results are required.1.1 These test methods are intended for determining the acid number of pine chemical products as defined in Terminology D804 including tall oil products, wood and gum rosin, and other related materials. These test methods may not be applicable to all modified rosin products. Two test methods are covered, as follows:1.1.1 Potentiometric method (referee), and1.1.2 Internal indicator method (alternate).1.2 The potentiometric method is suitable for use with both light- and dark-colored products. It should be considered the referee method. The internal indicator method is suitable for use only with light- and medium-colored products with a Gardner color of less than 12. It should be considered the alternate method.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 New and used petroleum products can contain basic constituents that are present as additives or as degradation products formed during service. The amount of these additives in an oil can be determined by titrating against an acid. The base number is a measure of the amount of basic substance in the oil, always under the conditions of the test. A decrease in base number is often used as a measure of lubricant degradation, but any condemning limits must be empirically established.5.2 This test method uses reagents that are considered less hazardous than most reagents used in alternate base number methods. It uses pre-packaged reagents to facilitate base number determinations in the field where scientific equipment is unavailable and quick results are at a premium.NOTE 1: Results obtained by this test method3 are similar to those obtained by Test Method D2896.1.1 This test method covers a procedure for determining the basic constituents in petroleum products in the field or laboratory using a pre-packaged test kit. The test uses a micro-titration resulting in a visual endpoint facilitated by a color indicator.1.1.1 This test method covers base numbers from 0 to 20. It can be extended to higher ranges by diluting the sample or by using a smaller sample size; however, the precision data were obtained for base numbers up to 20.1.2 This test method can be used to indicate relative changes that occur in an oil during use under oxidizing conditions. Although the test is performed under closely specified conditions with standardized reagents, the test method does not measure an absolute basic property that can be used to predict performance of an oil under service conditions. No general relationship between bearing corrosion and base number is known.1.3 The values stated in SI units are to be regarded as the standard.1.3.1 Exception—The values given in parentheses are for information only.1.4  This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 New and used petroleum products can contain basic constituents that are present as additives. The relative amounts of these materials can be determined by titration with acids. The base number is a measure of the amount of basic substance in the oil, always under the conditions of the test. It is sometimes used as a measure of lubricant degradation in service; however, any condemning limits must be empirically established.1.1 This test method covers the determination of basic constituents in petroleum products by titration with perchloric acid in glacial acetic acid.1.2 Procedures A and B use different titration solvent volumes and sample weights.NOTE 1: A round robin on a series of new and used oils and additive concentrates has shown that the two procedures give statistically equivalent results.1.3 Appendix X2 provides the use of an alternative solvent system which eliminates the use of chlorobenzene in this test method. The use of the alternative solvent gives statistically equivalent results; however, the precision is worse. Paragraph X2.5.5 provides guidance when comparing results using the two different solvents.1.4 The constituents that may be considered to have basic characteristics include organic and inorganic bases, amino compounds, salts of weak acids (soaps), basic salts of polyacidic bases, and salts of heavy metals.NOTE 2: This test method is applicable to both fresh oils and used oils as described in Sections 16, 17, and 19 and Appendix X1.1.5 This test method can be used to determine base number >300 mg KOH/g. However, the precision statement in Section 19 has been obtained only on base number ≤300 mg KOH/g.1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see Section 7, Section 10, and X2.2.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This procedure describes a rapid and sensitive method for estimating the stability reserve of an oil. The stability reserve is estimated in terms of a separability number, where a low value of the separability number indicates that there is a stability reserve within the oil. When the separability number is between 0 to 5, the oil can be considered to have a high stability reserve and asphaltenes are not likely to flocculate. If the separability number is between 5 to 10, the stability reserve in the oil will be much lower. However, asphaltenes are, in this case, not likely to flocculate as long as the oil is not exposed to any worse conditions, such as storing, aging, and heating. If the separability number is above 10, the stability reserve of the oil is very low and asphaltenes will easily flocculate, or have already started to flocculate.5.2 This test method can be used by refiners and users of oils, for which this test method is applicable, to estimate the stability reserves of their oils. Hence, this test method can be used by refineries to control and optimize their refinery processes. Consumers of oils can use this test method to estimate the stability reserve of their oils before, during, and after storage.FIG. 1 Schematic Representation of a Typical Measurement Using an Optical Scanning Device5.3 This test method is not intended for predicting whether oils are compatible before mixing, but can be used for determining the separability number of already blended oils. However, oils that show a low separability number are more likely to be compatible with other oils than are oils with high separability numbers.1.1 This test method covers the quantitative measurement, either in the laboratory or in the field, of how easily asphaltene-containing heavy fuel oils diluted in toluene phase separate upon addition of heptane. This is measured as a separability number (%) by the use of an optical scanning device.1.2 The test method is limited to asphaltene-containing heavy fuel oils. ASTM specification fuels that generally fall within the scope of this test method are Specification D396, Grade Nos. 4, 5, and 6, Specification D975, Grade No. 4-D, and Specification D2880, Grade Nos. 3-GT and 4-GT. Refinery fractions from which such blended fuels are made also fall within the scope of this test method.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM C1150-96 Standard Test Method for the Break-Off Number of Concrete (Withdrawn 2002) Withdrawn, No replacement 发布日期 :  1970-01-01 实施日期 : 

