4.1 Proper preparation and mounting of specimens is particularly critical for surface analysis. Improper preparation of specimens can result in alteration of the surface composition and unreliable data. Specimens should be handled carefully so as to avoid the introduction of spurious contaminants in the preparation and mounting process. The goal must be to preserve the state of the surface so that the analysis remains representative of the original.4.2 AES, XPS or ESCA, and SIMS are sensitive to surface layers that are typically a few nanometres thick. Such thin layers can be subject to severe perturbations caused by specimen handling (1)4 or surface treatments that may be necessary prior to introduction into the analytical chamber. In addition, specimen mounting techniques have the potential to affect the intended analysis.4.3 This guide describes methods that the surface analyst may need to minimize the effects of specimen preparation when using any surface-sensitive analytical technique. Also described are methods to mount specimens so as to ensure that the desired information is not compromised.4.4 Guide E1829 describes the handling of surface sensitive specimens and, as such, complements this guide.1.1 This guide covers specimen preparation and mounting prior to, during, and following surface analysis and applies to the following surface analysis disciplines:1.1.1 Auger electron spectroscopy (AES),1.1.2 X-ray photoelectron spectroscopy (XPS and ESCA), and1.1.3 Secondary ion mass spectrometry (SIMS).1.1.4 Although primarily written for AES, XPS, and SIMS, these methods will also apply to many surface sensitive analysis methods, such as ion scattering spectrometry, low energy electron diffraction, and electron energy loss spectroscopy, where specimen handling can influence surface sensitive measurements.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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This specification describes the construction and installation of standard reference specimens for quality control of laboratory sound transmission loss measurements. The reference specimen is composed of framed steel panels. The required materials for fabrication and installation are as follows: galvanized sheets, frame, and panels. Four kinds of installation may be done: Installation A using a single layer reference specimen, Installation B using double layer reference specimen with a common plate, Installation C using double layer reference specimen with separate plates-empty cavity, and Installation D using double layer reference specimen with separate plates and added layer of sound-absorbing material in the cavity.1.1 This specification describes the construction and installation of standard reference specimens for quality control of laboratory sound transmission loss measurements using Test Method E90.1.2 Laboratories may choose to construct and test all of the reference specimens described here or only a subset. Specific specimens may be required by a test method or an accrediting agency.1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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4.1 The purpose of testing dimension stone is to quantify the various material properties of the stone. The test should consistently predict performance of the stone in a specific application. Many of the test methods that have been developed are specific and attempt to approximate the anticipated behavior of the stone in the manner that is intended to be used, such as flexural strength, compressive strength, and anchor strength. Other test methods provide general information about the stone, such as absorption and density. Test data provides the designer with information required to produce rational designs and assess if the stone will perform adequately for its intended use.1.1 This guide covers sampling, selection, preparation, and conditioning of specimens that will be used to test material properties of dimension stone.1.2 This guide sets forth basic recommendations for sampling and preparation of dimension stone test specimens and provides information regarding variables that should be considered.1.3 This guide is intended to be used by architects, engineers, contractors and material suppliers who design, select, specify, install, purchase, fabricate, finish, or test natural stone products for construction applications.1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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5.1 The techniques described in this guide, if properly used in conjunction with a knowledge of behavior of particular material systems, will aid in the proper preparation of consolidated laminates for mechanical property testing.5.2 The techniques described are recommended to facilitate the consistent production of satisfactory test specimens by minimizing uncontrolled processing variance during specimen fabrication.5.3 Steps 3 through 8 of the 8-step process may not be required for particular specimen or test types. If the specimen or test does not require a given step in the process of specimen fabrication, that particular step may be skipped.5.4 A test specimen represents a simplification of the structural part. The test specimen's value lies in the ability of several sites to be able to test the specimen using standard techniques. Test data may not show identical properties to those obtained in a large structure, but a correlation can be made between test results and part performance. This may be due, in part, to the difficulty of creating a processing environment for test specimens that identically duplicates that of larger scale processes.5.5 Tolerances are guidelines based on current lab practices. This guide does not attempt to give detailed instructions due to the variety of possible panels and specimens that could be made. The tolerances should be used as a starting reference from which refinements can be made.1.1 This guide provides guidelines to facilitate the proper preparation of laminates and test specimens from fiber-reinforced organic matrix composite prepregs. The scope is limited to organic matrices and fiber reinforcement in unidirectional (tape) or orthagonal weave patterns. Other forms may require deviations from these general guidelines. Other processing techniques for test coupon preparation, for