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5.1 The volatile matter of petroleum coke affects the density of coke particles and can affect artifacts produced from further processing of the coke.5.2 The volatile matter can be used in estimating the calorific value of coke.1.1 This test method covers the determination of the volatile matter produced by pyrolysis or evolved when petroleum coke is subjected to the specific conditions of the test method.1.2 The interlaboratory study for precision covered materials with a volatile matter concentration ranging from about 8 % to 16 %.1.3 Samples having a thermal history above 600 °C are excluded.1.4 This test method is empirical and requires the entire test procedure to be closely followed to ensure that results from different laboratories will be comparable.1.5 This test method is not satisfactory for determining de-dusting material content.1.6 The values stated in SI units are to be regarded as standard.1.6.1 Exception—Non-SI units are shown in parentheses for information only.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user to establish appropriate safety, health, and environmental practices and to determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 The calculations of analytical data for the coal and coke test parameters listed in Section 6, assume the analysis sample has been prepared according to Practice D2013 and Test Method D3302.4.2 This practice provides formulas, to enable calculations of data from the as-determined analysis sample to various moisture bases, in common use by the coal and coke industry.4.3 This practice provides guidance to enable calculations of weight-average data from various lots or sublots, which, initially, are provided at different moisture bases.4.4 The principles given in this practice are applicable to the calculation of cumulative data (e.g., for trade purposes or for sieve analyses or washability analyses).1.1 This practice lists formulas that allow analytical data to be expressed in various bases in common use. Such bases are: as received, dry, equilibrium moisture, dry ash free, and others.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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