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4.1 These test methods for the chemical analysis of metals and alloys are primarily intended as referee methods to test such materials for compliance with compositional specifications, particularly those under the jurisdiction of ASTM Committees A01 on Steel, Stainless Steel, and Related Alloys and A04 on Iron Castings. It is assumed that all who use these test methods will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory under appropriate quality control practices such as those described in Guide E882.1.1 These test methods cover the chemical analysis of carbon steels, low-alloy steels, silicon electrical steels, ingot iron, and wrought iron having chemical compositions within the following limits:Element  Composition Range, %Aluminum 0.001  to 1.50Antimony 0.002  to 0.03Arsenic 0.0005 to 0.10Bismuth 0.005  to 0.50Boron 0.0005 to 0.02Calcium 0.0005 to 0.01Cerium 0.005  to 0.50Chromium 0.005  to 3.99Cobalt 0.01   to 0.30Columbium (Niobium) 0.002  to 0.20Copper 0.005  to 1.50Lanthanum 0.001  to 0.30Lead 0.001  to 0.50Manganese 0.01   to 2.50Molybdenum 0.002  to 1.50Nickel 0.005  to 5.00Nitrogen 0.0005 to 0.04Oxygen 0.0001 to 0.03Phosphorus 0.001  to 0.25Selenium 0.001  to 0.50Silicon 0.001  to 5.00Sulfur 0.001  to 0.60Tin 0.002  to 0.10Titanium 0.002  to 0.60Tungsten 0.005  to 0.10Vanadium 0.005  to 0.50Zirconium 0.005  to 0.151.2 The test methods in this standard are contained in the sections indicated as follows:  Sections   Aluminum, Total, by the 8-Quinolinol Gravimetric Method (0.20 % to 1.5 %) 124–131Aluminum, Total, by the 8-Quinolinol Spectrophotometric Method (0.003 % to 0.20 %) 76–86Aluminum, Total or Acid-Soluble, by the Atomic Absorption Spectrometry Method (0.005 % to 0.20 %) 308–317Antimony by the Brilliant Green Spectrophotometric Method (0.0002 % to 0.030 %) 142–151Bismuth by the Atomic Absorption Spectrometry Method (0.02 % to 0.25 %) 298–307Boron by the Distillation-Curcumin Spectrophotometric Method (0.0003 % to 0.006 %) 208–219Calcium by the Direct-Current Plasma Atomic Emission Spectrometry Method (0.0005 % to 0.010 %) 289–297Carbon, Total, by the Combustion Gravimetric Method (0.05 % to 1.80 %)—Discontinued 1995  Cerium and Lanthanum by the Direct Current Plasma Atomic Emission Spectrometry Method (0.003 % to 0.50 % Cerium, 0.001 % to 0.30 % Lanthanum) 249–257Chromium by the Atomic Absorption Spectrometry Method (0.006 % to 1.00 %) 220–229Chromium by the Peroxydisulfate Oxidation-Titration Method (0.05 % to 3.99 %) 230–238Cobalt by the Nitroso-R Salt Spectrophotometric Method (0.01 % to 0.30 %) 53–62Copper by the Sulfide Precipitation-Iodometric Titration Method (Discontinued 1989) 87–94Copper by the Atomic Absorption Spectrometry Method (0.004 % to 0.5 %) 279–288Copper by the Neocuproine Spectrophotometric Method (0.005 % to 1.50 %) 114–123Lead by the Ion-Exchange—Atomic Absorption Spectrometry Method (0.001 % to 0.50 %) 132–141Manganese by the Atomic Absorption Spectrometry Method (0.005 % to 2.0 %) 269–278Manganese by the Metaperiodate Spectrophotometric Method (0.01 % to 2.5 %) 9–18Manganese by the Peroxydisulfate-Arsenite Titrimetric Method (0.10 % to 2.50 %) 164–171Molybdenum by the Thiocyanate Spectrophotometric Method (0.01 % to 1.50 %) 152–163Nickel by the Atomic Absorption Spectrometry Method (0.003 % to 0.5 %) 318–327Nickel by the Dimethylglyoxime Gravimetric Method (0.1 % to 5.00 %) 180–187Nickel by the Ion-Exchange-Atomic-Absorption Spectrometry Method (0.005 % to 1.00 %) 188–197Nitrogen by the Distillation-Spectrophotometric Method (Discontinued 1988) 63–75Phosphorus by the Alkalimetric Method (0.02 % to 0.25 %) 172–179Phosphorus by the Molybdenum Blue Spectrophotometric Method (0.003 % to 0.09 %) 19–30Silicon by the Molybdenum Blue Spectrophotometric Method (0.01 % to 0.06 %) 103–113Silicon by the Gravimetric Titration Method (0.05 % to 3.5 %) 46–52Sulfur by the Gravimetric Method (Discontinued 1988) 31–36Sulfur by the Combustion-Iodate Titration Method (0.005 % to 0.3 %) (Discontinued 2017) 37–45Tin by the Sulfide Precipitation-Iodometric Titration Method (0.01 % to 0.1 %) 95–102Tin by the Solvent Extraction-Atomic Absorption Spectrometry Method (0.002 % to 0.10 %) 198–207Titanium by the Diantipyrylmethane Spectrophotometric Method (0.025 % to 0.30 %) 258–268Vanadium by the Atomic Absorption Spectrometry Method (0.006 % to 0.15 %) 239–2481.3 Test methods for the determination of several elements not included in this standard can be found in Test Methods E1019.1.4 Some of the composition ranges given in 1.1 are too broad to be covered by a single test method and therefore this standard contains multiple test methods for some elements. The user must select the proper test method by matching the information given in the and Interference sections of each test method with the composition of the alloy to be analyzed.1.5 The values stated in SI units are to be regarded as standard. In some cases, exceptions allowed in IEEE/ASTM SI 10 are also used.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazards statements are given in Section 6 and in special “Warning” paragraphs throughout these test methods.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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3.1 The oxidation of silicon carbide refractories at elevated temperatures is an important consideration in the application of these refractories. The product of oxidation is amorphous silica or cristobalite, depending upon the temperature at which oxidation takes place. This oxide formation is associated with expansion and degradation of strength. The quantity of water vapor in the atmosphere greatly affects the rate of oxidation.3.2 The test, which creates and measures the expansion, is suitable for guidance in product development and relative comparison in application work where oxidation potential is of concern. The variability of the test is such that it is not recommended for use as a referee test.1.1 This test method covers the evaluation of the oxidation resistance of silicon carbide refractories at elevated temperatures in an atmosphere of steam. The steam is used to accelerate the test. Oxidation resistance is the ability of the silicon carbide (SiC) in the refractory to resist conversion to silicon dioxide (SiO2) and its attendant crystalline growth.1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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DESIG: E360 96 (Reapproved 2001) ^TITLE: Standard Test Methods for Chemical Analysis of Silicon and Ferrosilicon ^SCOPE:1.1 These test methods cover the chemical analysis of silicon and ferrosilicon having chemical compositions within the following limits:0.10 maxElement Concentration, %Aluminum 2.0 maxArsenicCalcium 1.00 maxCarbon 0.50 maxChromium 0.50 maxCopper 0.30 maxManganese 1.00 maxNickel 0.30 maxPhosphorus 0.10 maxSilicon 20.00 to 99.5Sulfur 0.025 maxTitanium 0.20 max1.2 The test methods appear in the following order: SectionsArsenic by the Molybdenum Blue Photometric Method Aluminum by the Quinolinate Photometric and GravimetricMethods Silicon by the Sodium Peroxide Fusion-Perchloric Acid Dehydration Method 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 5 and 26.8.1, 27.4.1.1, and 36.3.1.