example, pultrusion, filament winding and resin-transfer molding, are not addressed.1.2 Specimen preparation is modeled as an 8-step process that is presented in Fig. 1 and Section 8. Laminate consolidation techniques are assumed to be by press or autoclave. This practice assumes that the materials are properly handled by the test facility to meet the requirements specified by the material supplier(s) or specification, or both. Proper test specimen identification also includes designation of process equipment, process steps, and any irregularities identified during processing.FIG. 1 8 Step Mechanical Test Data ModelNOTE 1: Material identification is mandatory. Continuous traceability of specimens is required throughout the process. Process checks (Appendix X4) may be done at the end of each step to verify that the step was performed to give a laminate or specimen of satisfactory quality. Steps 4 and 5 may be interchanged. For aramid fibers, step 5 routinely precedes step 4. Steps 6, 7 and 8 may be interchanged.1.3 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.1.3.1 Within the text, the inch-pound units are shown in brackets.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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5.1 Building products made with tapes are often used for applications for which Test Method E84 is used for compliance with building, life safety code or mechanical code requirements. This practice describes, in detail, specimen mounting procedures for tapes.5.2 Codes are often silent with regard to testing tapes for the assessment of flame spread and smoke development as surface burning characteristics. This practice describes specimen preparation and mounting procedures for such materials and products.5.3 The material shall be representative of the materials used in actual field installations.5.4 The limitations for this procedure are those associated with Test Method E84.1.1 This practice covers a procedure for specimen preparation and mounting when testing tapes to assess flame spread and smoke development as surface burning characteristics using Test Method E84. Tapes are to be tested in full coverage as applied to fiber cement board as described in Test Method E84.1.2 This practice applies to any tape intended for various uses within buildings.1.3 Testing is conducted in accordance with Test Method E84.1.4 This practice does not provide pass/fail criteria that can be used as a regulatory tool.1.5 This practice is not for system evaluation. It is for the comparison of the materials only.1.6 Use the values stated in inch-pound units as the standard, in referee decisions. The values in the SI system of units are given in parentheses, for information only; see IEEE/ASTM SI-10 for further details.1.7 This fire standard cannot be used to provide quantitative measures.1.8 Fire testing is inherently hazardous. Adequate safeguards for personnel and property shall be employed in conducting these tests.1.9 This standard gives instructions on specimen preparation and mounting, but the fire-test-response method is given in Test Method E84. See also Section 9.1.10 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes shall not be considered requirements of the standard.1.11 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.12 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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5.1 This test method provides reasonably accurate information with regard to the ability of an adhesive to withstand shearing forces. It may also be used to determine degree of cure and the effect of environment on shear strength.1.1 This test method covers the determination of the shear strength of curing liquid adhesives used for retaining cylindrical assemblies or for locking and sealing threaded fasteners.1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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5.1 The surface burning characteristics of wood products are often evaluated with Test Method E84 to comply with code requirements. This practice describes specimen preparation and mounting procedures for such materials and systems.5.2 If it can be demonstrated that none of the methods described in this practice are applicable to a particular wood product, other mounting methods shall be permitted to be used. This information shall be included in the report.5.3 The limitations for this procedure are those associated with Test Method E84.1.1 This practice describes procedures for specimen preparation and mounting when testing wood products to assess flames spread and smoke development as surface burning characteristics using Test Method E84 or Test Method E2768.1.1.1 Test Method E2768 uses the same test equipment as Test Method E84.1.2 This practice applies also to laminated products factory-produced with a wood substrate (see 8.6). This practice does not apply to wood veneers or facings intended to be applied on site over a wood substrate, which are covered by Practice E2404.1.3 Testing is conducted with Test Method E84 or with Test Method E2768.1.4 Testing for the reporting of the moisture content of the test specimen is conducted with Test Methods D4442.1.5 This practice does not provide pass/fail criteria that can be used as a regulatory tool.1.6 Units—Use the values stated in inch-pound units as the standard, in referee decisions. The values in the SI system of units are given in parentheses, for information only; see IEEE/ASTM SI-10 for further details.1.7 This fire standard cannot be used to provide quantitative measures.1.8 The text of this standard references notes and footnotes which provide explanatory materials. These notes and footnotes shall not be considered requirements of the standard.1.9 Fire testing of products and materials is inherently hazardous, and adequate safeguards for personnel and property shall be employed in conducting these tests. Fire testing involves hazardous materials and equipment. This standard gives instructions on specimen preparation and mounting, but the fire-test-response method is given in Test Method E84, or in Test Method E2768, as appropriate. See also Section 10.1.10 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.11 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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