4.1 Guide G96 describes a linear-polarization method and an electrical resistance method for online monitoring of corrosion in plant equipment without the need to enter the system physically to withdraw coupons. These two online monitoring techniques are useful in systems in which process upsets or other problems can create corrosive conditions. An early warning of corrosive attack can permit remedial action before significant damage occurs to process equipment. The two methods described in Guide G96 are suitable for uniform corrosion, but may not be sensitive enough for non-uniform corrosion, especially localized corrosion. This guide describes a new method for monitoring non-uniform corrosion, especially localized corrosion.4.2 The CMAS technique measures the net anodic current or net cathodic current from each of the individual electrodes (Iaex or Icex in Fig. 1), which is the characteristic of non-uniform corrosion such as localized corrosion and uneven general corrosion. Therefore, the CMAS technique can be used to estimate the rate of uneven general corrosion and localized corrosion (see Section 5).FIG. 1 Principle of CMAS ProbeNOTE 1: The upper section shows the electron flows from the corroding area to the less corroding areas inside a metal when localized corrosion takes place; the lower section shows the electron flows after the anodic and cathodic areas are separated into individual small electrodes and coupled through an external circuit that measures the anodic current (Iaex) and cathodic current (Icex) through each of the individual electrodes (4).4.3 Unlike uniform corrosion, the rate of non-uniform corrosion, especially localized corrosion, can vary significantly from one area to another area of the same metal exposed to the same environment. Allowance shall be made for such variations when the measured non-uniform corrosion rate is used to estimate the penetration of the actual metal structure or the actual wall of process equipment. This variability is less critical when relative changes in corrosion rate are to be detected, for example, to track the effectiveness of corrosion inhibitors in an inhibited system.4.4 The same as the method described in Guide G96, the CMAS technique described in this guide provides a technique for determining corrosion rates without the need to enter the system physically to withdraw coupons as required by the methods described in Guide G4.4.5 The same as the methods described in Guide G96, the CMAS technique is useful in systems in which process upsets or other problems can create corrosive conditions. An early warning of corrosive attack can permit remedial action before significant damage occurs to process equipment.4.6 The CMAS technique provides the instantaneous corrosion rate within 10 s to 40 s making it suitable for automatic corrosion inhibitor dosing control.4.7 The CMAS technique is an online technique and may be used to provide real-time measurements for internal corrosion of pipelines and process vessels, external corrosion of buried pipes and structures, and atmospheric corrosion of metal structures.1.1 This guide outlines the procedure for conducting corrosion monitoring in laboratories and plants by use of the coupled multielectrode array sensor (CMAS) technique.1.2 For plant applications, this technique can be used to assess the instantaneous non-uniform corrosion rate, including localized corrosion rate, on a continuous basis, without removal of the monitoring probes, from the plant.1.3 For laboratory applications, this technique can be used to study the effects of various testing conditions and inhibitors on non-uniform corrosion, including pitting corrosion and crevice corrosion.1.4 Units—The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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5.1 This practice provides a means for the users of ASTM Committee D02 standards to monitor the drift in sensed temperature of liquid-in-glass thermometer (LiG), and digital contact thermometers (DCT). Digital contact thermometers are sometimes referred to as portable electronic thermometers (PET) or simply digital thermometers.5.2 This practice is not suitable for determining the accuracy or calibration of a temperature-measuring device as the error in the ice bath temperature can be greater than 0.02 °C. For greater accuracy, the user should use Practice E563 to prepare the ice bath.5.3 The ice point is a common practical industrial reference point of thermometry. The ice point is relatively simple to realize and provides a readily available natural fixed-point reference temperature.5.4 This practice only checks the measurement drift at a single temperature. It will not detect a change in measurement response with change in temperature. Temperature-measuring devices should be recalibrated at set intervals. See device supplier for recommendations.5.5 This practice provides a technique to determine minimum immersion depth of the sensing probe of the thermometer using an ice bath. The minimum immersion depth determined by this practice may change when the differential temperature differs significantly from the conditions described. A greater differential will likely increase the minimum immersion depth.1.1 This practice describes two procedures for use with temperature measurement devices. Methodology is described for determining minimum immersion depth for thermal sensors, in particular RTDs or similar temperature sensors. Included is a procedure for consistently preparing a reference bath for the purpose of monitoring measurement drift of thermal sensors such as liquid-in-glass or digital contact thermometers.1.2 This practice focuses on temperature measurement drift in a laboratory. If the user requires greater measurement accuracy, then they should follow the instructions in Practice E563.