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This specification covers three grades, Grades A, B, and C, of carbon-manganese-silicon steel plates intended primarily for service in welded pressure vessels where improved low temperature notch toughness is important. The maximum thickness of plates is limited only by the capacity of the composition to meet the specified mechanical property requirements. The steel shall be killed and the plates shall undergo heat treatment. Tensile properties such as tensile strength, yield strength and elongation shall be determined by subjecting the steel plates to a tension test.1.1 This specification2 covers three grades of carbon-manganese-silicon steel plates intended primarily for service in welded pressure vessels where improved low temperature notch toughness is important.1.2 The maximum thickness of plates is limited only by the capacity of the composition to meet the specified mechanical property requirements.1.3 For plates produced from coil and furnished without heat treatment or with stress relieving only, the additional requirements, including additional testing requirements and the reporting of additional test results, of Specification A20/A20M apply.1.4 The values stated in either inch-pound units or SI units are to be regarded separately as standard. Within the text, the SI units are shown in brackets. The values stated in each system are not exact equivalents; therefore, each system must be used independently of the other. Combining values from the two systems may result in nonconformance with the specification.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification covers alloy steels having a chromium content equal to or less than 11.0% in plate, sheet, strip form for corrosion, and heat-resisting applications. Some steels, especially the high silicon containing steels, because of their particular alloy content and specialized properties, may require special care in their fabrication and welding. The steel shall conform to the requirements as to chemical composition. The mechanical properties such as tensile strength, yield strength, elongation and hardness shall be determined.1.1 This specification covers alloy steels having a chromium content equal to or less than 11.0 % in plate, sheet, strip form for corrosion, and heat-resisting applications.1.2 Some steels covered by this specification, especially the high silicon containing steels, because of their particular alloy content and specialized properties, may require special care in their fabrication and welding. Specific procedures are of fundamental importance, and it is presupposed that all parameters will be in accordance with approved methods capable of producing the desired properties in the finished fabrication.1.3 The values stated in inch-pound units or SI units are to be regarded separately as standard. The values stated in each system are not exact equivalents; therefore, each system must be used independently of the other. Combining values from the two systems may result in nonconformance with the specification.1.4 This specification and the applicable material specifications are expressed in both inch-pound and SI units. However, unless the order specifies the applicable "M" specification designation (SI units), the material shall be furnished in inch-pound units.

