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AS 2008-1997 Residual bitumen for pavements 被代替 发布日期 :  1997-02-05 实施日期 : 

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11.1 The indentation and the residual indentation of resilient floor covering is important since the resistance and recovery from indentation reflects on the ability of the resilient floor covering to perform properly after installation.11.2 The indentation of a resilient floor covering shall be measured using a specified type of indentor, flat or spherical, under a specified load and time.11.3 The residual indentation of a resilient floor covering shall be measured after a specified recovery time.11.4 See Table 1 for detailed testing and conditioning requirements by products (specification) type.1.1 This test method covers procedures to determine short-term indentation and residual indentation of resilient flooring, when subjected to concentrated loads.1.2 The test methods appear in the following order:   SectionIndentation by McBurney2 Test  4 to 10Indentation and Residual Indentation  11 to 151.3 There are two procedures with their respective apparatus. The first (McBurney Test) is described in Sections 4 to 10 and is restricted to a spherical foot. It is only used for initial indentation measurements of VCT. The second is described in Sections 11 to 15 and has interchangeable feet with variable geometry. It is used to measure initial and residual indentation.1.4 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The use of this test method can significantly reduce the risk of sudden catastrophic failure of threaded articles and fasteners, below their design strength, due to hydrogen embrittlement.1.1 This test method covers the determination of, on a statistical basis, the probability of the existence of hydrogen embrittlement or degradation in:1.1.1 A batch of barrel electroplated, autocatalytic plated, phosphated, or chemically processed threaded articles or fasteners and1.1.2 A batch of rack plated threaded articles, fasteners, or rod.1.2 Industrial practice for threaded articles, fasteners, and rod has evolved three graduated levels of test exposure to ensure reduced risk of hydrogen embrittlement (see Section 3). These levels have evolved from commercial applications having varying levels of criticality. In essence, they represent the confidence level that is required. They also represent the time that finished goods are held before they can be shipped and used. This time equates to additional cost to the manufacturer that may of necessity be added to the cost of the finished goods.1.3 This test method is applicable to threaded articles, fasteners, and rod made from steel with ≥1000 MPa (with corresponding hardness values of 300 HV10 kgf, 303 HB, or 31 HRc) or surface hardened threaded articles, fasteners, or rod.1.4 This test method shall be carried out after hydrogen embrittlement relief heat treatment in accordance with the requirements of Guide B850. It may also be used for assessing differences in processing solutions, conditions, and techniques. This test method has two main functions: first, when used with a statistical sampling plan it can be used for lot acceptance or rejection, and second, it can be used as a control test to determine the effectiveness of the various processing steps including pre- and post-baking treatments to reduce the mobile hydrogen in the articles, fasteners, or rod. While this test method is capable of indicating those items that are embrittled to the extent defined in Section 3, it does not guarantee complete freedom from embrittlement.1.5 This test method does not relieve the processor from imposing and monitoring suitable process control.1.6 This test method has been coordinated with ISO/DIS 10587 and is technically equivalent. (Warning—Great care should be taken when applying this test method. The heads of embrittled articles, fasteners, or rod may suddenly break off and become flying projectiles capable of causing blindness or other serious injury. This hazard can occur as long as 200 h after the test has started. Hence, shields or other apparatus should be provided to avoid such injury.)Note 1—Test Method F1940 can be used as a process control and verification to prevent hydrogen embrittlement in fasteners covered by this test method.Note 2—The use of inhibitors in acid pickling baths does not necessarily guarantee avoidance of hydrogen embrittlement.