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5.1 This practice allows the collection of a representative sample of LPG that may contain trace volatile dissolved components such as methane, ethane, and nitrogen. Sampling by Practice D1265 can result in a small, but predictable, loss of these lighter components. Practice D1265 is suitable for collecting samples for routine specification testing, as the small loss of light components is not significant under Specification D1835 specification requirements. Practice D3700 is recommended whenever highly accurate determination of light components is required. For example, compositions determined on samples collected according to Practice D3700 may be used to establish the product value of NGL mixtures (see Appendix X1).1.1 This practice covers the equipment and procedures for obtaining a representative sample of liquefied petroleum gas (LPG), such as specified in ASTM Specification D1835, GPA 2140, and comparable international standards. It may also be used for other natural gas liquid (NGL) products that are normally single phase (for example, NGL mix, field butane, and so forth), defined in other industry specifications or contractual agreements, and for volatile (higher vapor pressure) crude oils.NOTE 1: Some floating piston cylinders have such tight piston seals that the vapor pressure of some high vapor pressure crude oils may not be sufficient to allow sampling without a handle to move the piston. An alternative sampling practice for UN Class 3 liquids (under 300 kPa at 52 °C) is Practice D8009, which utilizes a Manual Piston Cylinder (MPC) sampler.1.2 This practice is not intended for non-specification products that contain significant quantities of undissolved gases (N2, CO2), free water or other separated phases, such as raw or unprocessed gas/liquids mixtures and related materials. The same equipment can be used for these purposes, but additional precautions are generally needed to obtain representative samples of multi-phase products (see Appendix X1).1.3 This practice includes recommendations for the location of a sample point in a line or vessel. It is the responsibility of the user to ensure that the sampling point is located so as to obtain a representative sample.1.4 The values stated in SI units are to be regarded as standard.1.4.1 Exception—The values given in parentheses are for information only.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices, and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification covers piston or plunger operated volumetric apparatus (POVA), in particular, the requirements, operating conditions, and test methods. POVA covered by this specification are pipettes, dispensers (with and without valve), dilutors, and displacement burets (with and without valve). Single measurement, replicate delivery, durability, functional (such as tests for leakage, broken parts, existence of air bubbles, and contamination), volumetric, and gravimetric tests shall be performed and shall conform to the requirements specified.1.1 This specification covers requirements, operating conditions, and test procedures for piston or plunger operated volumetric apparatus (POVA), as well as requirements for pipette operator training and qualification.1.2 This specification is applicable to all types of POVA. The following precautionary caveat pertains only to the test procedure portion, Annex A1 and Annex A2, of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Hydraulically operated stationary piston samplers are used to gather soil samples for laboratory or field testing and analysis for geologic investigations, soil chemical composition studies, and water quality investigations. The sampler is sometimes used when attempts to recover unstable soils with thin-walled tubes, Practice D1587/D1587M, are unsuccessful. Examples of a few types of investigations in which hydraulic stationary piston samplers may be used include building site foundation studies containing soft sediments, highway and dam foundation investigations where softer soil formation need evaluation, wetland crossings utilizing floating structures, and hazardous waste site investigations. Hydraulically operated stationary piston samplers provide specimens necessary to determine the physical and chemical composition of soils and, in certain circumstances, contained pore fluids (see Guide D6169/D6169M).5.2 Hydraulically operated stationary piston samplers can provide relatively intact soil samples of soft or loose formation materials for testing to determine accurate information on the physical characteristics of that soil. Samples of soft formation materials can be tested to determine numerous soil characteristics such as; soil stratigraphy, particle size, water content, permeability, shear strength, compressibility, and so forth. The chemical composition of soft formation soils can also be determined from the sample if provisions are made to ensure that clean, decontaminated tools are used in the sample gathering procedure. Field-extruded samples can be field-screened or laboratory-analyzed to determine the chemical composition of soil and contained pore fluids. Using sealed or protected sampling tools, cased boreholes, and proper advancement techniques can help in the acquisition of good representative samples. A general knowledge of subsurface conditions at the site is beneficial.5.3 The use of this practice may not be the correct method for investigations of softer formations in all cases. As with all sampling methods, subsurface conditions affect the performance of the sample gathering equipment and methods used. For example, research indicates that clean sands may undergo volume changes in the sampling process, due to drainage.5 The hydraulically operated stationary piston sampler is generally not effective for cohesive formations with unconfined, undrained shear strength in excess of 2.0 tons per square foot, coarse sands, compact gravelly tills containing boulders and cobbles, compacted gravel, cemented soil, or solid rock. These formations may damage the sample or cause refusal to penetration. A small percentage of gravel or gravel cuttings in the base of the borehole can cause the tube to bend and deform, resulting in sample disturbance. Certain cohesive soils, depending on their water content, can create friction on the thin-walled tube which can exceed the hydraulic delivery force. Some rock formations can weather into soft or loose deposits where the hydraulically operated stationary piston sampler may be