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ASTM E364-94(2000) Standard Test Methods for Chemical Analysis of Ferrochrome-Silicon (Withdrawn 2006) Withdrawn, No replacement 发布日期 :  1970-01-01 实施日期 : 

1.1 These test methods cover the chemical analysis of ferrochrome-silicon having chemical compositions within the following limits:Element Concentration,%Aluminum 0.50 maxAntimony 0.005 maxArsenic 0.005 maxBismuth 0.005 maxBoron 0.005 maxCarbon 0.15 maxChromium 34.0 to 47.0Cobalt 0.10 maxColumbium 0.050 maxCopper 0.050 maxLead 0.005 maxManganese 0.75 maxMolybdenum 0.050 maxNickel 0.50 maxNitrogen 0.050 maxPhosphorus 0.030 maxSilicon 30.0 to 45.0Silver 0.005 maxSulfur 0.030 maxTantalum 0.050 maxTin 0.005 maxTitanium 0.50 maxVanadium 0.50 maxZinc 0.005 maxZirconium 0.050 max1.2 The test methods appear in the following order: SectionsArsenic by the Molybdenum Blue Photometric Method 8-18Chromium by the Acid Dissolution Titrimetric Method 19-25Silicon by the Sodium Peroxide Fusion-Perchloric Acid Dehydration Method 26-331.3This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For precautions to be observed in these test methods, refer to Practices E50, and to precautions included in the individual methods.

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This specification covers manganese-silicon carbon steel plates for use in welded boilers and other pressure vessels. Plates under this specification are produced in two grades. The steel shall be killed and shall conform to the fine austenitic grain size requirement. Tension test shall be made to conform to the requirements specified.1.1 This specification2 covers manganese-silicon carbon steel plates for use in welded boilers and other pressure vessels.1.2 Plates under this specification are produced in two grades. The specified minimum yield strength decreases for thicknesses over 1 in. [25 mm].1.3 The maximum thickness of plates is limited only by the capacity of the composition to meet the specified mechanical property requirements.1.4 For plates produced from coil and furnished without heat treatment or with stress relieving only, the additional requirements, including additional testing requirements and the reporting of additional test results, of Specification A20/A20M apply.1.5 The values stated in either inch-pound units or SI units are to be regarded separately as standard. Within the text, the SI units are shown in brackets. The values stated in each system are not exact equivalents; therefore, each system must be used independently of the other. Combining values from the two systems may result in nonconformance with the specification.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Catalyst fines in fuel oils can cause abnormal engine wear. These test methods provide a means of determining silicon and aluminum, the major constituents of the catalysts.1.1 These test methods cover the determination of aluminum and silicon in fuel oils at concentrations between 5 mg/kg and 150 mg/kg for aluminum and 10 mg/kg and 250 mg/kg for silicon.1.2 Test Method A—Inductively coupled plasma atomic emission spectrometry is used in this test method to quantitatively determine aluminum and silicon.1.3 Test Method B—Flame atomic absorption spectrometry is used in this test method to quantitatively determine aluminum and silicon.1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific warning statements are given in Sections 7.6, 10.1, and 11.5.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM A922-05(2020) Standard Specification for Silicon Metal Active 发布日期 :  1970-01-01 实施日期 : 

This specification covers different sizes of several grades of silicon metal. The metal shall undergo chemical analysis and shall conform to specified chemical composition requirements.1.1 This specification covers several grades of silicon metal.1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard. The SI equivalents of inch-pound units given may be approximate.1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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1.1 This specification covers grades of nominal-wall-thickness, austenitic alloy steel tubing for general corrosion-resisting and low- or high-temperature service, having a specified minimum chromium content of less than 10.50 %.1.2 The tubing sizes and thicknesses usually furnished to this specification are 1/4 in. (6.4 mm) in inside diameter and larger and 0.020 in. (0.51 mm) in nominal wall-thickness and heavier.1.3 Mechanical property requirements do not apply to tubing smaller than 1/8 in. (3.2 mm) in inside diameter or 0.015 in. (0.38 mm) in thickness.1.4 Some steels covered by this specification, especially the high silicon containing steels, because of their particular alloy content and specialized properties, may require special care in their fabrication and welding. Specific procedures are of fundamental importance, and it is presupposed that all parameters will be in accordance with approved methods capable of producing the desired properties in the finished fabrication.1.5 The values stated in either inch-pound units or SI units are to be regarded separately as standard. The values stated in each system are not exact equivalents; therefore, each system must be used independently of the other. Combining values from the two systems may result in nonconformance with the specification. Unless the order specifies the applicable "M" specification designation (SI units), the material shall be furnished in inch-pound units.