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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5.1 Residual fuel oils can contain H2S in the liquid phase and this can result in hazardous vapor phase levels of H2S in storage tank headspaces. The vapor phase levels can vary significantly according to the headspace volume, fuel temperature and agitation. Measurement of H2S levels in the liquid phase provides a useful indication of the residual fuel oil’s propensity to form high vapor phase levels, and lower levels in the residual fuel oil will directly reduce risk of H2S exposure. It is critical, however, that anyone involved in handling fuel oil, such as vessel owners and operators, continue to maintain appropriate safety practices designed to protect the crew, tank farm operators and others who can be exposed to H2S.5.1.1 The measurement of H2S in the liquid phase is appropriate for product quality control, while the measurement of H2S in the vapor phase is appropriate for health and safety purposes.5.2 This test method was developed to provide refineries, fuel terminals and independent testing laboratories, which do not have access to analytical instruments such as a gas chromatograph, with a simple and consistent field test method for the rapid determination of H2S in the vapor phase above residual fuel oils.NOTE 1: D5705 is one of three test methods for quantitatively measuring H2S in residual fuels:1) Test Method D6021 is an analytical test method to determine H2S levels in the liquid phase.2) Test Method D7621 is a rapid test method to determine H2S levels in the liquid phase.NOTE 2: Because of the reactivity, absorptivity and volatility of H2S, any measurement method only provides an H2S concentration at a given moment in time.5.3 This test method does not necessarily simulate the vapor phase H2S concentration in a fuel storage tank. It does, however, provide a level of consistency so that the test result is only a function of the residual fuel oil sample and not the test method, operator, or location. No general correlation can be established between this field test and actual vapor phase concentrations of H2S in residual fuel oil storage or transports. However, a facility that produces fuel oil from the same crude source under essentially constant conditions might be able to develop a correlation for its individual case.1.1 This test method covers the field determination of hydrogen sulfide (H2S) in the vapor phase (equilibrium headspace) of a residual fuel oil sample.1.2 The test method is applicable to liquids with a viscosity range of 5.5 mm2/s at 40 °C to 50 mm2/s at 100 °C. The test method is applicable to fuels conforming to Specification D396 Grade Nos. 4, 5 (Heavy), and 6.1.3 The applicable range is from 5 μmol/mol to 4000 μmol/mol (micromoles per mole) (5 ppm v/v to 4000 ppm v/v (parts per million by volume)).1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The observation and measurement of strains in transparent or translucent materials is extensively used in various modeling techniques of experimental stress analysis.5.2 Internal strains induced in manufacturing processes such as casting, molding, welding, extrusion, and polymer stretching can be assessed and parts exhibiting excessive strains identified. Such measurements can lead to elimination of defective parts, process improvement, control of annealing operation, etc.5.3 When testing for physical properties, polariscopic examination of specimens is required, to eliminate those specimens exhibiting abnormal internal strain level (or defects). For example: Test Methods D638 (Note 8) and D882 (Note 11) recommend a polariscopic examination.5.4 The birefringence of oriented polymers can be related to orientation, shrinkage, etc. The measurements of birefringence aid in characterization of these polymers.5.5 For many materials, there may be a specification that requires the use of this test method, but with some procedural modifications that take precedence when adhering to the specification. Therefore, it is advisable to refer to that material specification before using this test method. Table 1 of Classification System D4000 lists the ASTM materials standards that currently exist.1.1 This quantitative test method covers measurements of direction of principal strains, ε1 and ε2, and the photoelastic retardation, δ, using a compensator, for the purpose of analyzing strains in transparent or translucent plastic materials. This test method can be used to measure birefringence and to determine the difference of principal strains or normal strains when the principal directions do not change substantially within the light path.1.2 In addition to the method using a compensator described in this test method, other methods are in use, such as the goniometric method (using rotation of the analyzer) mostly applied for measuring small retardation, and expressing it as a fraction of a wavelength. Nonvisual methods employing spectrophotometric measurements and eliminating the human judgment factor are also possible.1.3 Test data obtained by this test method is relevant and appropriate for use in engineering design.1.4 The values stated in either SI units or inch-pound units are to be regarded as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.NOTE 1: There is no known ISO equivalent to this test method.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method covers a procedure for experimentally determining macroscopic residual stress tensor components of quasi-isotropic bearing steel materials by XRD. Here the stress components are represented by the tensor σij as shown in Eq 1 (1,5 p. 40). The stress strain relationship in any direction of a component is defined by Eq 2 with respect to the azimuth phi(φ) and polar angle psi(ψ) defined in Fig. 1 (1, p. 132). 