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5.1 Susceptibility to damage from concentrated out-of-plane forces is one of the major design concerns of many structures made of advanced composite laminates. Knowledge of the damage resistance properties of a laminated composite plate is useful for product development and material selection.5.2 QSI testing can serve the following purposes:5.2.1 To simulate the force-displacement relationships of impacts governed by boundary conditions (1-7).5 These are typically relatively large-mass low-velocity hard-body impacts on plates with a relatively small unsupported region. Since the test is run slowly in displacement control, the desired damage state can be obtained in a controlled manner. Associating specific damage events with a force during a drop-weight impact test is often difficult due to the oscillations in the force history. In addition, a specific sequence of damage events may be identified during quasi-static loading while the final damage state is only identifiable after a drop-weight impact test.5.2.2 To provide an estimate of the impact energy required to obtain a similar damage state for drop-weight impact testing if all others parameters are held constant.5.2.3 To establish quantitatively the effects of stacking sequence, fiber surface treatment, variations in fiber volume fraction, and processing and environmental variables on the damage resistance of a particular composite laminate to a concentrated indentation force.5.2.4 To compare quantitatively the relative values of the damage resistance parameters for composite materials with different constituents. The damage response parameters can include dent depth, damage dimensions and through-thickness locations, Fmax , Ea, and Emax, as well as the force versus indenter displacement curve.5.2.5 To impart damage in a specimen for subsequent damage tolerance tests, such as Test Method D7137/D7137M.5.2.6 To measure the indentation response of the specimen with and without bending using the two specimen configurations (edge supported and rigidly backed).5.3 The properties obtained using this test method can provide guidance in regard to the anticipated damage resistance capability of composite structures of similar material, thickness, stacking sequence, etc. However, it must be understood that the damage resistance of a composite structure is highly dependent upon several factors including geometry, thickness, stiffness, mass, support conditions, etc. Significant differences in the relationships between force/energy and the resultant damage state can result due to differences in these parameters. For example, properties obtained using the specimen supported over a circular hole would more likely reflect the damage resistance characteristics of an un-stiffened monolithic skin or web than that of a skin attached to sub-structure which resists out-of-plane deformation. Similarly, test specimen properties would be expected to be similar to those of a panel with equivalent length and width dimensions, in comparison to those of a panel significantly larger than the test specimen, which tends to divert a greater proportion of the energy into elastic deformation.5.4 The standard indenter geometry has a blunt, hemispherical tip. Historically, for the standard laminate configuration, this indenter geometry has generated a larger amount of internal damage for a given amount of external damage than is typically observed for similar indenters using sharp tips. Alternative indenter geometries may be appropriate depending upon the damage resistance characteristics being examined. For example, the use of sharp tip geometries may be appropriate for certain damage visibility and penetration resistance assessments.5.5 Some testing organizations may desire to use this test method in conjunction with Test Method D7137/D7137M to assess the compression residual strength of specimens containing a specific damage state, such as a defined dent depth, damage geometry, etc. In this case, the testing organization should subject several specimens to multiple energy or force levels using this test method. A relationship between energy or force and the desired damage parameter can then be developed. Subsequent QSI and compression residual strength tests can then be performed using specimens indented at an interpolated energy or force level that is expected to produce the desired damage state.1.1 This test method determines the damage resistance of multidirectional polymer matrix composite laminated plates subjected to a concentrated indentation force (Fig. 1). Procedures are specified for determining the damage resistance for a test specimen supported over a circular opening and for a rigidly-backed test specimen. The composite material forms are limited to continuous-fiber reinforced polymer matrix composites, with the range of acceptable test laminates and thicknesses defined in 8.2. This test method may prove useful for other types and classes of composite materials.FIG. 1 Quasi-Static Indentation Test1.1.1 Instructions for modifying these procedures to determine damage resistance properties of sandwich constructions are provided in Practice D7766/D7766M.1.2 A flat, square composite plate is subjected to an out-of-plane, concentrated force by slowly pressing a hemispherical indenter into the surface. The damage resistance is quantified in terms of a critical contact force to cause a specific size and type of damage in the specimen.1.3 The test method may be used to screen materials for damage resistance, or to inflict damage into a specimen for subsequent damage tolerance testing. The indented plate can be subsequently tested in accordance with Test Method D7137/D7137M to measure residual strength properties. Drop-weight impact per Test Method D7136/D7136M may be used as an alternate method of creating damage from an out-of-plane force and measuring damage resistance properties.1.4 The damage resistance properties generated by this test method are highly dependent upon several factors, which include specimen geometry, layup, indenter geometry, force, and boundary conditions. Thus, results are generally not scalable to other configurations, and are particular to the combination of geometric and physical conditions tested.1.5 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.1.5.1 Within the text the inch-pound units are shown in brackets.