1.1 This test method covers determination of the break-off number of hardened concrete in test specimens or structures, by measuring the force required to cause failure of a pre-cast or drilled core specimen loaded as a cantilever. 1.2 The values stated in SI units are to be regarded as the standard. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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2.1 This test method is intended for use in the determination of the acidity as free fatty acids in the absence of ammonium or triethanolamine soaps in sulfonated and sulfated oils for the purpose of quality assurance.1.1 This test method covers the determination of the acidity as free fatty acids existing in a sample of sulfonated or sulfated oil, or both, by titrating the sample dissolved in a solvent. It is not applicable in the presence of ammonium or triethanolamine soaps or salts or other compounds that do not react neutral to phenolphthalein when dissolved in alcohol.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D1832-04(2009) Standard Test Method for Peroxide Number of Petroleum Wax (Withdrawn 2014) Withdrawn, No replacement 发布日期 :  1970-01-01 实施日期 : 

The magnitude of the peroxide number is an indication of the quantity of oxidizing constituents present. Deterioration of petroleum wax results in the formation of peroxides and other oxygen-carrying compounds. The peroxide number measures those compounds that will oxidize potassium iodide.1.1 This test method covers the determination of the peroxide number of petroleum wax.1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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5.1 This test method measures the acid number of oils obtained from laboratory oxidation tests using smaller amounts of sample than Test Methods D974 or D664. It has specific application in Test Method D943 in which small aliquots of oil are periodically removed for testing by Test Method D3339. This test method, therefore, provides a means of monitoring the relative oxidation of oils, by measuring changes in acid number, at different time intervals and under the various oxidizing test conditions.1.1 This test method covers the determination of acidic constituents in new or used petroleum products and lubricants soluble or nearly soluble in mixtures of toluene, and isopropyl alcohol. The test method is especially intended for cases in which the amount of sample available to be analyzed is too small to allow accurate analysis by Test Methods D974 or D664. It is applicable for the determination of acids having dissociation constants in water larger than 10−9. Extremely weak acids having dissociation constants smaller than 10−9 do not interfere. Salts titrate if their hydrolysis constants are larger than 10−9.1.2 This test method can be used to indicate relative changes in acid number that occur in an oil during use under oxidizing conditions. Although the titration is made under definite equilibrium conditions, the method does not measure an absolute acidic property that can be used to predict performance of an oil under service conditions. No general relationship between bearing corrosion and acid number is known.1.3 Since this test method requires substantially less sample than Test Methods D974 or D664, it provides an advantageous means of monitoring an oxidation test by changes in acid number by (1) minimizing test sample depletion for acid number analyses and thus minimizing the disturbance of the test or (2) allowing additional acid number analyses to be made while maintaining the same test sample depletion and thus providing additional data.NOTE 1: Some oils, such as many cutting oils, rust-proofing oils, and similar compounded oils, or excessively dark-colored oils, may be more difficult to analyze by this test method due to obscurity of the color-indicator end point. These oils can be analyzed by Test Method D664 provided sufficient sample is available. However, this situation is much less likely using Test Method D3339 than using Test Method D974 due to the use of a more highly dilute sample during the titration and due to the greater stability of the end point color change. The acid numbers obtained by Test Method D3339 may or may not be numerically the same as those obtained by Test Method D664 but they should be of the same order of magnitude.NOTE 2: The results obtained using this method have been found to be numerically the same as those obtained using Test Method D974, within the precision of the two methods, for new or oxidized lubricants of the type primarily intended for hydraulic or steam turbine type service. The oxidized lubricants were obtained using the Test Method D943 oxidation test. This correlation is shown by the correlation coefficient r = 0.989 with slope s = + 1.017 and intercept y = + 0.029, calculated using the acid numbers obtained using both titration methods for the samples used for the precision statement (12.2).21.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see Sections 7 and 9, A1.1.4, A2.3.1, and A2.10.1.