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4.1 Upper limits for the formaldehyde emission rates have been established for wood panel building products made with urea-formaldehyde adhesives and permanently installed in homes or used as components in kitchen cabinets and similar industrial products. This test method is intended for use in conjunction with the test method referenced by HUD 24 for manufactured housing and by Minnesota Statutes for housing units and building materials. This method may also be used for monitoring products for compliance to the California Air Resources Board (CARB) regulation for composite wood products and the Environmental Protection Agency Formaldehyde Emission Standards for Composite Wood Products, EPA TSCA Title VI 40 CFR Section 770. This test method provides a means of testing smaller samples and reduces the time required for testing.4.2 Formaldehyde concentration levels obtained by this small-scale method may differ from expected in full-scale indoor environments. Variations in product loading, temperature, relative humidity, and air exchange will affect formaldehyde emission rates and thus likely indoor air formaldehyde concentrations.4.3 This test method requires the use of a chamber of 0.02 to 1 m3 in volume to evaluate the formaldehyde concentration in air using the following controlled conditions:4.3.1 Conditioning of specimens prior to testing,4.3.2 Exposed surface area of the specimens in the test chamber,4.3.3 Test chamber temperature and relative humidity,4.3.4 The Q/A ratio, and4.3.5 Air circulation within the chamber.1.1 This test method measures the formaldehyde concentrations in air emitted by wood product test specimens under defined test conditions of temperature and relative humidity. Results obtained from this small-scale chamber test method are intended to be comparable to results obtained from testing larger product samples by the large chamber test method for wood products, Test Method E1333. The results may be correlated to values obtained from Test Method E1333. The quantity of formaldehyde in an air sample from the small chamber is determined by a modification of NIOSH 3500 chromotropic acid test procedure. As with Test Method E1333, other analytical procedures may be used to determine the quantity of formaldehyde in the air sample provided that such methods give results comparable to those obtained by using the chromotropic acid procedure. However, the test results and test report must be properly qualified and the analytical procedure employed must be accurately described.1.2 The wood-based panel products to be tested by this test method are characteristically used for different applications and are tested at different relative amounts or loading ratios to reflect different applications. This is a test method that specifies testing at various loading ratios for different product types. However, the test results and test report must be properly qualified and must specify the make-up air flow, sample surface area, and chamber volume.1.3 Ideal candidates for small-scale chamber testing are products relatively homogeneous in their formaldehyde release characteristics. Still, product inhomogeneities must be considered when selecting and preparing samples for small-scale chamber testing.1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Uranium and plutonium oxides can be used as a nuclear-reactor fuel in the form of pellets. In order to be suitable for use as a nuclear fuel the starting material must meet certain specifications, such as found in Specifications C757, C833, C753, C776, C1008, or as specified by the purchaser. The uranium concentration, plutonium concentration, or both, and the isotopic abundances are measured by mass spectrometry following this test method.5.2 The separated heavy element fractions placed on mass spectrometric filaments must be very pure. The quantity required depends upon the sensitivity of the instrument detection system. If an electron multiplier detector is to be used, only a few nanograms are required. If a Faraday cup is used, a few micrograms are needed. Chemical purity of the sample becomes more important as the sample size decreases, because ion emission of the sample is suppressed by impurities.1.1 This test method covers the determination of the concentration and isotopic composition of uranium and plutonium in solutions. The purified uranium or plutonium from samples ranging from nuclear materials to environmental or bioassay matrices is loaded onto a mass spectrometric filament. The isotopic ratio is determined by thermal ionization mass spectrometry, the concentration is determined by isotope dilution.1.2 The values stated in SI units are to be regarded as the standard. Values in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Indoor CO2 concentrations have been described and used by some people as an indicator of indoor air quality. These uses have included both appropriate and inappropriate interpretations of indoor CO2 concentrations. Appropriate uses include estimating expected levels of occupant comfort in terms of human body odor, studying occupancy patterns, investigating the levels of contaminants that are related to occupant activity, and screening for the sufficiency of ventilation rates relative to occupancy. Inappropriate uses include the application of simple relationships to determine outdoor air ventilation rates per person from indoor CO2 concentrations without verifying the assumptions upon which