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The prepreg volatiles content, matrix content, reinforcement content, and filler content of composite prepreg materials are used to control material manufacture and subsequent fabrication processes, and are key parameters in the specification and production of such materials, as well as in the fabrication of products made with such materials.5.2 The extraction products resulting from this test method (the extract, the residue, or both) can be analyzed to assess chemical composition and degree of purity.1.1 This test method covers a Soxhlet extraction procedure to determine the matrix content, reinforcement content, and filler content of composite material prepreg. Volatiles content, if appropriate, and required, is determined by means of Test Method D3530.1.1.1 The reinforcement and filler must be substantially insoluble in the selected extraction reagent and any filler must be capable of being separated from the reinforcement by filtering the extraction residue.1.1.2 Reinforcement and filler content test results are total reinforcement content and total filler content; hybrid material systems with more than one type of either reinforcement or filler cannot be distinguished.1.2 This test method focuses on thermosetting matrix material systems for which the matrix may be extracted by an organic solvent. However, other, unspecified, reagents may be used with this test method to extract other matrix material types for the same purposes.1.3 Alternate techniques for determining matrix and reinforcement content include Test Methods D3171 (matrix digestion), D2584 (matrix burn-off/ignition), and D3529 (matrix dissolution and ignition loss). Test Method D2584 is preferred for reinforcement materials, such as glass, quartz, or silica, that are unaffected by high-temperature environments.1.4 The technical content of this standard has been stable since 1997 without significant objection from its stakeholders. As there is limited technical support for the maintenance of this standard, changes since that date have been limited to items required to retain consistency with other ASTM D30 Committee standards. The standard therefore should not be considered to include any significant changes in approach and practice since 1997. Future maintenance of the standard will only be in response to specific requests and performed only as technical support allows.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 9 and 7.2.3 and 8.2.1.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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1.1 This specification covers requirements and test methods for materials, dimensions, workmanship, and markings for on-site manufactured multilayer reinforced polyethylene composite pipe. It covers nominal sizes 6 in. through 36 in. (150 mm through 915 mm). These multilayered reinforced polyethylene composite pipe products2 are assembled and installed in various lengths, including long continuous lengths. These products are intended for the transport of crude oil, natural gas and hazardous liquids in the rehabilitation of existing pipelines and for new pipelines.NOTE 1: Hazardous liquids are those liquids defined by the U.S. Department of Transportation in 49 CFR 195.2.1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Refer to Guide D8509.1.1 This test method determines the fastener pull-through resistance of multidirectional polymer matrix composites reinforced by high-modulus fibers. Fastener pull-through resistance is characterized by the force-versus-displacement response exhibited when a mechanical fastener is pulled through a composite plate, with the force applied perpendicular to the plane of the plate. The composite material forms are limited to continuous-fiber or discontinuous-fiber (tape or fabric, or both) reinforced composites for which the laminate is symmetric and balanced with respect to the test direction. The range of acceptable test laminates and thicknesses is defined in 8.2.1.2 Two test procedures and configurations are provided. The first, Procedure A, is suitable for screening and fastener development purposes. The second, Procedure B, is configuration-dependent and is suitable for establishing design values. Both procedures can be used to perform comparative evaluations of candidate fasteners/fastener system designs.1.3 The specimens described herein may not be representative of actual joints which may contain one or more free edges adjacent to the fastener, or may contain multiple fasteners that can change the actual boundary conditions.1.4 This test method is consistent with the recommendations of CMH-17, which describes the desirable attributes of a fastener pull-through test method.1.5 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.1.5.1 Within the text, the inch-pound units are shown in brackets.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Refer to Guide D8509.1.1 This practice provides instructions for modifying static open-hole tensile and compressive strength test methods to determine the fatigue behavior of composite materials subjected to cyclic tensile or compressive forces, or both. The composite material forms are limited to continuous-fiber reinforced polymer matrix composites in which the laminate is both symmetric and balanced with respect to the test direction. The range of acceptable test laminates and thicknesses are described in 8.2.1.2 This practice supplements Test Methods D5766/D5766M and D6484/D6484M with provisions for testing specimens under cyclic loading. Several important test specimen parameters, for example fatigue force (stress) ratio, are not mandated by this practice; however, repeatable results require that these parameters be specified and reported.1.3 This practice is limited to test specimens subjected to constant amplitude uniaxial loading, where the machine is controlled so that the test specimen is subjected to repetitive constant amplitude force (stress) cycles. Either engineering stress or applied force may be used as a constant amplitude fatigue variable. The repetitive loadings may be tensile, compressive, or reversed, depending upon the test specimen and procedure utilized.1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.1.4.1 Within the text the inch-pound units are shown in brackets.