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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3.1 Degradation in sensor performance can occur due to dropping, mechanical shock while mounted on the test structure, temperature cycles, and so forth. It is necessary and desirable to have a simple measurement procedure that will check the consistency of sensor response, while holding all other variables constant.3.2 While test blocks of many different kinds have been used for this purpose for many years, an acrylic polymer rod offers the best all-around combination of suitable acoustic properties, practical convenience, ease of procurement and low cost.3.3 Because the acoustic properties of the acrylic rod are known to depend on temperature, this practice requires that the rod, sensors, and couplant be stabilized at the same working temperature, prior to verifying the sensors.3.4 Attention should be paid to storage conditions for the acrylic polymer rod. For example, it should not be left in a freezing or hot environment overnight, unless it is given time for temperature stabilization before use.3.5 Properly applied and with proper record keeping, this practice can be used in many ways. The user organization must determine the context for its use, the acceptance standards and the actions to be taken based on the lead break results. The following uses are suggested:3.5.1 To determine when a sensor is no longer suitable for use.3.5.2 To check sensors that have been exposed to high-risk conditions, such as dropping, overheating, and so forth.3.5.3 To get an early warning of sensor degradation over time. This can lead to identifying conditions of use, which are damaging sensors, and thus, to better equipment care and lower replacement costs.3.5.4 To obtain matched sets of sensors, preamplifiers, instrumentation channels, or a combination thereof, for more uniform performance of the total system.3.5.5 To save time and money, by eliminating the installation of bad sensors.3.5.6 To verify sensors quickly but consistently in the field and to assist trouble-shooting when a channel does not pass a performance check.FIG. 1 Acrylic Rod Description3.6 All the above uses are recommended for consideration. The purpose of this practice is not to call out how these uses are to be implemented, but only to state how the test itself is to be performed so that the results obtained will be accurate and reliable.1.1 This practice is used for routinely checking the sensitivity of acoustic emission (AE) sensors. It is intended to provide a reliable, precisely specified way of comparing a set of sensors, or telling whether an individual sensor's sensitivity has degraded during its service life, or both.1.2 This practice is not a “calibration” nor does it give frequency response information.1.3 Units—The values stated in SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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5.1 Oxygen gas transmission rate is an important determinant of the protection afforded by barrier materials. It is not, however, the sole determinant, and additional tests, based on experience, must be used to correlate package performance with O2GTR. This test method is suitable as a referee method of testing, provided that the user and source have agreed on sampling procedures, standardization procedures, test conditions, and acceptance criteria.1.1 This test method covers a procedure for the determination of the steady-state rate of transmission of oxygen gas into packages. More specifically, the method is applicable to packages that in normal use will enclose a dry environment.1.2 The values stated in SI units are to be regarded as the standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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5.1 Eddy current methods are used for nondestructively locating and characterizing discontinuities and geometric property variations in magnetic or nonmagnetic electrically conducting materials. Conformable eddy current sensor arrays permit examination of planar and non-planar materials but usually require suitable fixtures to hold the sensor array near the surface of the material of interest, such as a layer of foam behind the sensor array along with a rigid support structure.5.2 In operation, the sensor arrays are standardized with measurements in air or a reference part, or both. Responses measured from the sensor array may be converted into physical property values, such as lift-off, electrical conductivity, or magnetic permeability, or a combination thereof. Proper instrument operation is verified by ensuring that these measurement responses or property values are within a prescribed range. Performance verification is performed periodically. Performance verification on a discontinuity-free reference standard or regions of the material being examined that