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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3.1 This test method is intended for use in the determination of the acid number of sulfonated and sulfated oils for the purpose of quality assurance.1.1 This test method covers determination of the acidity as free fatty acids in the presence of ammonium or triethanolamine soaps, or both, existing in a sample of sulfonated or sulfated oil, or both, by calculation from the total alkalinity and free-and-alkali combined fatty acids.1.2 The values stated in SI units are to be regarded as standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Petroleum products can contain additives that react with alkali to form metal soaps. Fats are examples of such additives. Also, certain used engine oils, especially from turbine or internal combustion engines, can contain chemicals that will similarly react with alkali. The saponification number expresses the amount of base that will react with 1 g of sample when heated in a specific manner. This then gives an estimation of the amount of acid present in the sample, that is, any free acid originally present plus any combined (for example, in esters) that have been converted to metal soaps during the heating procedure.5.2 Saponification numbers are also used in setting product specifications for lubricants and additives.1.1 These test methods cover the determination of the amount of constituents in petroleum products such as lubricants, additives, and transmission fluids that will saponify under the conditions of the test.NOTE 1: Statements defining this test and its significance when applied to electrical insulating oils of mineral origin will be found in Guide D117. Experience has shown that for transformer oils, Test Method D94, modified by use of 0.1 M KOH solution and 0.1 M HCl, is more suitable.1.1.1 Two test methods are described: Method A—Color Indicator Titration (Sections 6 – 13), and Method B—Potentiometric Titration (Sections 14 – 23).1.2 Because compounds of sulfur, phosphorus, the halogens, and certain other elements that are sometimes added to petroleum products also consume alkali and acids, the results obtained indicate the effect of these extraneous materials in addition to the saponifiable material present. Results on products containing such materials, on used internal-combustion-engine crankcase oils, and on used turbine oils must be interpreted with caution.NOTE 2: The materials referred to above, which are not normally considered saponifiable matter, include inorganic or certain organic acids, most nonalkali soaps, and so forth. The presence of such materials increases the saponification number above that of fatty saponifiable materials for which the test method is primarily intended. The odor of hydrogen sulfide near the end of the back-titration in the saponification test is an indication that certain types of reactive sulfur compounds are present in the sample. In the case of other reactive sulfur, chlorine, and phosphorus compounds and other interfering materials, no simple indication is given during the test. A gravimetric determination of the actual amount of fatty acids is probably the most reliable method for such compounds. Test Methods D128 or IP Method 284/86 can be used to determine fatty acids gravimetrically.1.3 The values stated in SI units are to be regarded as the standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Sections 6, 7, 8, 10, 15, 16, 17, and 19.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 New and used petroleum products, biodiesel, and blends of biodiesel may contain acidic constituents that are present as additives or as degradation products formed during service, such as oxidation products. The relative amount of these materials can be determined by titrating with bases. The acid number is a measure of this amount of acidic substance in the oil, always under the conditions of the test. The acid number is used as a guide in the quality control of lubricating oil formulations. It is also sometimes used as a measure of lubricant degradation in service. Any condemning limits must be empirically established.5.2 Since a variety of oxidation products contribute to the acid number and the organic acids vary widely in corrosion properties, the test method cannot be used to predict corrosiveness of oil or biodiesel and blends under service conditions. No general correlation is known between acid number and the corrosive tendency of biodiesel and blends or oils toward metals.1.1 This test method covers procedures for the determination of acidic constituents in petroleum products, lubricants, biodiesel, and blends of biodiesel.1.1.1 Test Method A—For petroleum products and lubricants soluble or nearly soluble in mixtures of toluene and propan-2-ol. It is applicable for the determination of acids whose dissociation constants in water are larger than 10–9; extremely weak acids whose dissociation constants are smaller than 10–9 do not interfere. Salts react if their hydrolysis constants are larger than 10–9. The range of acid numbers included in the precision statement is 0.1 mg/g KOH to 150 mg/g KOH.1.1.2 Test Method B—Developed specifically for biodiesel and biodiesel blends with low acidity and slightly different solubility. This test method requires the use of an automatic titrator with automatic endpoint-seeking capability.NOTE 1: In new and used oils, the constituents that may be considered to have acidic characteristics include organic and inorganic acids, esters, phenolic compounds, lactones, resins, salts of heavy metals, salts of ammonia and other weak bases, acid salts of polybasic acids, and addition agents such as inhibitors and detergents.1.2 The test method may be used to indicate relative changes that occur in oil during use under oxidizing conditions regardless of the color or other properties of the resulting oil. Although the titration is made under definite equilibrium conditions, the test method is not intended to measure an absolute acidic property that can be used to predict performance of oil under service conditions. No general relationship between bearing corrosion and acid number is known.NOTE 2: The acid number obtained by this standard may or may not be numerically the same as that obtained in accordance with Test Methods D974 and D3339. There has not been any attempt to correlate this method with other non-titration methods.NOTE 3: A few laboratories have made the observation that there is a difference in Test Method D664 results when aqueous versus nonaqueous buffers are used.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D613-24 Standard Test Method for Cetane Number of Diesel Fuel Oil Active 发布日期 :  1970-01-01 实施日期 : 