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1.1 This specification covers seamless and straight-seam welded austenitic steel pipe intended for high-temperature and general corrosive service, having a specified minimum chromium content of less than 10.50 %.1.2 Appendix X1 lists the dimensions of welded and seamless stainless steel pipe as shown in ANSI B36.19. Pipe having other dimensions may be furnished provided such pipe complies with all other requirements of this specification.1.3 The values stated in either inch-pound units or SI units are to be regarded separately as standard. The values stated in each system are not exact equivalents; therefore, each system must be used independently of the other. Combining values from the two systems may result in nonconformance with the specification. Unless the order specifies the applicable "M" specification designation (SI units), the material shall be furnished in inch-pound units.

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1.1 This specification details the generic criteria requirements of high pure titanium sputtering targets used as thin film material for through-silicon vias (TSV) metallization in advance packaging.1.2 Sputtering target purity, grain size, inner quality, bonding, dimension, and appearance specifications are included in this specification along with references for qualification test methods. Reliability, certification, traceability, and packaging requirements are also included.1.2.1 Purity Requirements: 1.2.1.1 Metallic element impurities, and1.2.1.2 Non-metallic element impurities.1.2.2 Grain Size Requirements—Grain size.1.2.3 Inner Quality Requirements—Internal defect.1.2.4 Bonding Requirements: 1.2.4.1 Backing plate, and1.2.4.2 Bonding ratio.1.2.5 Configuration Requirements: 1.2.5.1 Dimension,1.2.5.2 Tolerance, and1.2.5.3 Surface roughness.1.2.6 Appearance Requirements—Surface cleanness.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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This specification covers hot- and cold-finished alloy steel bars including rounds, squares, hexagons, and hot-rolled or extruded shapes for use in corrosion and heat-resisting service. The steel specimens shall be furnished in the solution annealed condition with subsequent light drawing and straightening permitted. The steel materials shall conform to the required chemical compositions of carbon, manganese, phosphorus, sulfur, silicon, nickel, chromium, and molybdenum. Mechanical tests shall be performed wherein the materials shall conform to the required values of tensile strength, yield strength, elongation, and hardness.1.1 This specification covers hot- and cold-finished alloy steel bars having a chromium content equal to or less than 11.0 % including rounds, squares, hexagons, and hot-rolled or extruded shapes for use in corrosion and heat-resisting service.1.2 Some steels covered by this specification, especially the high silicon-containing steels, because of their particular alloy content and specialized properties, may require special care in their fabrication and welding. Specific procedures are of fundamental importance, and it is presupposed that all parameters will be in accordance with approved test methods capable of producing the desired properties in the finished fabrication.1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.1.4 This specification and the applicable material specifications are expressed in both inch-pound and SI units. However, unless the order specifies the applicable “M” specification designation (SI units), the material shall be furnished in inch-pound units.

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ASTM A701/A701M-10(2020) Standard Specification for Ferromanganese-Silicon Active 发布日期 :  1970-01-01 实施日期 : 

This specification covers ferromanganese-silicon alloy. The alloys which are available in different sizes shall conform to the required chemical composition for manganese, carbon, silicon, phosphorus, arsenic, tin, lead, and chromium.1.1 This specification covers a manganese-silicon alloy.1.2 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.1.2.1 This specification is expressed in both inch-pound units and in SI units (within the text, the SI units are shown in brackets); however, unless the purchase order or contract specifies the applicable M specification designation (SI units), the inch-pound units shall apply.1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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1.1 This specification covers chromium-manganese-silicon alloy steel plates, intended particularly for welded boilers and other pressure vessels.1.2 Plates under this specification are available in two grades having strength levels as follows:Grade Tensile Strengthksi [MPa]A 75-95 [515-655]B 85-110 [585-760]1.3 The maximum thickness of plates is limited only by the capacity of the composition to meet the specified mechanical property requirements; however, current practice normally limits the maximum thickness of plates furnished under this specification to 2 in. [50 mm].1.4 Grade A is suitable for rivets and when so used the bars shall be subject to the requirements for rolled bars specified in Specification A 31, except for the chemical and mechanical requirements.1.5 The values stated in either inch-pound units or SI units are to be regarded separately as standard. Within the text, the SI units are shown in brackets. The values stated in each system are not exact equivalents. Therefore, each system must be used independently of the other. Combining values from the two systems may result in nonconformance with this specification.

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