these relationships are based, and the interpretation of indoor CO2 concentrations as a comprehensive indicator of indoor air quality.5.2 Outdoor air ventilation rates affect contaminant levels in buildings and building occupants' perception of the acceptability of the indoor environment. Minimum rates of outdoor air ventilation are specified in building codes and indoor air quality standards, for example, ASHRAE Standard 62. The compliance of outdoor air ventilation rates with relevant codes and standards are often assessed as part of indoor air quality investigations in buildings. The outdoor air ventilation rate of a building depends on the size and distribution of air leakage sites, pressure differences induced by wind and temperature, mechanical system operation, and occupant behavior. Given all of this information, ventilation rates are predictable; however, many of these parameters are difficult to determine in practice. Therefore, measurement is required to determine outdoor air change rates reliably.5.3 The measurement of CO2 concentrations has been promoted as a means of determining outdoor air ventilation rates per person. This approach, referred to in this guide as equilibrium analysis, is based on a steady-state, single-zone mass balance of CO2 in the building and is sometimes presented with little or no discussion of its limitations and the assumptions on which it is based. As a result, in some cases, the technique has been misused and indoor CO2 concentration measurements have been misinterpreted.5.4 When the assumptions upon which equilibrium analysis is based are valid, the technique can yield reliable measurements of outdoor air ventilation rates. In addition, indoor CO2 concentrations can be used to determine other aspects of building ventilation when used properly. By applying a mass balance at an air handler, the percent outdoor air intake in the supply airstream can be determined based on the CO2 concentrations in the supply, return, and outdoor air. This percentage can be multiplied by the supply airflow rate of the air handler to yield the outdoor air intake rate of the air handler. In addition, the decay of indoor CO2 concentrations can be monitored in a building after the occupants have left to determine the outdoor air change rate of the building.5.5 Continuous monitoring of indoor and outdoor CO2 concentrations can be used to study some aspects of ventilation system performance, the quality of outdoor air, and building occupancy patterns.1.1 This guide describes how measured values of indoor carbon dioxide (CO2) concentrations can be used in evaluations of indoor air quality and building ventilation.1.2 This guide describes the determination of CO2 generation rates from people as a function of body size and level of physical activity.1.3 This guide describes the experimentally-determined relationship between CO2 concentrations and the acceptability of a space in terms of human body odor.1.4 This guide describes the following uses of indoor CO2 concentrations to evaluate building ventilation–mass balance analysis to determine the percent outdoor air intake at an air handler, the tracer gas decay technique to estimate whole building air change rates, and the constant injection tracer gas technique at equilibrium to estimate whole building air change rates.1.5 This guide discusses the use of continuous monitoring of indoor and outdoor CO2 concentrations as a means of evaluating building ventilation and indoor air quality.1.6 This guide discusses some concentration measurement issues, but it does not include or recommend a method for measuring CO2 concentrations.1.7 This guide does not address the use of indoor CO2 to control outdoor air intake rates.1.8 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.9 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.10 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This guide describes stabilization criteria for recording field measurements of temperature, DO, SC, and pH.5.2 This guide describes the procedures used to calibrate and check meters to be used in the field to records these measurements and the procedures to be use in the field to obtain these data.5.3 This guide describes quality assurance procedures to be followed when obtaining cross-sectional means of temperature, DO, SC, and pH of water flowing in open channels.5.4 Field measurement must accurately represent the water flowing in the open channel being measured. Methods need to be used that will result in an accurate representation of the mean of the parameter of interest. Procedures must be used that will take into consideration the variation in the parameter across the sections and with depth.5.5 Temperature and DO must be measured directly in the water in the open channel. SC and pH are often measured in situ, but also may be measured in a subsample of a composite sample collected using discharge-weighted methods.1.1 This guide describes procedures to collect cross-sectional means of temperature, dissolved oxygen (DO), specific electrical conductance (SC), and pH of water flowing in open channels.1.2 This guide provides guidelines for preparation and calibration of the equipment to collect cross-sectional means of temperature, DO, SC, and pH of water flowing in open channels.1.3 This guide describes what equipment should be used to collect cross-sectional means of temperature, DO, SC, and pH of water flowing in open channels.1.4 This guide covers the cross-sectional means of temperature, DO, SC, and pH of fresh water flowing in open channels.