5.1.1 Alternatively, Eq 2 may also be shown in the following arrangement (2, p. 126): 5.2 Using XRD and Bragg’s law, interplanar strain measurements are performed for multiple orientations. The orientations are selected based on a modified version of Eq 2, which is dictated by the mode used. Conflicting nomenclature may be found in literature with regard to mode names. For example, what may be referred to as a ψ (psi) diffractometer in Europe may be called a χ (chi) diffractometer in North America. The three modes considered here will be referred to as omega, chi, and modified-chi as described in 9.5. 5.3 Omega Mode (Iso Inclination) and Chi Mode (Side Inclination)—Interplanar strain measurements are performed at multiple ψ angles along one φ azimuth (let φ = 0°) (Figs. 2 and 3), reducing Eq 2 to Eq 3. Stress normal to the surface (σ33) is assumed to be insignificant because of the shallow depth of penetration of X-rays at the free surface, reducing Eq 3 to Eq 4. Post-measurement corrections may be applied to account for possible σ33 influences (12.12). Since the σij values will remain constant for a given azimuth, the s1{hkl} term is renamed C. FIG. 2 Omega Mode Diagram for Measurement in σ11 Direction FIG. 3 Chi Mode Diagram for Measurement in σ11 Direction Note 1: Stress matrix is rotated 90° about the surface normal compared to Fig. 2 and Fig. 14. 5.3.1 The measured interplanar spacing values are converted to strain using Eq 24, Eq 25, or Eq 26. Eq 4 is used to fit the strain versus sin2ψ data yielding the values σ11, τ13, and C. The measurement can then be repeated for multiple phi angles (for example 0, 45, and 90°) to determine the full stress/strain tensor. The value, σ11, will influence the overall slope of the data, while τ13 is related to the direction and degree of elliptical opening. Fig. 4 shows a simulated d versus sin2ψ profile for the tensor shown. Here the positive 20-MPa τ13 stress results in an elliptical opening in which the positive psi range opens upward and the negative psi range opens downward. A higher τ13 value will cause a larger elliptical opening. A negative 20-MPa τ13 stress would result in the same elliptical opening only the direction would be reversed with the positive psi range opening downwards and the negative psi range opening upwards as shown in Fig. 5. FIG. 4 Sample d (2θ) Versus sin2ψ Dataset with σ11 = -500 MPa and τ13 = +20 MPa FIG. 5 Sample d (2θ) Versus sin2ψ Dataset with σ11 = -500 MPa and τ13 = -20 MPa 5.4 Modified Chi Mode—Interplanar strain measurements are performed at multiple β angles with a fixed χ offset, χm (Fig. 6). Measurements at various β angles do not provide a constant φ angle (Fig. 7), therefore, Eq 2 cannot be simplified in the same manner as for omega and chi mode. FIG. 6 Modified Chi Mode Diagram for Measurement in σ11 Direction FIG. 7 ψ and φ Angles Versus β Angle for Modified Chi Mode with χm = 12° 5.4.1 Eq 2 shall be rewritten in terms of β and χm. Eq 5 and 6 are obtained from the solution for a right-angled spherical triangle (3). 5.4.2 Substituting φ and ψ in Eq 2 with Eq 5 and 6 (see X1.1), we get: 5.4.3 Stress normal to the surface (σ33) is assumed to be insignificant because of the shallow depth of penetration of X-rays at the free surface reducing Eq 7 to Eq 8. Post-measurement corrections may be applied to account for possible σ33 influences (see 12.12). Since the σij values and χm will remain constant for a given azimuth, the s1{hkl} term is renamed C, and the σ22 term is renamed D. 5.4.4 The σ11 influence on the d versus sin2β plot is similar to omega and chi mode (Fig. 8) with the exception that the slope shall be divided by cos2χm. This increases the effective 1/2 s2{hkl} by a factor of 1/cos2χm for σ11. FIG. 8 Sample d (2θ) Versus sin2β Dataset with σ11 = -500 MPa 5.4.5 The τij influences on the d versus sin2β plot are more complex and are often assumed to be zero (3). However, this may not be true and significant errors in the calculated stress may result. Figs. 9-13 show the d versus sin2β influences of individual shear components for modified chi mode considering two detector positions (χm = +12° and χm = -12°). Components τ12 and τ13 cause a symmetrical opening about the σ11 slope influence for either detector position (Figs. 9-11); therefore, σ11 can still be determined by simply averaging the positive and negative β data. Fitting the opening to the τ12 and τ13 terms may be possible, although distinguishing between the two influences through regression is not normally possible. FIG. 9 Sample d (2θ) versus sin2β Dataset with χm = +12°, σ11 = -500 MPa, and τ12 = -100 MPa FIG. 10 Sample d (2θ) Versus sin2β Dataset with χm = -12°, σ11 = -500 MPa, and τ12 = -100 MPa FIG. 11 Sample d (2θ) Versus sin2β Dataset with χm = +12 or -12°, σ11 = -500 MPa, and τ13 = -100 MPa FIG. 12 Sample d (2θ) Versus sin2β Dataset with χm = +12°, σ11 = -500 MPa, τ23 = -100 MPa, and Measured σ11 = -472.5 MPa FIG. 13 Sample d (2θ) Versus sin2β Dataset with χm = -12°, σ11 = -500 MPa, τ23 = -100 MPa, and Measured σ11 = -527.5 MPa 5.4.6 The τ23 value affects the d versus sin2β slope in a similar fashion to σ11 for each detector position (Figs. 12 and 13). This is an unwanted effect since the σ11 and τ23 influence cannot be resolved for one χm position. In this instance, the τ23 shear stress of -100 MPa results in a calculated σ11 value of -472.5 MPa for χm = +12° or -527.5 MPa for χm = -12°, while the actual value is -500 MPa. The value, σ11 can still be determined by averaging the β data for both χm positions. 