4.1 This practice may be used for material development, material comparison, quality assurance, characterization, reliability assessment, and design data generation.4.2 Continuous fiber-reinforced ceramic matrix composites are generally characterized by crystalline matrices and ceramic fiber reinforcements. These materials are candidate materials for structural applications requiring high degrees of wear and corrosion resistance, and high-temperature inherent damage tolerance (that is, toughness). In addition, continuous fiber-reinforced glass matrix composites are candidate materials for similar but possibly less demanding applications. Although flexural test methods are commonly used to evaluate the mechanical behavior of monolithic advanced ceramics, the nonuniform stress distribution in a flexural test specimen in addition to dissimilar mechanical behavior in tension and compression for CFCCs leads to ambiguity of interpretation of test results obtained in flexure for CFCCs. Uniaxially loaded tensile tests provide information on mechanical behavior for a uniformly stressed material.4.3 The cyclic fatigue behavior of CFCCs can have appreciable nonlinear effects (for example, sliding of fibers within the matrix) which may be related to the heat transfer of the specimen to the surroundings. Changes in test temperature, frequency, and heat removal can affect test results. It may be desirable to measure the effects of these variables to more closely simulate end-use conditions for some specific application.4.4 Cyclic fatigue by its nature is a probabilistic phenomenon as discussed in STP 91A (1) and STP 588 (2).4 In addition, the strengths of the brittle matrices and fibers of CFCCs are probabilistic in nature. Therefore, a sufficient number of test specimens at each testing condition is required for statistical analysis and design, with guidelines for sufficient numbers provided in STP 91A (1), STP 588 (2), and Practice E739. Studies to determine the influence of test specimen volume or surface area on cyclic fatigue strength distributions for CFCCs have not been completed. The many different tensile test specimen geometries available for cyclic fatigue testing may result in variations in the measured cyclic fatigue behavior of a particular material due to differences in the volume of material in the gage section of the test specimens.4.5 Tensile cyclic fatigue tests provide information on the material response under fluctuating uniaxial tensile stresses. Uniform stress states are required to effectively evaluate any nonlinear stress-strain behavior which may develop as the result of cumulative damage processes (for example, matrix microcracking, fiber/matrix debonding, delamination, cyclic fatigue crack growth, etc.)4.6 Cumulative damage due to cyclic fatigue may be influenced by testing mode, testing rate (related to frequency), differences between maximum and minimum force (R or Α), effects of processing or combinations of constituent materials, environmental influences (including test environment and pre-test conditioning), or combinations thereof. Some of these effects may be consequences of stress corrosion or subcritical (slow) crack growth which can be difficult to quantify. Other factors which may influence cyclic fatigue behavior are: matrix or fiber material, void or porosity content, methods of test specimen preparation or fabrication, volume percent of the reinforcement, orientation and stacking of the reinforcement, test specimen conditioning, test environment, force or strain limits during cycling, wave shapes (that is, sinusoidal, trapezoidal, etc.), and failure mode of the CFCC.4.7 The results of cyclic fatigue tests of test specimens fabricated to standardized dimensions from a particular material or selected portions of a part, or both, may not totally represent the cyclic fatigue behavior of the entire, full-size end product or its in-service behavior in different environments.4.8 However, for quality control purposes, results derived from standardized tensile test specimens may be considered indicative of the response of the material from which they were taken for given primary processing conditions and post-processing heat treatments.4.9 The cyclic fatigue behavior of a CFCC is dependent on its inherent resistance to fracture, the presence of flaws, or damage accumulation processes, or both. There can be significant damage in the CFCC test specimen without any visual evidence such as the occurrence of a macroscopic crack. This can result in a loss of stiffness and retained strength. Depending on the purpose for which the test is being conducted, rather than final fracture, a specific loss in stiffness or retained strength may constitute failure. In cases where fracture occurs, analysis of fracture surfaces and fractography, though beyond the scope of this practice, is recommended.1.1 This practice covers the determination of constant-amplitude, axial tension-tension cyclic fatigue behavior and performance of continuous fiber-reinforced advanced ceramic composites (CFCCs) at ambient temperatures. This practice builds on experience and existing standards in tensile testing CFCCs at ambient temperatures and addresses various suggested test specimen geometries, specimen fabrication methods, testing modes (force, displacement, or strain control), testing rates and