functional. The absence of groundwater can affect the performance of this sampling tool, and since this sampling method can introduce water to the borehole, it may not be suitable for sampling above the groundwater table when water is utilized as the activation fluid. As with all sampling and borehole advancement methods, precautions must be taken to prevent cross-contamination of aquifers through migration of contaminates up or down the borehole. Refer to Guide D6286/D6286M on selecting drilling methods for environmental site characterization for additional information about work at hazardous waste sites.NOTE 1: The quality of the result produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this practice are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.Practice D3740 was developed for agencies engaged in the laboratory testing and/or inspection of soil and rock. As such, it is not totally applicable to agencies performing this practice. However, user of this practice must recognize that the framework of Practice D3740 is appropriate for evaluating the quality of an agency performing this practice. Currently, there is no known qualifying national authority that inspects agencies that perform this practice.1.1 This practice covers a procedure for sampling of cohesive, organic, or fine-grained soils, or combination thereof, using a thin-walled metal tube that is inserted into the soil formation by means of a hydraulically operated piston. It is used to collect relatively intact soil samples suitable for laboratory tests to determine structural and chemical properties for geotechnical and environmental site characterizations.1.1.1 Guidance on preservation and transport of samples in accordance with Practice D4220/D4220M may apply. Samples for classification may be preserved using procedures similar to Class A. In most cases, a thin-walled tube sample can be considered as Class B, C, or D. Refer to Guide D6169/D6169M for use of the hydraulically operated stationary piston soil sampler for environmental site characterization. This sampling method is often used in conjunction with rotary drilling methods such as fluid rotary; Guide D5783; and hollow stem augers, Practice D6151/D6151M. Sampling data shall be reported in the field log in accordance with Guide D5434.1.2 The hydraulically operated stationary piston sampler is limited to soils and unconsolidated materials that can be penetrated with the available hydraulic pressure that can be applied without exceeding the structural strength of the thin-walled tube. This standard addresses typical hydraulic piston samplers used on land or shallow water in drill holes. The standard does not address specialized offshore samplers for deep marine applications that may or may not be hydraulically operated. This standard does not address operation of other types of mechanically advanced piston samplers. For information on other soil samplers, refer to Guide D6169/D6169M.1.3 Units—The values stated in either inch-pound units or SI units [presented in brackets] are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard. Reporting of results in units other than shall not be regarded as nonconformance with this standard.1.4 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026, unless superseded by this standard.1.5 This practice does not purport to address all the safety concerns, if any, associated with its use and may involve use of hazardous materials, equipment, and operations. It is the responsibility of the user of this practice to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Also, the user must comply with prevalent regulatory codes, such as OSHA (Occupational Health and Safety Administration) guidelines, while using this practice. For good safety practice, consult applicable OSHA regulations and other safety guides on drilling.21.6 This practice offers a set of instructions for performing one or more specific operations. This practice cannot replace education or experience and should be used in conjunction with professional judgement. Not all aspects of this practice may be applicable in all circumstances. This practice is not intended to represent or replace the standard of care by which the adequacy of a given professional service must be judged, nor should this document be applied without consideration of a project's many unique aspects. The word “Standard” in the title means only that the document has been approved through the ASTM consensus process. This practice does not purport to comprehensively address all of the methods and potential issues associated with sampling of soil. Users should seek qualified professionals for decisions as to the proper equipment and methods that would be most successful for their site exploration. Other methods may be available for drilling and sampling of soil, and qualified professionals should have flexibility to exercise judgment as to possible alternatives not covered in this practice. The practice is current at the time of issue, but new alternative methods may become available prior to revisions, therefore, users should consult with manufacturers or producers prior to specifying program requirements.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Many petroleum products, as well as non-petroleum materials, are used as lubricants for bearings, gears, compressor cylinders, hydraulic equipment, etc. Proper operation of this equipment depends upon the viscosity of these liquids.5.2 Oscillating piston viscometers allow viscosity measurement of a broad range of materials including transparent, translucent and opaque liquids. The measurement principle and stainless steel construction makes the Oscillating Piston Viscometer resistant to damage and suitable for portable operations. The measurement itself is automatic and does not require an operator to time the oscillation of the piston. The electromagnetically driven piston mixes the sample while under test. The instrument requires a sample volume of less than 5 mL and typical solvent volume of less than 10 mL which minimizes cleanup effort and waste.1.1 This test method covers the measurement of dynamic viscosity and derivation of kinematic viscosity of liquids, such as new and in-service lubricating oils, by means of an oscillating piston viscometer.1.2 This test method is applicable to Newtonian and non-Newtonian liquids; however the precision statement was developed using Newtonian liquids.1.3 The range of dynamic viscosity covered by this test method is from 0.2 mPa·s to 20 000 mPa·s (which is approximately the