do not contain discontinuities ensures that the electrical and geometric properties, such as electrical conductivity, layer thickness, or lift-off, or a combination thereof, are appropriate for the sensor array. Performance verification on a discontinuity-containing reference standard ensures that the sensor array response to the discontinuity is appropriate.5.3 The sensor array dimensions, including the size and number of sense elements, and the operating frequency are selected based on the type of examination being performed. The depth of penetration of eddy currents into the material under examination depends upon the frequency of the signal, the electrical conductivity and magnetic permeability of the material, and some dimensions of the sensor array. The depth of penetration is equal to the conventional skin depth at high frequencies but is also related to the sensor array dimensions at low frequencies, such as the size of the drive winding and the gap distance between the drive winding and sense element array. For surface-breaking discontinuities on the surface adjacent to the sensor array, high frequencies should be used where the penetration depth is less than the thickness of the material under examination. For subsurface discontinuities or wall thickness measurements, lower frequencies and larger sensor dimensions should be used so that the depth of penetration is comparable to the material thickness.5.4 Insulating layers or coatings may be present between the sensor array and the surface of the electrically conducting material under examination. The sensitivity of a measurement to a discontinuity generally decreases as the coating thickness or lift-off, or both, increases. For eddy current sensor arrays having a linear drive conductor and a linear array of sense elements, the spacing between the drive conductor and the array of sense elements should be smaller than or comparable to the thickness of the insulating coating. For other array formats the depth of sensitivity should be verified empirically.5.5 Models for the sensor response may be used to convert responses measured from the sensor array into physical property values, such as lift-off, electrical conductivity, magnetic permeability, coating thickness, or substrate thickness, or a combination thereof. For determining two property values, one operational frequency can be used. For nonmagnetic materials and examination for crack-like discontinuities, the lift-off and electrical conductivity should be determined. For magnetic materials, when the electrical conductivity can be measured or assumed constant, then the lift-off and magnetic permeability should be determined. The thickness can only be determined if a sufficiently low excitation frequency is used where the depth of sensitivity is greater than the material thickness of interest. For determining more than two property values, measurements at operating conditions having at least two depths of penetration should be used; these different depths of penetration can be achieved by using multiple operational frequencies or multiple spatial wavelengths.5.6 Processing of the measurement response or property value data may be performed to highlight the presence of discontinuities, to reduce background noise, and to characterize detected discontinuities. As an example, a correlation filter can be applied in which a reference signature response for a discontinuity is compared to the measured responses for each sensor array element to highlight discontinuity-like defects. Care must be taken to properly account for the effect of interferences such as edges and coatings on such signatures.5.7 The measurement and analysis methods described in this guide can also be applied to applications where the sensor array is mounted against a surface or embedded within the material being examined. In that situation the sensor array response is monitored over a period of time instead of the scanning the sensor array over a specific location. This leads to the horizontal axes for the B-scans and C-scans to correspond to time or some other input associated with the test such as the number of loading cycles.1.1 This guide covers the use of conformable eddy current sensor arrays for nondestructive examination of electrically conducting materials for discontinuities and material quality. The discontinuities include surface breaking and subsurface cracks and pitting as well as near-surface and hidden-surface material loss. The material quality includes coating or layer thickness, electrical conductivity, magnetic permeability, surface roughness, and other properties that vary with the electrical conductivity or magnetic permeability.1.2 This guide is intended for use on nonmagnetic and magnetic metals as well as composite materials with an electrically conducting component, such as reinforced carbon-carbon composite or polymer matrix composites with carbon fibers.1.3 This guide applies to planar as well as non-planar materials with and without insulating coating layers.1.4 Units—The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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5.1 The OTR is an important determinant of the packaging protection afforded by barrier materials. It is not, however, the sole determinant, and additional tests, based on experience, must be used to correlate