frequencies, allowable bending, and procedures for data collection and reporting. This practice does not apply to axial cyclic fatigue tests of components or parts (that is, machine elements with nonuniform or multiaxial stress states).1.2 This practice applies primarily to advanced ceramic matrix composites with continuous fiber reinforcement: uni-directional (1-D), bi-directional (2-D), and tri-directional (3-D) or other multi-directional reinforcements. In addition, this practice may also be used with glass (amorphous) matrix composites with 1-D, 2-D, 3-D, and other multi-directional continuous fiber reinforcements. This practice does not directly address discontinuous fiber-reinforced, whisker-reinforced or particulate-reinforced ceramics, although the methods detailed here may be equally applicable to these composites.1.3 The values stated in SI units are to be regarded as the standard and are in accordance with IEEE/ASTM SI 10.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Refer to Section 7 for specific precautions.

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4.1 This practice may be used for material development, material comparison, quality assurance, characterization, reliability assessment, and design data generation.4.2 High-strength, monolithic advanced ceramic materials are generally characterized by small grain sizes (<50 μm) and bulk densities near the theoretical density. These materials are candidates for load-bearing structural applications requiring high degrees of wear and corrosion resistance, and high-temperature strength. Although flexural test methods are commonly used to evaluate strength of advanced ceramics, the nonuniform stress distribution in a flexure specimen limits the volume of material subjected to the maximum applied stress at fracture. Uniaxially loaded tensile strength tests may provide information on strength-limiting flaws from a greater volume of uniformly stressed material.4.3 Cyclic fatigue by its nature is a probabilistic phenomenon as discussed in STP 91A and STP 588 (1, 2).4 In addition, the strengths of advanced ceramics are probabilistic in nature. Therefore, a sufficient number of test specimens at each testing condition is required for statistical analysis and design, with guidelines for sufficient numbers provided in STP 91A (1), STP 588 (2), and Practice E739. The many different tensile specimen geometries available for cyclic fatigue testing may result in variations in the measured cyclic fatigue behavior of a particular material due to differences in the volume or surface area of material in the gage section of the test specimens.4.4 Tensile cyclic fatigue tests provide information on the material response under fluctuating uniaxial tensile stresses. Uniform stress states are required to effectively evaluate any nonlinear stress-strain behavior which may develop as the result of cumulative damage processes (for example, microcracking, cyclic fatigue crack growth, etc.).4.5 Cumulative damage processes due to cyclic fatigue may be influenced by testing mode, testing rate (related to frequency), differences between maximum and minimum force (R or Α), effects of processing or combinations of constituent materials, or environmental influences, or both. Other factors that influence cyclic fatigue behavior are: void or porosity content, methods of test specimen preparation or fabrication,test specimen conditioning, test environment, force or strain limits during cycling, wave shapes (that is, sinusoidal, trapezoidal, etc.), and failure mode. Some of these effects may be consequences of stress corrosion or sub-critical (slow) crack growth which can be difficult to quantify. In addition, surface or near-surface flaws introduced by the test specimen fabrication process (machining) may or may not be quantifiable by conventional measurements of surface texture. Therefore, surface effects (for example, as reflected in cyclic fatigue reduction factors as classified by Marin (3)) must be inferred from the results of numerous cyclic fatigue tests performed with test specimens having identical fabrication histories.4.6 The results of cyclic fatigue tests of specimens fabricated to standardized dimensions from a particular material or selected portions of a part, or both, may not totally represent the cyclic fatigue behavior of the entire full-size end product or its in-service behavior in different environments.4.7 However, for quality control purposes, results derived from standardized tensile test specimens may be considered indicative of the response of the material from which they were taken for given primary processing conditions and post-processing heat treatments.4.8 The cyclic fatigue behavior of an advanced ceramic is dependent on its inherent resistance to fracture, the presence of flaws, or damage accumulation processes, or both. There can be significant damage in the test specimen without any visual evidence such as the occurrence of a macroscopic crack. This can result in a specific loss of stiffness and retained strength. Depending on the purpose for which the test is being conducted, rather than final fracture, a specific loss in stiffness or retained strength may constitute failure. In cases where fracture occurs, analysis of fracture surfaces and fractography, though beyond the scope of this practice, are recommended.1.1 This