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5.1 Capillary ion electrophoresis provides a simultaneous separation and determination of several inorganic anions using nanolitres of sample in a single injection. All anions present in the sample matrix will be visualized yielding an anionic profile of the sample.5.2 Analysis time is less than 5 minutes with sufficient sensitivity for drinking water and wastewater applications. Time between samplings is less than seven minutes allowing for high sample throughput.5.3 Minimal sample preparation is necessary for drinking water and wastewater matrices. Typically, only a dilution with water is needed.5.4 This test method is intended as an alternative to other multi-analyte methods and various wet chemistries for the determination of inorganic anions in water and wastewater. Compared to other multi-analyte methods the major benefits of CIE are speed of analysis, simplicity, and reduced reagent consumption and operating costs.1.1 This test method covers the determination of the inorganic anions fluoride, bromide, chloride, nitrite, nitrate, ortho-phosphate, and sulfate in drinking water, wastewater, and other aqueous matrices using capillary ion electrophoresis (CIE) with indirect UV detection. See Figs. 1-6.1.2 The test method uses a chromate-based electrolyte and indirect UV detection at 254 nm. It is applicable for the determination or inorganic anions in the range of 0.1 to 50 mg/L except for fluoride whose range is 0.1 to 25 mg/L.1.3 It is the responsibility of the user to ensure the validity of this test method for other anion concentrations and untested aqueous matrices.NOTE 1: The highest accepted anion concentration submitted for precision and bias extend the anion concentration range for the following anions: Chloride to 93 mg/L, Sulfate to 90 mg/L, Nitrate to 72 mg/L, and ortho-phosphate to 58 mg/L.1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 9.

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5.1 The ER of a battery separator is a standard measurement used by separator and battery manufacturers for quality control purposes and separator selection.5.2 Separator ER and the separator's interaction with the electrolyte, that is resistance to wetting or flow, will contribute to the internal resistance of the battery and this has the potential to limit the electrical output of a battery. The ER determination is a tool for battery manufacturers to use in design, material selection, and performance specifications.5.3 The change in the bath electrical resistance imparted by a separator is affected by the porosity, thickness, and tortuousity of the pore structure of the separator, the wettability of the separator to the electrolyte, and the temperature and concentration of the electrolyte.5.4 Incomplete wetting or saturation of the pore structure limits the lowest ER value obtainable from a separator structure. Separators are pretreated to assure that the specimen being tested has been adequately wetted out. A separator that is not fully wetted out (saturated) will give a higher ER.5.5 This test method is intended to give a rapid and repeatable measurement that approximates the change in ER that could happen when the separator is used in a battery.1.1 This test method covers the pretreatment, test conditions, apparatus, and procedure to determine the ionic resistivity, commonly referred to in the battery industry as electrical resistance (ER) of an alkaline battery separator immersed in an electrolyte of 40 % potassium hydroxide (KOH).1.2 The values stated in SI units are to be regarded as the standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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3.1 This practice can be used to extract carbides, borides, TCP and GCP phases, which can then be qualitatively or quantitatively analyzed by X-ray diffraction or microanalysis.23.2 Careful control of parameters is necessary for reproducible quantitative results. Within a given laboratory, such results can be obtained routinely; however, caution must be exercised when comparing quantitative results from different laboratories.33.3 Comparable qualitative results can be obtained routinely among different laboratories using this procedure.31.1 This practice covers a procedure for the isolation of carbides, borides, TCP (topologically close-packed), and GCP (geometrically close-packed) phases (Note 1) in nickel and nickel-iron base gamma prime strengthened alloys. Contamination of the extracted residue by coarse matrix (gamma) or gamma prime particles, or both, reflects the condition of the alloy rather than the techniques mentioned in this procedure.1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. (See 4.3.2.1 and 5.1.1.)NOTE 1: Ni3 Ti (eta phase) has been found to be soluble in the electrolyte for some alloys.FIG. 1 Schematic Diagram of Extraction Cell1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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