5.4.7 The use of the modified chi mode may be used to determine σ11 but shall be approached with caution using one χm position because of the possible presence of a τ23 stress. The combination of multiple shear stresses including τ23 results in increasingly complex shear influences. Chi and omega mode are preferred over modified chi for these reasons. 1.1 This test method covers a procedure for experimentally determining macroscopic residual stress tensor components of quasi-isotropic bearing steel materials by X-ray diffraction (XRD). 1.2 This test method provides a guide for experimentally determining stress values, which play a significant role in bearing life. 1.3 Examples of how tensor values are used are: 1.3.1 Detection of grinding type and abusive grinding; 1.3.2 Determination of tool wear in turning operations; 1.3.3 Monitoring of carburizing and nitriding residual stress effects; 1.3.4 Monitoring effects of surface treatments such as sand blasting, shot peening, and honing; 1.3.5 Tracking of component life and rolling contact fatigue effects; 1.3.6 Failure analysis; 1.3.7 Relaxation of residual stress; and 1.3.8 Other residual-stress-related issues that potentially affect bearings. 1.4 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D1253-14(2021)e1 Standard Test Method for Residual Chlorine in Water Active 发布日期 :  1970-01-01 实施日期 : 

5.1 Chlorine is used to destroy or deactivate a variety of unwanted chemicals and microorganisms in water and wastewater.5.2 An uncontrolled excess of chlorine in water, whether free available or combined, can adversely affect the subsequent use of the water.1.1 This test method covers the determination of residual chlorine in water by direct amperometric titration.1.2 Within the constraints specified in Section 6, this test method is not subject to commonly encountered interferences and is applicable to most waters. Some waters, however, can exert an iodine demand, usually because of organic material, making less iodine available for measurement by this test method. Thus, it is possible to obtain falsely low chlorine readings, even though the test method is working properly, without the user's knowledge.1.3 Precision data for this test method were obtained on estuary, inland main stem river, fresh lake, open ocean, and fresh cooling tower blowdown water. Bias data could not be determined because of the instability of solutions of chlorine in water. It is the user's responsibility to ensure the validity of the test method for untested types of water.1.4 In the testing by which this standard was validated, the direct and back starch-iodide titrations and the amperometric back titration, formerly part of this standard, were found to be unworkable and were discontinued in 1986. Historical information is presented in Appendix X1.NOTE 1: Orthotolidine test methods have been omitted because of poor precision and accuracy.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 These test methods cover, in single procedures, the determination of Ni, V, and Fe in crude oils and residual oils. These test methods complement Test Method D1548, which covers only the determination of vanadium.4.2 When fuels are combusted, vanadium present in the fuel can form corrosive compounds. The value of crude oils can be determined, in part, by the concentrations of nickel, vanadium, and iron. Nickel and vanadium, present at trace levels in petroleum fractions, can deactivate catalysts during processing. These test methods provide a means of determining the concentrations of nickel, vanadium, and iron.1.1 These test methods cover the determination of nickel, vanadium, and iron in crude oils and residual fuels by inductively coupled plasma (ICP) atomic emission spectrometry. Two different test methods are presented.1.2 Test Method A (Sections 7 – 11 and 18 – 22)—ICP is used to analyze a sample dissolved in an organic solvent. This test method uses oil-soluble metals for calibration and does not purport to quantitatively determine or detect insoluble particulates.1.3 Test Method B (Sections 12 – 22)—ICP is used to analyze a sample that is decomposed with acid.1.4 The concentration ranges covered by these test methods are determined by the sensitivity of the instruments, the amount of sample taken for analysis, and the dilution volume. A specific statement is given in 15.2. Typically, the low concentration limits are a few tenths of a milligram per kilogram. Precision data are provided for the concentration ranges specified in Section 21.1.5 The values stated in SI units are to be regarded as standard.1.5.1 Exception—The values given in parentheses are for information only.