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The results of this test method may be used to determine nitrogen oxides and carbon monoxide emission concentrations from natural gas combustion at stationary sources.5.2 This test method may also be used to monitor emissions during short-term emission tests or periodically in order to optimize process operation for nitrogen oxides and carbon monoxide control.1.1 This test method covers the determination of nitrogen oxides (NO and NO2), carbon monoxide (CO), and oxygen (O2) concentrations in controlled and uncontrolled emissions from natural gas-fired reciprocating engines, combustion turbines, boilers, and process heaters using portable analyzers with electrochemical sensors. Due to the inherent cross sensitivities of the electrochemical cells, this test method should not be applied to other pollutants or emission sources without a complete investigation of possible analytical interferences and a comparative evaluation with EPA test methods.1.1.1 The procedures and specifications of this test method were originally developed during laboratory and field tests funded by the Gas Research Institute (GRI).2 Comparative emission tests were conducted only on natural gas-fired combustion sources. Subsequently, the U.S. Environmental Protection Agency (EPA) sponsored Environmental Technology Verification (ETV) program conducted further evaluations of electrochemical cell analyzers, which included laboratory tests and field tests on natural gas and diesel-fueled generators. The EPA has reviewed the ETV test results, published additional information, and provided technical input that has been considered in the update of this test method.31.2 This test method contains notes that are explanatory and are not part of the mandatory requirements of the standard.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This technique is destructive, in that the glass fragments may need to be crushed, and digested in acid.4.2 Although the concentration ranges of the calibration curves shown in Appendix X1 are applicable to soda lime and borosilicate glass, this method is useful for the accurate measurement of element concentrations from a wide variety of glass samples.4.3 The determination of the element concentrations in glass yields data that can be used to compare fragments.4.4 It should be recognized that the method measures the bulk concentration of the target elements. Any extraneous material present on the glass that is not removed before digestion can result in inaccurate concentrations of the measured elements.4.5 The precision and accuracy of the method should be established in each laboratory that employs the method.1.1 One objective of a forensic glass examination is to compare glass samples to determine if they can be discriminated using their physical, optical or chemical properties (for example, color, refractive index (RI), density, elemental composition). If the samples are distinguishable in any of these observed and measured properties, it may be concluded that they did not originate from the same source of broken glass. If the samples are indistinguishable in all of these observed and measured properties, the possibility that they originated from the same source of glass cannot be eliminated. The use of an elemental analysis method such as inductively coupled plasma mass spectrometry yields high discrimination among sources of glass. (1-16)21.2 This test method covers a procedure for quantitative determination of the concentrations of magnesium (Mg), aluminum (Al), iron (Fe), titanium (Ti), manganese (Mn), rubidium (Rb), strontium (Sr), zirconium (Zr), barium (Ba), lanthanum (La), cerium (Ce), neodymium (Nd), samarium (Sm), and lead (Pb) in glass samples.1.3 This procedure is applicable to irregularly shaped samples as small as 200 micrograms, for the comparison of fragments of a known source to the recovered fragments from a questioned source. These elements are present in soda lime and borosilicate glass in μg/L to % levels.1.4 This procedure is applicable to other elements, other types of glass, and other concentration ranges with appropriate modifications of the digestion procedure (if needed for full recovery of the additional elements), calibration standards and the mass spectrometer conditions. Calcium and potassium, for example, could be added to the list of analytes in a modified analysis scheme. Alternative methods for the determination of concentrations of elements in glass are listed in the references.1.5 For any given glass, approximately 40 elements are likely to be present at detectable concentrations using this procedure with minor modifications. The element set stated here is an example of some of these elements that can be detected in glass and used for forensic comparisons.1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.7 This standard cannot replace knowledge, skills, or abilities acquired through education, training, and experience and is to be used in conjunction with professional judgment by individuals with such discipline-specific knowledge, skills, and abilities.1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 The permissible level of heavy metals in certain coatings is specified by governmental regulatory agencies. This test method provides a fully documented procedure for determining low concentrations of mercury present in both water and solvent-reducible coatings to determine compliance.1.1 