【国外标准】 Standard Test Method for Nondestructive Assay of Plutonium, Tritium and 241Am by Calorimetric Assay
本网站 发布时间:
2024-02-28
开通会员免费在线看70000余条国内标准,赠送文本下载次数,单本最低仅合13.3元!还可享标准出版进度查询、定制跟踪推送、标准查新等超多特权!  
查看详情>>
标准简介
适用范围:
5.1 This test method is considered to be the most accurate NDA technique for the assay of many physical forms of Pu. Isotopic measurements by gamma-ray spectroscopy or destructive analysis techniques are part of this test method when it is applied to the assay of Pu.5.1.1 Calorimetry has been applied to a wide variety of Pu-bearing solids including metals, alloys, oxides, fluorides, mixed Pu-U oxides, mixed oxide fuel pins, waste, and scrap, for example, ash, ash heels, salts, crucibles, and graphite scarfings) (2, 3). This test method has been routinely used at U.S. and European facilities for Pu process measurements and nuclear material accountability since the mid 1960’s (2-9).5.1.2 Pu-bearing materials have been measured in calorimeter containers ranging in size from about 0.025 m to about 0.63 m in diameter and from about 0.076 m to about 1.38 m in height.5.1.3 Gamma-ray spectroscopy typically is used to determine the Pu isotopic composition and 241Am to Pu ratio (see Test Method C1030). However, isotopic information from mass spectrometry and alpha counting measurements may be used instead (see Test Method C697).5.2 This test method is considered to be the most accurate NDA method for the measurement of tritium. For many physical forms of tritium compounds calorimetry is currently the only practical measurement technique available.5.3 Physical standards representative of the materials being assayed are not required for the test method.5.3.1 This test method is largely independent of the elemental distribution of the nuclear materials in the matrix.5.3.2 The accuracy of the method can be degraded for materials with inhomogeneous isotopic composition.5.4 The thermal power measurement is traceable to national measurement systems through electrical standards used to directly calibrate the calorimeters or to calibrate secondary 238Pu heat standards.5.5 Heat-flow calorimetry has been used to prepare secondary standards for neutron and gamma-ray assay systems (7-12).5.6 Four parameters of the item and the item packaging affect measurement time. These four parameters are density, mass, thermal conductivity, and change in temperature. The measurement well of passive calorimeters will also affect measurement time because it too will need to come to the new equilibrium temperature. Calorimeters operated in power compensation mode maintain a constant measurement well temperature and have no additional effect on measurement time.5.6.1 Calorimeter measurement times range from 20 minutes (13) for smaller, temperature-conditioned containers up to 72 h (14) for larger containers and items with long thermal-time constants.5.6.2 Measurement times may be reduced by using equilibrium prediction techniques, by temperature preconditioning of the item to be measured, by operating the calorimeter using the power compensation technique, or by optimization of the item container (low thermal mass and high thermal conductivity) and packaging.1.1 This test method describes the nondestructive assay (NDA) of plutonium, tritium, and 241Am using heat flow calorimetry. For plutonium the typical range of applicability, depending on the isotopic composition, corresponds to ~0.1 g to ~5 g quantities while for tritium the typical range extends from ~0.001 g to ~400 g. This test method can be applied to materials in a wide range of container sizes up to 380 L. It has been used routinely to assay items whose thermal power ranges from 0.001 W to 135 W.1.2 This test method requires knowledge of the relative abundances of the plutonium isotopes and the 241Am/Pu mass ratio to determine the total plutonium mass.1.3 This test method provides a direct measure of tritium content.1.4 This test method provides a measure of 241Am either as a single isotope or mixed with plutonium.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
标准号:
ASTM C1458-16
标准名称:
Standard Test Method for Nondestructive Assay of Plutonium, Tritium and 241Am by Calorimetric Assay
英文名称:
Standard Test Method for Nondestructive Assay of Plutonium, Tritium and 241Am by Calorimetric Assay标准状态:
Active-
发布日期:
-
实施日期:
出版语种:
- 推荐标准
- 国家标准计划
- 24/30491443 DC standard
- 24/30489392 DC BS EN IEC 62358 Ferrite cores. Standard inductance factor for gapped cores and its tolerance
- BS ISO 19848:2024 - TC Tracked Changes. Ships and marine technology. Standard data for shipboard machinery and equipment
- BS ISO 19848:2024 Ships and marine technology. Standard data for shipboard machinery and equipment
- BS IEC 61360-7:2024 Standard data element types with associated classification scheme
- 24/30487130 DC BS EN 50566:2017/A2:2024 Product standard to demonstrate the compliance of wireless communication
- 24/30486472 DC - Product standard
- KS M ISO 4259-4 석유 및 관련 제품 — 측정 방법과 결과의 정밀도 — 제4부: 개별 실험실에서 표준 시험방법의 실행에 대한 ‘통계적 관리’ 상태를 확인하기 위한 통계적 관리도의 사용
- KS C IEC 61340-4-7 정전기학 — 제4-7부: 구체적 적용 분야에 대한 표준 시험방법 — 이온화
- KS C IEC 61340-4-6 정전기학 — 제4-6부: 구체적 적용 분야에 대한 표준 시험방법 — 손목접지대
- KS C IEC 61340-4-8 정전기학 — 제4-8부: 구체적 적용 분야에 대한 표준 시험방법 — ESD 차폐성 — 봉투
- 24/30485973 DC standard
- BS EN 14662-1:2023 - TC Tracked Changes. Ambient air quality. Standard method for measurement of benzene concentrations
- KS C IEC 61837-2 주파수 제어 및 선택을 위한 표면 실장형 압전 장치 — 표준 아웃라인 및 단자 리드 연결 — 제2부: 세라믹 함체
- BS EN IEC 61753-081-02:2023 Fibre optic interconnecting devices and passive components. Performance standard