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Residual strain measurements are an aid in the design and fabrication of MEMS devices. The value for residual strain can be used in Young's modulus calculations.1.1 This test method covers a procedure for measuring the compressive residual strain in thin films. It applies only to films, such as found in microelectromechanical systems (MEMS) materials, which can be imaged using an optical interferometer, also called an interferometric microscope. Measurements from fixed-fixed beams that are touching the underlying layer are not accepted.1.2 This test method uses a non-contact optical interferometric microscope with the capability of obtaining topographical 3-D data sets. It is performed in the laboratory.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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6.1 This test method provides standard procedures for experimentally determining the XEC for use in the measurement of residual and applied stresses using x-ray diffraction techniques. It also provides a standard means of reporting the precision of the XEC.6.2 This test method is applicable to any crystalline material that exhibits a linear relationship between stress and strain in the elastic range, that is, only applicable to elastic loading.6.3 This test method should be used whenever residual stresses are to be evaluated by x-ray diffraction techniques and the XEC of the material are unknown.1.1 This test method covers a procedure for experimentally determining the x-ray elastic constants (XEC) for the evaluation of residual and applied stresses by x-ray diffraction techniques. The XEC relate macroscopic stress to the strain measured in a particular crystallographic direction in polycrystalline samples. The XEC are a function of the elastic modulus, Poisson’s ratio of the material and the hkl plane selected for the measurement. There are two XEC that are referred to as 1/2 S2hkl and S1 hkl.1.2 This test method is applicable to all x-ray diffraction instruments intended for measurements of macroscopic residual stress that use measurements of the positions of the diffraction peaks in the high back-reflection region to determine changes in lattice spacing.1.3 This test method is applicable to all x-ray diffraction techniques for residual stress measurement, including single, double, and multiple exposure techniques.1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method provides a quantitative measure useful in the evaluation of the performance of fiber–reinforced concrete. It allows for comparative analysis among beams containing different fiber types, including materials, dimension and shape, and different fiber contents. Results can be used to optimize the proportions of fiber–reinforced concrete mixtures, to determine compliance with construction specifications, to evaluate fiber–reinforced concrete which has been in service, and as a tool for research and development of fiber–reinforced concrete (See Note 2).NOTE 2: Banthia and Dubey3 compared results using this test method with residual strengths at the same net deflections using a test protocol that is similar to that described in Test Method C1609/C1609M on 45 beams with a single fiber configuration at proportions of 0.1, 0.3, and 0.5 % by volume. The results by this test method were on average 6.4 % lower than by the procedure of Test Method C1609/C1609M.5.2 Test results are intended to reflect either consistency or differences among variables used in proportioning the fiber–reinforced concrete to be tested, including fiber type (material), fiber size and shape, fiber amount, beam preparation (sawed or molded), and beam conditioning.5.3 In molded beams fiber orientation near molded surfaces will be affected by the process of molding. For tests of fiber-reinforced concrete containing relatively rigid or stiff fibers of length greater than 35 mm [1.4 in.], the use of sawed beams cut from samples with an initial width and depth of at least 3 times the length of the fiber is required to minimize effects of fiber orientation. When sawed beams are employed, and to avoid the effects of fiber orientation, care shall be applied to ensure that the flexural tensile surface of the beam is a sawed surface.1.1 This test method covers the determination of residual strength of a fiber–reinforced concrete test beam. The average residual strength is computed using specified beam deflections that are obtained from a beam that has been cracked in a standard manner. The test provides data needed to obtain that portion of the load–deflection curve beyond which a significant amount of cracking damage has occurred and it provides a measure of post–cracking strength, as such strength is affected by the use of fiber–reinforcement.1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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5.1 Residual fuel oils can contain H2S in the liquid phase, and this can result in hazardous vapor phase levels of H2S in storage tank headspaces. The vapor phase levels can vary significantly according to the headspace volume, fuel