This test method covers the determination of the content of mercury in the range between 10 and 1000 ppm (mg/kg) present in liquid coatings, coatings vehicles, or in dried films obtained from previously coated substrates. There is no reason to believe that higher levels could not be determined by this test method, provided that appropriate dilutions and adjustments in specimen size and reagent quantities are made.1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in Section 7 and 9.1.1.1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Intended Use: 4.1.1 This guide may be used by various parties involved in sediment corrective action programs, including regulatory agencies, project sponsors, environmental consultants, toxicologists, risk assessors, site remediation professionals, environmental contractors, and other stakeholders.4.2 Importance of the CSM: 4.2.1 The CSM should be continuously updated and refined to describe the physical properties, chemical composition and occurrence, biologic features, and environmental conditions of the sediment corrective action project (Guide E1689).4.3 Reference Material: 4.3.1 This guide should be used in conjunction with other ASTM guides listed in 2.1 (especially Guides E3344 and E3382); this guide should also be used in conjunction with the material in the References at the end of this guide (including 1). Utilizing these reference materials will direct the user in developing representative background concentrations for a sediment site.4.4 Flexible Site-Specific Implementation: 4.4.1 This guide provides a systematic, but flexible, framework to accommodate variations in approaches by regulatory agencies and by the user based on project objectives, site complexity, unique site features, regulatory requirements, newly developed guidance, newly published scientific research, changes in regulatory criteria, advances in scientific knowledge and technical capability, and unforeseen circumstances.4.5 Regulatory Frameworks: 4.5.1 This guide is intended to be applicable to a broad range of local, state, tribal, federal, or international jurisdictions, each with its own unique regulatory framework. As such, this guide does not provide a detailed discussion of the requirements or guidance associated with any of these regulatory frameworks, nor is it intended to supplant applicable regulations and guidance. The user of this guide will need to be aware of the regulatory requirements and guidance in the jurisdiction where the work is being performed.4.6 Systematic Project Planning and Scoping Process: 4.6.1 When applying this guide, the user should undertake a systematic project planning and scoping process to collect information to assist in making site-specific, user-defined decisions for a particular project, including assembling an experienced team of project professionals. These practitioners should have the appropriate expertise to scope, plan, and execute a sediment data acquisition and analysis program. This team may include, but is not limited to, project sponsors, environmental consultants, toxicologists, site remediation professionals, analytical chemists, geochemists, and statisticians.4.7 Use of Representative Background to Set a Boundary: 4.7.1 Representative background concentrations for sediments can be used to delineate a sediment corrective action, establishing the boundary of the sediment corrective action area by distinguishing site-related impacts from representative background concentrations. This application requires the development of a BTV for the representative background data set.4.8 Use of Representative Background to Establish Cleanup Levels: 4.8.1 Representative background concentrations for sediments can be used to establish cleanup levels for use in sediment corrective actions. In cases where risk-based sediment cleanup levels are below representative background concentrations, background concentrations are typically used as the cleanup level (4). This ensures that the cleanup levels are sustainable. Any recontamination from ongoing sources will eventually result in surface sediment concentrations greater than the risk-based cleanup level, but the surface sediment should still meet a cleanup level based on representative background concentrations, even following recontamination.4.9 Use of Representative Background in Risk Assessments: 4.9.1 Representative background concentrations can be used in the risk assessment process (including human and ecological risk assessments) to understand risks posed by background levels of contaminants to human health and the environment, and the incremental risks posed by site-related releases or activities (or both) that result in sediment concentrations that exceed representative background concentrations. Conversely, they can be used to estimate the risk reduction for various contaminants, if sediment is remediated from existing COC concentrations to lower values (that is, representative background concentrations).4.10 Use of Representative Background in Post-Remedy Monitoring Programs: 4.10.1 Post-remedy monitoring programs can also use representative background sediment concentrations either as a corrective action target or to understand how post-remedy concentrations compare to the sources not attributable to current or historical site releases or activities. Typically, source control actions taken to ensure that site-related releases are controlled and will not re-contaminate the post-corrective action sediments must