kinematic viscosity range of 0.2 mm2/s to 22 000 mm2/s for new oils) in the temperature range between –40 °C to 190 °C; however the precision has been determined only for new and used oils in the range of 34 mPa·s to 1150 mPa·s at 40 °C, 5.7 mPa·s to 131 mPa·s at 100 °C, and 46.5 mm2/s to 436 mm2/s at 40 °C.1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This practice allows the collection of a representative sample of crude oil and/or condensate that may contain trace volatile dissolved components such as methane, ethane, propane, and fixed gases that would normally be lost using conventional atmospheric sampling methods. These highly volatile components can result in vapor pressure conditions above atmospheric pressure. This practice is recommended whenever accurate determination of vapor pressure, flash point, or other properties are required and where loss of volatile components can affect the test results.5.2 This practice is intended for capturing samples of crude oil and/or condensate for testing for the purpose of classification for transportation of dangerous goods as UN Class 3 Flammable Liquids, but is not limited to classification testing. Other test methods with sensitivities to light end loss may also utilize this sampling practice.5.3 Practice D3700 using a floating piston cylinder is recommended whenever true vapor pressures greater than 300 kPa at 50 °C are anticipated.1.1 This practice includes the equipment and procedures for obtaining a representative sample of “live” or high vapor pressure crude oils, condensates, and/or liquid petroleum products from low pressure sample points, where there is insufficient sample point pressure to use a Floating Piston Cylinder (FPC) as described in Practice D3700.1.2 This practice is intended for use with sample types, such as UN Class 3 Flammable Liquids, that might have been collected and transported using open containers. The use of a manual piston cylinder in place of open containers is intended to prevent the loss of volatile (light end) components, which can impact subsequent test results.1.3 This practice is suitable for sampling crude oils, condensates, and/or liquid petroleum products having true vapor pressures less than 300 kPa (43 psia nominal) at 50 °C. This practice applies to samples that will typically fall between Practices D4057 (API MPMS Chapter 8.1) and D3700. This practice shall not be used for materials classified as UN Class 2 Gases2 (“…having a vapor pressure greater than 300 kPa at 50 °C or is completely gaseous at 20 °C at 101.3 kPa.”).1.4 This practice allows for sampling of crude oils that flow freely at the conditions of sampling.1.5 It is the responsibility of the user to ensure that the sampling point is located so as to obtain a representative sample.1.6 The values stated in SI units are to be regarded as standard.1.6.1 Exception—The values given in parentheses are for information only.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The efficiency and fuel economy of spark ignition and diesel engines is affected in part by the friction between moving parts. Although no reliable, in situ friction measurements exist for fired internal combustion engines, it has been estimated that at least half of the friction losses in such engines are due to those at the ring and liner interface. This test method involves the use of a reciprocating sliding arrangement to simulate the type of oscillating contact that occurs between a piston ring and its mating cylinder bore surface near the top-dead-center position in the cylinder where most severe surface contact conditions occur. There are many types of engines and engine operating environments; therefore, to allow the user the flexibility to tailor this test to conditions representative of various engines, this standard test method allows flexibility in selecting test loads, speeds, lubricants, and durations of testing. Variables that can be adjusted in this procedure include: normal force, speed of oscillation, stroke length, duration of testing, temperature of testing, method of specimen surface preparation, and the materials and lubricants to be evaluated. Guidance is provided here on the set-up of the test, the manner of specimen fixturing and alignment, the selection of a lubricant to simulate conditioned oil characteristics (for a diesel engine), and the means to run-in the ring specimens to minimize variability in test results.5.2 Engine oil spends the majority of its operating lifetime in a state that is representative of use-conditioned oil. That is, fresh oil is changed by exposure to the heat, chemical environment, and confinement in lubricated contact. It ages, changing viscosity, atomic weight, solids content, acidity, and chemistry. Conducting piston ring and cylinder liner material evaluations in fresh, non-conditioned oil is therefore unrealistic for material screening. But additive-depleted, used oil can result in high wear and corrosive attack of engine parts. The current test is intended for use with lubricants that simulate tribological behavior after in-service oil conditioning, but preceding the point of severe engine damage.1.1 This test method covers procedures for conducting laboratory bench-scale friction tests of materials, coatings, and surface treatments intended for use in piston rings and cylinder liners in diesel or spark-ignition engines. The goal of this procedure is to provide a means for preliminary, cost-effective screening or evaluation of candidate ring and liner materials. A reciprocating sliding arrangement is used to simulate the contact that occurs between a piston ring and its mating liner near the top-dead-center position in the cylinder where liquid lubrication is least effective, and most wear is known to occur. Special attention is paid to specimen alignment, running-in, and lubricant condition.1.2 This test method does not purport to simulate all aspects of a fired engine’s operating environment, but is intended to serve as a means for preliminary screening for assessing the frictional characteristics of candidate piston ring and liner material combinations in the presence of fluids that behave as use-conditioned engine oils. Therefore, it is beyond the scope of this test method to describe how one might establish correlations between the described test results and the frictional characteristics of rings and cylinder bore materials for specific engine designs or operating conditions.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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