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This AE examination is useful to detect micro-damage generation, accumulation, and growth of new or existing flaws. The examination is also used to detect significant existing damage from friction-based AE generated during loading or unloading of these regions. The damage mechanisms that can be detected include matrix cracking, fiber splitting, fiber breakage, fiber pull-out, debonding, and delamination. During loading, unloading, and load holding, damage that does not emit AE energy will not be detected.5.2 When the detected signals from AE sources are sufficiently spaced in time so as not to be classified as continuous AE, this practice is useful to locate the region(s) of the 2-D test sample where these sources originated and the accumulation of these sources with changing load or time, or both.5.3 The probability of detection of the potential AE sources depends on the nature of the damage mechanisms, flaw characteristics, and other aspects. For additional information, see X1.4.5.4 Concentrated damage in fiber/polymer composites can lead to premature failure of the composite item. Hence, the use of AE to detect and locate such damage is particularly important.5.5 AE-detected flaws or damage concentrated in a certain region may be further characterized by other NDE techniques (for example, visual, ultrasonic, etc.) and may be repaired as appropriate. Repair procedure recommendations and the subsequent examination of the repair are outside the scope of this practice. For additional information, see X1.5.5.6 This practice does not address sandwich core, foam core, or honeycomb core plate-like composites due to the fact that currently there is little in the way of published work on the subject resulting in a lack of a sufficient knowledge base.5.7 Refer to Guide E2533 for additional information about types of defects detected by AE, general overview of AE as applied to polymer matrix composites, discussion of the Felicity ratio (FR) and Kaiser effect, advantages and limitations, AE of composite parts other than flat panels, and safety hazards.1.1 This practice covers acoustic emission (AE) examination or monitoring of panel and plate-like composite structures made entirely of fiber/polymer composites.1.2 The AE examination detects emission sources and locates the region(s) within the composite structure where the emission originated. When properly developed AE-based criteria for the composite item are in place, the AE data can be used for nondestructive examination (NDE), characterization of proof testing, documentation of quality control, or for decisions relative to structural-test termination prior to completion of a planned test. Other NDE methods may be used to provide additional information about located damage regions. For additional information, see X1.1 in Appendix X1.1.3 This practice can be applied to aerospace composite panels and plate-like elements as a part of incoming inspection, during manufacturing, after assembly, continuously (during structural health monitoring), and at periodic intervals during the life of a structure.1.4 This practice is meant for fiber orientations that include cross-plies, angle-ply laminates, or two-dimensional woven fabrics. This practice also applies to 3-D reinforcement (for example, stitched, z-pinned) when the fiber content in the third direction is less than 5 % (based on the whole composite).1.5 This practice is directed toward composite materials that typically contain continuous high modulus greater than 20 GPa [3 Msi] fibers.1.6 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D4762-23 Standard Guide for Testing Polymer Matrix Composite Materials Active 发布日期 :  1970-01-01 实施日期 : 

4.1 This guide is intended to aid in the selection of standards for polymer matrix composite materials. It specifically summarizes the application of standards from ASTM Committee D30 on Composite Materials that apply to continuous-fiber reinforced polymer matrix composite materials. For reference and comparison, many commonly used or applicable ASTM standards from other ASTM Committees are also included.1.1 This guide summarizes the application of ASTM standard test methods (and other supporting standards) to continuous-fiber reinforced polymer matrix composite materials. The most commonly used or most applicable ASTM standards are included, emphasizing use of standards of Committee D30 on Composite Materials.1.2 This guide does not cover all possible standards that could apply to polymer matrix composites and restricts discussion to the documented scope. Commonly used but non-standard industry extensions of test method scopes, such as application of static test methods to fatigue testing, are not discussed. A more complete summary of general composite testing standards, including non-ASTM test methods, is included in the Composite Materials Handbook (CMH-17).2 Additional specific recommendations for testing textile (fabric, braided) composites are contained in Guide D6856.1.3 This guide does not specify a system of measurement; the systems specified within each of the referenced standards shall apply as appropriate. Note that the referenced standards of ASTM Committee D30 are either SI-only or combined-unit standards with SI units listed first.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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