be developed based on an understanding of ongoing contributions from representative background. Ongoing sources unrelated to current or historical site-related releases or activities (that may or may not be subject to source control actions) must be considered in this evaluation.4.11 Other Considerations: 4.11.1 This guide does not cover all components of a program to develop representative sediment background concentrations.4.11.2 The overarching process to develop representative background concentrations (including CSM considerations) is not covered in detail in this guide but is discussed in more depth in Guide E3382.4.11.3 The selection of a background reference area(s) for the sediment site is not covered in detail in this guide but is extensively described in Guide E3344.4.11.4 Sediment sampling and laboratory analyses are not covered in this guide. Guides E3163 and E3164 contain extensive information concerning sediment sampling and laboratory analyses.4.11.5 Data quality objectives are not covered in this guide. Data quality objectives are described in (5).4.11.6 Background study design considerations are not covered in this guide but are described in other references, including Guides E3163 and E3164, as well as (6, 7).4.11.7 Geospatial analysis considerations are not thoroughly discussed in this guidance but are discussed in more depth relative to environmental evaluations in (8), which focuses on quality assurance concerns relative to geospatial analyses.4.11.8 In this guide, only the concentrations of COCs are considered to be in scope. Residual background radioactivity is out of scope.4.12 Structure and Components of This Guide: 4.12.1 The user of this guide should review the overall structure and components of this guide before proceeding with use, including:Section 1 Section 2 Referenced DocumentsSection 3 TerminologySection 4 Section 5 Overview of Representative Background Concentration Development ProcessSection 6 Development of Candidate Background Data SetsSection 7 Evaluation of Candidate Background Data Sets to Obtain Representative Background Data SetsSection 8 Data VisualizationSection 9 Evaluation of High Nondetect Data PointsSection 10 Evaluation of Outlying Data PointsSection 11 Forensic Chemistry Evaluation of Organic ContaminantsSection 12 Geochemical Evaluation of MetalsSection 13 Methodology Application to Develop a Representative Background Data Set from a Candidate Background Data SetSection 14 Development of Representative Background ConcentrationsSection 15 Comparison of Sediment Site and Representative Background Data Sets Using Statistical Two-Sample TestingSection 16 KeywordsAppendix X1 Organic and Inorganic Chemistry OverviewAppendix X2 Illustrative Case Studies from One Example Sediment SiteAppendix X3 Summaries for Outlier Testing and Two-Sample Statistical TestingReferences  1.1 This guide describes data visualization, statistical, forensic chemistry and geochemical methodologies (including case studies) used in the evaluation of candidate background data sets; this evaluation leads to the development of representative background data sets for the sediment site. Statistical methodologies can then be applied to the representative background data sets to develop background threshold values (BTVs) that are measures of the upper limit of representative sediment background concentrations for the sediment site. In addition, representative background data sets and sediment site data sets can be compared using two-sample statistical tests to determine if there are statistically significant differences (at a specified confidence level) between the two data sets (such as, the median or mean values of the two data sets are significantly different).1.1.1 This guide is intended to inform, complement, and support, but not supersede the guidelines established by local, state, tribal, federal, or international agencies.1.2 Technically defensible representative sediment background concentrations are critical for several purposes (1).2 These include sediment site delineation, establishing remedial goals and cleanup levels, remedy selection, assessment of risks posed by representative background concentrations, and establishing appropriate post-remedial monitoring plans.1.3 The overarching framework for the development of representative sediment background concentrations at sediment sites is presented in Guide E3382. Guide E3240 provides a general discussion of how conceptual site model (CSM) development fits into the risk-based corrective action framework for contaminated sediment sites, while Guide E3382 provides a detailed discussion of the elements of a sediment site CSM that need to be considered when developing representative sediment background concentrations. Guide E3344 describes how to select an appropriate background reference area(s) from which to collect sediment samples for laboratory analysis. Guide E3164 describes the sampling methodologies to obtain sediment samples in the field (whether from the sediment site or background reference area[s]), while Guide E3163 discusses appropriate laboratory methodologies for the chemical analysis of potential contaminants of concern (PCOCs) in the sediment samples. Relevant content contained in Guides E3344 and E3382 is summarized herein, but the individual guides should be consulted for more detailed coverage of these topics.1.4 This guide focuses on the approach for the development of representative sediment background concentrations used for remedial