5.1 The cetane number provides a measure of the ignition characteristics of diesel fuel oil in compression ignition engines.5.2 This test method is used by engine manufacturers, petroleum refiners and marketers, and in commerce as a primary specification measurement related to matching of fuels and engines.5.3 Cetane number is determined at constant speed in a precombustion chamber type compression ignition test engine. The relationship of test engine performance to full scale, variable speed, variable load engines is not completely understood.5.4 This test method may be used for unconventional fuels such as synthetics, vegetable oils, and the like. However, the relationship to the performance of such materials in full scale engines is not completely understood.1.1 This test method covers the determination of the rating of diesel fuel oil in terms of an arbitrary scale of cetane numbers using a standard single cylinder, four-stroke cycle, variable compression ratio, indirect injected diesel engine.1.2 The cetane number scale covers the range from zero (0) to 100, but typical testing is in the range of 30 to 65 cetane number.1.3 The values for operating conditions are stated in SI units and are to be regarded as the standard. The values given in parentheses are the historical inch-pound units for information only. In addition, the engine measurements continue to be in inch-pound units because of the extensive and expensive tooling that has been created for these units.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For more specific warning statements, see Annex A1.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This is a quick method used for the determination of the approximate yarn number of short-length specimens taken from packages or fabrics.5.2 Because any error present in the reported length of the specimen is multiplied many times when calculating the theoretical yarn number using Eq 2 or Eq 3, it is extremely important that the length be measured as precisely as practicable.5.3 For the analysis of fabrics, this test method is adequate for estimating the approximate yarn number of the yarn used to weave or knit the fabric, but the results obtained by this test method may not agree with the nominal yarn number of the yarns actually used to make the fabric because of the changes in the yarn number produced by the weaving or knitting operations, the finishing treatments, and the dissecting operations. This test method is suitable for the evaluation of yarns as they occur in the finished fabric, when that information is needed.5.4 The yarn number obtained from the lengths taken from packages should not be expected to agree exactly with the values obtained by the use of the more precise methods of determining the yarn number included in Test Method D1907. If a sufficient number of consecutive specimens were tested, however, a close agreement with Option 1 of Test Method D1907 can be expected.5.5 This test method is designed to measure the yarn number of the single yarns present as a component of a plied yarn and the yarn number of the original single yarns used to produce a high twist yarn for a crepe fabric.5.6 This test method is not recommended for acceptance testing because of the short lengths used. In some cases, the purchaser and the supplier may have to test a commercial shipment of one or more specific materials by the best available method, even though the method has not been recommended for acceptance testing of commercial shipments.5.6.1 In such a case, if there is disagreement arising from the differences in values reported by the purchaser and supplier when using this method for acceptance testing, the statistical bias, if any, between the laboratory of the purchaser and the laboratory of the supplier should be determined with each comparison being based on testing specimens randomly drawn from one sample of material of the type being evaluated.1.1 This test method covers the determination of the yarn number of all types of cotton, woolen, worsted, and man-made fiber yarns taken from packages; or from any textile fabrics in which the yarns are intact and can be removed in measurable lengths. The test method is not applicable to yarns taken from napped or cut pile fabrics. Because this test method is based on short-length specimens, the results should only be considered as approximations of yarn number.NOTE 1: For a more precise procedure for the determination of yarn number, refer to Test Method D1907.NOTE 2: The following additional methods for the determination of yarn number have been approved for yarns made from specific fibers: Specification D541, D578, and D681.1.2 This test method is applicable to yarns which stretch less than 5 % when tension on yarn is increased from 0.25 to 0.75 cN/tex (0.25 to 0.75 gf/tex). By mutual agreement it may be adapted to yarns which stretch more than 5 % by use of tension lower than that specified in the method for elastomers or use of tension higher than that specified in the method to pull the crimp out of textured yarns.1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 The ability to absorb kerosine is an indication of the ability to absorb hot asphalt. The kerosine number is used in calculating saturation efficiency.1.1 This test method covers the determination of the relative saturating capacity of unsaturated (dry) felt papers used in roofing.1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 The rubber-filler interaction needed in silica technology for the rubber industry is based on the use of silane-coupling agents that react with the silanol groups on the surface of the silica during the processing step called silanization. Silane-coupling agents are multifunctional molecules able to create molecular bridges between the elastomer or rubber matrix and the silica surface.1.1 This test method is used to determine the number of silanol groups on the surface of silica by titration according to a method as developed by Sears. This test method is suitable for characterizing rubber-grade silicas.1.2 Units—The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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