practice covers the determination of constant-amplitude, axial, tension-tension cyclic fatigue behavior and performance of advanced ceramics at ambient temperatures to establish “baseline” cyclic fatigue performance. This practice builds on experience and existing standards in tensile testing advanced ceramics at ambient temperatures and addresses various suggested test specimen geometries, test specimen fabrication methods, testing modes (force, displacement, or strain control), testing rates and frequencies, allowable bending, and procedures for data collection and reporting. This practice does not apply to axial cyclic fatigue tests of components or parts (that is, machine elements with nonuniform or multiaxial stress states).1.2 This practice applies primarily to advanced ceramics that macroscopically exhibit isotropic, homogeneous, continuous behavior. While this practice applies primarily to monolithic advanced ceramics, certain whisker- or particle-reinforced composite ceramics, as well as certain discontinuous fibre-reinforced composite ceramics, may also meet these macroscopic behavior assumptions. Generally, continuous fibre-reinforced ceramic composites (CFCCs) do not macroscopically exhibit isotropic, homogeneous, continuous behavior and application of this practice to these materials is not recommended.1.3 The values stated in SI units are to be regarded as the standard and are in accordance with IEEE/ASTM SI 10.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Refer to Section 7 for specific precautions.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 The axial force fatigue test is used to determine the effect of variations in material, geometry, surface condition, stress, and so forth, on the fatigue resistance of metallic materials subjected to direct stress for relatively large numbers of cycles. The results may also be used as a guide for the selection of metallic materials for service under conditions of repeated direct stress.4.2 In order to verify that such basic fatigue data generated using this practice is comparable, reproducible, and correlated among laboratories, it may be advantageous to conduct a round-robin-type test program from a statistician's point of view. To do so would require the control or balance of what are often deemed nuisance variables; for example, hardness, cleanliness, grain size, composition, directionality, surface residual stress, surface finish, and so forth. Thus, when embarking on a program of this nature it is essential to define and maintain consistency a priori, as many variables as reasonably possible, with as much economy as prudent. All material variables, testing information, and procedures used should be reported so that correlation and reproducibility of results may be attempted in a fashion that is considered reasonably good current test practice.4.3 The results of the axial force fatigue test are suitable for application to design only when the specimen test conditions realistically simulate service conditions or some methodology of accounting for service conditions is available and clearly defined.1.1 This practice covers the procedure for the performance of axial force controlled fatigue tests to obtain the fatigue strength of metallic materials in the fatigue regime where the strains are predominately elastic, both upon initial loading and throughout the test. This practice is limited to the fatigue testing of axial unnotched and notched specimens subjected to a constant amplitude, periodic forcing function in air at room temperature.1.2 The use of this test method is limited to specimens and does not cover testing of full-scale components, structures, or consumer products.1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.4 The text of this standard references notes and footnotes that provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.NOTE 1: The following documents, although not directly referenced in the text, are considered important enough to be listed in this practice:E739 Practice for Statistical Analysis of Linear or Linearized Stress-Life (S-N) and Strain-Life (ε-N) Fatigue DataSTP 566 Handbook of Fatigue Testing2STP 588 Manual on Statistical Planning and Analysis for Fatigue Experiments3STP 731 Tables for Estimating Median Fatigue Limits41.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 It is well understood how to measure the forces applied to a specimen under static conditions. Practices E4 details the required process for verifying the static force measurement capabilities of testing machines. During dynamic operation however, additional errors may manifest themselves in a testing machine. Further verification is necessary to confirm the dynamic force measurement capabilities of testing machines.NOTE 1: The static machine verification accomplished by Practices E4 simply establishes the reference. Indicated forces measured from the force cell are compared with the dynamometer conditioned forces statically for confirmation and then dynamically for dynamic verification of the fatigue testing system's force output.NOTE 2: The dynamic accuracy of the force cell's output will not always meet the accuracy requirement of this standard without correction. Dynamic correction to the force cell output can be applied provided that verification is performed after the correction has been applied.NOTE 3: Overall test accuracy is a combination of measurement accuracy and control accuracy. This practice provides methods to evaluate either or both. As control accuracy is dependent on many more variables than measurement accuracy it is imperative that the test operator utilize appropriate measurement tools to confirm that the testing machine’s control behavior is consistent between verification activities and actual testing activities.4.2 Dynamic errors are primarily span dependent, not level dependent. That is, the error for a particular force endlevel during dynamic operation is dependent on the immediately preceding force endlevel. Larger spans imply larger absolute errors for the same force endlevel.4.3 Due to the many test machine factors that influence dynamic force accuracy, verification is recommended for every new combination of potential error producing factors. Primary factors are specimen design, machine configuration, test frequency, and loading span. Clearly, performing a full verification for each configuration is often impractical. To address this problem, dynamic verification is taken in two parts.4.3.1 First, one or more full verifications are performed at least annually. The main body of this practice describes that procedure. This provides the most accurate estimate of dynamic errors, as it will account for electronic as well as acceleration-induced sources of error.4.3.2 The second part, described in Annex A1, is a simplified verification procedure. It provides a simplified method of estimating acceleration-induced errors only. This procedure is to be used for common configuration changes (that is, specimen/grip/crosshead height changes).4.4 Dynamic verification of the fatigue system is recommended over the entire range of force and frequency over which the planned fatigue test series is to be performed. Endlevels are limited to the machine's verified static force as defined by the current static force verification when tested in accordance with Practices E4.NOTE 4: There is uncertainty as to whether or not the vibration in a frame will be different when operating in compression as opposed to tension. As a consequence, this practice recommends performing verifications at maximum tension and maximum compression endlevels. The total span does not need to be between those two levels, but can be performed as two tests.NOTE 5: Primary electronic characteristics affecting dynamic measurement accuracy are noise and bandwidth. Excessive noise is generally the dominant effect at the minimum test frequency. Insufficient bandwidth-induced errors are generally most significant at the maximum test frequency.1.1 This practice covers procedures for the dynamic verification of cyclic force amplitude control or measurement accuracy during constant amplitude testing in an axial fatigue testing system. It is based on the premise that force verification can be done with the use of a strain gaged elastic element. Use of this practice gives assurance that the accuracies of forces applied by the machine or dynamic force readings from the test machine, at the time of the test, after any user applied correction factors, fall within the limits recommended in Section 9. It does not address static accuracy which must first be addressed using Practices E4 or equivalent.1.2 Verification is specific to a particular test machine configuration and specimen. This standard is recommended to be used for each configuration of testing machine and specimen. Where dynamic correction factors are to be applied to test machine force readings in order to meet the accuracy recommended in Section 9, the verification is also specific to the correction process used. Finally, if the correction process is triggered or performed by a person, or both, then the verification is specific to that individual as well.1.3 It is recognized that performance of a full verification for each configuration of testing machine and specimen configuration could be prohibitively time consuming and/or expensive. Annex A1 provides methods for estimating the dynamic accuracy impact of test machine and specimen configuration changes that may occur between full verifications. Where test machine dynamic accuracy is influenced by a person, estimating the dynamic accuracy impact of all individuals involved in the correction process is recommended. This practice does not specify how that assessment will be done due to the strong dependence on owner/operators of the test machine.1.4 This practice is intended to be used periodically. Consistent results between verifications is expected. Failure to obtain consistent results between verifications using the same machine configuration implies uncertain accuracy for dynamic tests performed during that time period.1.5 This practice addresses the accuracy of the testing machine's force control or indicated forces, or both, as compared to a dynamometer's indicated dynamic forces. Force control verification is only applicable for test systems that have some form of indicated force peak/valley monitoring or amplitude control. For the purposes of this verification, the dynamometer's indicated dynamic forces will be considered the true forces. Phase lag between dynamometer and force transducer indicated forces is not within the scope of this practice.1.6 The results of either the Annex A1 calculation or the full