actions performed under various regulatory programs, including the Comprehensive Environmental Response, Compensation, and Liability Act (CERCLA). Although many of the references cited in this guide are CERCLA oriented, the guide is applicable to remedial actions performed under local, state, tribal, federal, and international cleanup programs. However, the guide does not describe requirements for each jurisdiction. The requirements for the regulatory entity under which the cleanup is being performed should be reviewed to confirm compliance.1.5 This guide is designed to apply to contaminated sediment sites where sediment data have been collected and are readily available. Additionally, this guide assumes that risk assessments have been performed, so that the contaminants of concern (COCs) that exceed risk-based thresholds have been identified.1.5.1 Furthermore, this guide presumes that the identified risk-based thresholds are low enough to pose corrective action implementation challenges, or the site is subject to recontamination from uncontrolled ongoing anthropogenic or natural sources, or both. In all cases, representative sediment background concentrations will be useful for determining the extent of corrective remedial actions (when used as remedial goals or cleanup levels), evaluating risks posed by representative background concentrations, and establishing appropriate post-remedial monitoring plans.1.6 Units—The values stated in SI or CGS units are to be regarded as standard. No other units of measurement are included in this standard.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This procedure can be used to limit the need for screening tests prior to performing a test for estimating the LC50 of a non-reactive and non-electrolytic chemical to the fathead minnow. By eliminating the screening test, fewer fish need be tested. The time used for preparing and performing the screening test can also be saved. The value obtained in this procedure can be used as the preliminary estimate of the LC50 in a full-scale test.5.2 Estimates can be used to set testing priority of groups of non-reactive and non-electrolytic chemicals.5.3 If the estimated value is more than 0.3 times the experimental value, the mechanism of action is probably narcosis. If less, the effect concentration is considered to reflect a different mechanism of action.5.4 This practice estimates a maximum LC50, that is, non-reactive and non-electrolytic chemicals are at least as toxic as the practice predicts, but may have a lower LC50 if acting by a more specific mechanism. Data on a chemical indicating a lower toxicity than predicted should be considered suspect or an artifact because of limited solubility of the test material.1.1 This practice covers a procedure for estimating the fathead minnow (Pimephales promelas) 96-h LC50 of nonreactive (that is, covalently bonded without unsaturated residues) and nonelectrolytic (that is, require vigorous reagents to facilitate substitution, addition, replacement reactions and are non-ionic, non-dissociating in aqueous solutions) organic chemicals acting solely by narcosis, also referred to as Meyer-Overton toxicity relationship.21.2 This procedure is accurate for organic chemicals that are toxic due to narcosis and are non-reactive and non-electrolytic. Examples of appropriate chemicals are: alcohols, ketones, ethers, simple halogenated aliphatics, aromatics, and aliphatic substituted aromatics. It is not appropriate for chemicals whose structures include a potential toxiphore (that structural component of a chemical molecule that has been identified to show mammalian toxicity, for example CN is known to be reponsible for inactivation of enzymes, NO2 for decoupling of oxidative phosphorylation, both leading to mammalian toxicity). Examples of chemicals inappropriate for this practice are: carbamates, organophosphates, phenols, beta-gamma unsaturated alcohols, electrophiles, and quaternary ammonium salts.1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 The permissible level of heavy metals in certain coatings is specified by governmental regulatory agencies. This test method provides a fully documented procedure for determining low concentrations of lead, cadmium, and cobalt present in both water and solvent-reducible coatings to determine compliance.1.1 This test method covers the determination of lead2 contents between 0.01 and 5 %, cadmium contents between 50 and 150 ppm (mg/kg), and cobalt contents between 50 and 2000 ppm (mg/kg) present in the nonvolatile portion of liquid coatings or contained in dried films. There is no reason to believe that higher levels of all three elements could not be determined by this test method, provided that appropriate dilutions and adjustments in specimen size and reagent quantities are made.1.2 Only pigmented coatings were used for evaluating this test method, but there is no reason to believe that varnishes and lacquers could not be analyzed successfully, provided that appropriate precautions are taken.1.3 This test method is not applicable to the determination of lead in samples containing antimony pigments (low recoveries are obtained).1.4 If lead is present in the sample to be analyzed in the form of an organic lead compound at a concentration greater than 0.1 %, small losses of lead may occur, resulting in slightly poorer precision than shown in Section 12.1.5 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in Section 7.