packaging performance with OTR. It is suitable as a referee method of testing, provided that the purchaser and the seller have agreed on sampling procedures, standardization procedures, test conditions, and acceptance criteria.5.2 Limited statistical data on correlations with Test Method D1434 methods are available4; however, the oxygen transmission rate of a standard reference material (see 12.1) as determined manometrically by NIST, is in good agreement with the values obtained in the coulometric interlaboratory test using material from the same manufacturing lot. Thus, this test method may be used as a referee method.1.1 This test method covers a procedure for determination of the steady-state rate of transmission of oxygen gas through plastics in the form of film, sheeting, laminates, coextrusions, or plastic-coated papers or fabrics. It provides for the determination of (1) oxygen gas transmission rate (OTR), (2) the permeance of the film to oxygen gas (PO2), and (3) oxygen permeability coefficient (P′O2) in the case of homogeneous materials.1.2 This test method does not purport to be the only method for measurement of OTR. There may be other methods of OTR determination that use other oxygen sensors and procedures.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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5.1 Poor indoor air quality has been implicated in significant adverse acute and chronic impacts on occupant health and performance. The ability to assess the components contributing to poor indoor air quality is critical for determining best practices for improving indoor air quality.5.2 Measurement of pollutants in indoor environments using sensors and sensor systems provides information needed to improve indoor air quality through pollutant source control, ventilation, filtration or other treatments.5.3 This method uses a test characterization chamber system equipped with reference monitor(s) to evaluate the response of test sensors or test sensor systems to specific types of particles (for example, salt, polystyrene latex, or dust). To facilitate reproducible results, the test particles used within this method are standardized and have known properties. The user is cautioned that a single particle type is not representative of all particles found indoors. The relative response of test sensors or test sensor systems to a reference monitor can vary by a factor of two for different particle types (for example, primary or secondary, organic or inorganic, outdoor or indoor origin; see 6.11.3 for further discussion). Furthermore, the user is cautioned that the lower limit of particle size detection for optical test sensors and test sensor systems is generally 0.3 μm in diameter; particles below this size are generally undetected and may represent a significant health concern as well.1.1 This test method uses a chamber system to evaluate the performance of stationary PM2.5 sensors (sensors) and particle sensor systems (sensor systems) subjected to various test conditions, including temperature, relative humidity, PM2.5 concentration, and coarse PM interferent concentration.1.1.1 This test method covers sensors and sensor systems that can be continuously powered and continuously operated for the duration of any test described in this method through line power or an internal battery of sufficient output. This test method is not meant to evaluate sensors or sensor systems without these capabilities.1.1.2 This test method evaluates the performance of sensors and sensor systems that allow users to collect data in a systemic manner to assess the capabilities and limitations of these devices.1.1.3 This test method is not meant to evaluate sensors or sensor systems without data storage and recording capabilities.1.1.4 This test method is not intended to evaluate indoor air quality sensors and sensor systems for purposes of regulation of outdoor air, homeland security, law enforcement or forensic activity.1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.1.3 The text of this standard references notes and footnotes that provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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5.1 Knowledge of the water content of lubricating oils, additives, and similar products is important in the manufacture, purchase, sale, transfer, or use of such petroleum products to help in predicting their quality and performance characteristics.5.2 For lubricating oils, the presence of water can lead to premature corrosion and wear, an increase in the debris load resulting in diminished lubrication and premature plugging of filters, impedance to the effect of additives, and undesirable support of deleterious bacterial growth.1.1 This test method covers the quantitative determination of water in new and in-service lubricating oils and additives in the range of 10 mg/kg to 100 000 mg/kg (0.001 wt./wt. to 10 % wt./wt.) using a relative humidity (RH) sensor. Methanol, acetonitrile, and other compounds are known to interfere with this test method.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 Warning—Samples tested in this test method can be flammable, explosive, and toxic. Use caution when handling them before and after testing.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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