temperature, and agitation. Measurement of H2S levels in the liquid phase provides a useful indication of the residual fuel oil’s propensity to form high vapor phase levels, and lower levels in the residual fuel oil will directly reduce risk of H2S exposure. It is critical, however, that anyone involved in handling fuel oil, such as vessel owners and operators, continue to maintain appropriate safety practices designed to protect the crew, tank farm operators and others who can be exposed to H2S.5.1.1 The measurement of H2S in the liquid phase is appropriate for product quality control, while the measurement of H2S in the vapor phase is appropriate for health and safety purposes.5.2 This test method was developed so refiners, fuel terminal operators and independent testing laboratory personnel can analytically measure the amount of H2S in the liquid phase of residual fuel oils.NOTE 1: Test Method D6021 is one of three test methods for quantitatively measuring H2S in residual fuels:1) Test Method D5705 is a simple field test method for determining H2S levels in the vapor phase.2) Test Method D7621 is a rapid test method to determine H2S levels in the liquid phase.5.3 H2S concentrations in the liquid and vapor phase attempt to reach equilibrium in a static system. However, this equilibrium and the related liquid and vapor concentrations can vary greatly depending on temperature and the chemical composition of the liquid phase. A concentration of 1 mg/kg (μg/g) (ppmw) of H2S in the liquid phase of a residual fuel can typically generate an actual gas concentration of >50 μL/L(ppmv) to 100 μL/L(ppmv) of H2S in the vapor phase, but the equilibrium of the vapor phase is disrupted the moment a vent or access point is opened to collect a sample.NOTE 2: Because of the reactivity, absorptivity, and volatility of H2S any measurement method only provides an H2S concentration at a given moment in time.1.1 This test method covers a method suitable for measuring the total amount of hydrogen sulfide (H2S) in heavy distillates, heavy distillate/residual fuel blends, or residual fuels as defined in Specification D396 Grade 4, 5 (Light), 5 (Heavy), and 6, when the H2S concentration in the fuel is in the 0.01 μg/g (ppmw) to 100 μg/g (ppmw) range.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see 7.5, 8.2, 9.2, 10.1.4, and 11.1.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Vinyl chloride-containing polymers are widely used to package a variety of materials, including foods.5.2 Vinyl chloride monomer has been shown to be a human carcinogen. Threshold toxicity value has not been established.5.3 Plastic manufacturers, food packagers, government agencies, etc. have a need to know the residual vinyl chloride monomer content of vinyl chloride-containing polymers.1.1 This test method is suitable for determining the residual vinyl chloride monomer (RVM) content of homopolymer and copolymers of vinyl chloride down to a concentration of ∼5 µg/kg (ppb).1.2 This test method is applicable to any polymer form, such as resin, compound, film, bottle wall, etc. that can be dissolved in a suitable solvent.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in Section 9 and Note 10.NOTE 1: This standard is equivalent to ISO 6401.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Excessive amounts of sodium can indicate the presence of materials that cause high wear of burner pumps and valves, and contribute to deposits of boiler heating surfaces.1.1 This test method covers the determination of sodium in residual fuel oil by means of a flame photometer. Its precision in low ranges limits its application to samples containing more than 15 mg/kg sodium. Other elements commonly found in residual fuel oil do not interfere.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements see 7.3, 7.5, 7.7, 9.2, 7.8, 7.9, and Note 3.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The procedure in this test method for a sample as specified herein is intended for the purpose of determining the residual moisture present in a RDF analysis sample.5.2 The residual moisture value is used to correct as-determined analysis results such as gross heating value, sulfur, and ash to dry sample basis results.1.1 This test method covers the measurement of residual moisture in refuse-derived fuel (RDF) analysis samples. It is used to calculate on a dry basis other determinations performed on analysis RDF samples. It is used with air-dry moisture results to calculate total moisture (Note 1). The total moisture is used to calculate as-received values or other analyses performed on a sample.NOTE 1: In some instances, RDF moisture may change during size-reduction steps of the RDF analysis sample preparation procedure. This moisture change, unless suitable corrections are made, will affect the accuracy of the total moisture value as calculated from the air-dry and residual moisture results.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For more specific precautionary information, see Section 7.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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