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The determination of endotoxin concentrations in MWF is a parameter that can be used in decision-making for prudent fluid management practices (fluid draining, cleaning, recharging, or biocide dosages).5.2 This standard provides a practice for analysts who perform quantitative endotoxin analyses of water-miscible MWF.1.1 This practice covers quantitative methods for the sampling and determination of bacterial endotoxin concentrations in water-miscible metalworking fluids (MWF).1.2 Users of this practice need to be familiar with the handling of MWF.1.3 This practice gives an estimate of the endotoxin concentration in the sampled MWF.1.4 This practice replaces Method E2250.1.5 This practice seeks to minimize interlaboratory variation of endotoxin data but does not ensure uniformity of results.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The measurement of particulate matter and collected residue emission rates is an important test method widely used in the practice of air pollution control. Particulate matter measurements after control devices are necessary to determine total emission rates into the atmosphere.5.1.1 These measurements, when approved by national, state, provincial, or other regional agencies, are often required for the purpose of determining compliance with regulations and statutes.5.1.2 The measurements made before and after control devices are often necessary to demonstrate conformance with regulatory or contractual performance specifications.5.2 The collected residue obtained with this test method is also important in characterizing stack emissions. However, the utility of these data is limited unless a chemical analysis of the collected residue is performed.5.3 These measurements also can be used to calibrate continuous particulate emission monitoring systems by correlating the output of the monitoring instruments with the data obtained by using this test method.1.1 This test method2 covers a method for the measurement of particulate matter (dust) concentration in emission gases in the concentrations below 20 mg/m3 standard conditions, with special emphasis around 5 mg/m3.1.2 To meet the requirements of this test method, the particulate sample is weighed to a specified level of accuracy. At low dust concentrations, this is achieved by:1.2.1 Precise and repeatable weighing procedures,1.2.2 Using low tare weight weighing dishes,1.2.3 Extending the sampling time at conventional sampling rates, or1.2.4 Sampling at higher rates at conventional sampling times (high-volume sampling).1.3 This test method differs from Test Method D3685/D3685M by requiring the mass measurement of filter blanks, specifying weighing procedures, and requiring monitoring of the flue gas flow variability over the testing period. It requires that the particulate matter collected on the sample filter have a mass at least five times a positive mass difference on the filter blank. High volume sampling techniques or an extension of the sampling time may be employed to satisfy this requirement. This test method has tightened requirements on sampling temperature fluctuations and isokinetic sampling deviation. This test method has eliminated the in-stack filtration technique.1.4 This test method may be used for calibration of automated monitoring systems (AMS). If the emission gas contains unstable, reactive, or semi-volatile substances, the measurement will depend on the filtration temperature.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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1.1 This test method is applicable to the determination of uranium (U) and plutonium (Pu) concentrations and their isotopic abundances (Note 1) in solutions which result from the dissolution of nuclear reactor fuels either before or after irradiation. A minimum sample size of 50 [mu]g of irradiated U will contain sufficient Pu for measurement and will minimize the effects of cross contamination by environment U. Note 1—The isotopic abundance of Pu can be determined by this test method; however, interference from U may be encountered. This interference may be due to (1) inadequate chemical separation of uranium and plutonium, (2) uranium contamination within the mass spectrometer, and (3) uranium contamination in the filament. One indication of uranium contamination is a changing 238/239 ratio during the mass spectrometer run, in which case, a meaningful Pu analysis cannot be obtained on that run. If inadequate separation is the problem, a second pass through the separation may remove the uranium. If contamination in the mass spectrometer or on the filaments is the problem, use of a larger sample, for example, 1 μg, on the filament may ease the problem. A recommended alternative method of determining Pu isotopic abundance without U interference is alpha spectroscopy using Practice D3084. The Pu abundance should be obtained by determining the ratio of alpha particle activity of Pu to the sum of the activities of Pu and Pu. (1) The contribution of Pu and Pu to the alpha activity differs from their isotopic abundances due to different specific activities. 1.2 The procedure is applicable to dissolver solutions of uranium fuels containing plutonium, aluminum, stainless steel, or zirconium. Interference from other alloying constituents has not been investigated and no provision has been made in the test method for fuels used in the Th U fuel cycle. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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