experimental verification must be reported per Section 10 of this standard.1.7 This practice provides no assurance that the shape of the actual waveform conforms to the intended waveform within any specified tolerance.1.8 This standard is principally focused at room temperature operation. It is believed there are additional issues that must be addressed when testing at high temperatures. At the present time, this standard practice must be viewed as only a partial solution for high temperature testing.1.9 The values stated in inch-pound units are to be regarded as standard. No other units of measurement are included in this standard.1.10 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.11 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Fatigue test results may be significantly influenced by the properties and history of the parent material, the operations performed during the preparation of the fatigue specimens, and the testing machine and test procedures used during the generation of the data. The presentation of fatigue test results should include citation of basic information on the material, specimens, and testing to increase the utility of the results and to reduce to a minimum the possibility of misinterpretation or improper application of those results.1.1 This practice covers the desirable and minimum information to be communicated between the originator and the user of data derived from constant-force amplitude axial, bending, or torsion fatigue tests of metallic materials tested in air and at room temperature.NOTE 1: Practice E466, although not directly referenced in the text, is considered important enough to be listed in this standard.1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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1.1 This test method covers procedures for the performance of constant amplitude fatigue testing of metallic staples used in internal fixation of the musculoskeletal system. This test method may be used when testing in air at ambient temperature or in an aqueous or physiological solution. 1.2 The values stated in SI units are to be regarded as the standard. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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5.1 This test method describes a uniaxial, constant amplitude, fully reversed fatigue test to characterize the fatigue performance of a uniform cylindrical waisted specimen manufactured from acrylic bone cement.5.2 This test method considers two approaches to evaluating the fatigue performance of bone cement:5.2.1 Testing is conducted at three stress levels to characterize the general fatigue behavior of a cement over a range of stresses. The stress level and resultant cycles to failure of the specimens can be plotted on an S-N diagram.5.2.2 Another approach is to determine the fatigue life of a particular cement. The fatigue life for orthopaedic bone cement is to be determined up to 5 million (5 × 106) cycles.5.3 This test method does not define or suggest required levels of performance of bone cement. This fatigue test method is not intended to represent the clinical use of orthopaedic bone cement, but rather to characterize the material using standard and well-established methods. The user is cautioned to consider the appropriateness of this test method in view of the material being tested and its potential application.5.4 It is widely reported that multiple clinical factors affect the fatigue performance of orthopaedic bone cement; however, the actual mechanisms involves multiple factors. Clinical factors which may affect the performance of bone cement include: temperature and humidity, mixing method, time of application, surgical technique, bone preparation, implant design, anatomical site, and patient factors, among others. This test method does not specifically address all of these clinical factors. The test method can be used to compare different acrylic bone cement formulations and products and different mixing methods and environments (that is, mixing temperature, vacuum, centrifugation, and so forth).1.1 This test method describes test procedures for evaluating the constant amplitude, uniaxial, tension-compression uniform fatigue performance of acrylic bone cement materials.1.2 This test method is relevant to orthopedic bone cements based on acrylic resins, as specified in Specification F451 and ISO 16402. The procedures in this test method may or may not apply to other surgical cement materials.1.3 It is not the intention of this test method to define levels of performance of these materials. It is not the intention of this test method to directly simulate the clinical use of these materials, but rather to allow for comparison between acrylic bone cements to evaluate fatigue behavior under specified conditions.1.4 A rationale is given in Appendix X2.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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1.1 This test method covers the determination of the effect of repetitions of the same magnitude of flexural stress on plastics by fixed-cantilever type testing machines, designed to produce a constant-amplitude-of-force on the test specimen each cycle. 1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only. 1.3 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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