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4.1 These test methods were developed to measure the types and amounts of aromatics in mineral spirits to determine compliance with air pollution regulations that restrict the aromatic content of solvents. They have been demonstrated to be workable and to produce accurate results. However, due to the sensitivity of the tests to operating variables, some laboratories having limited experience with gas chromatographic analyses of hydrocarbons may experience difficulty in performing the tests.1.1 These test methods cover the determination of ethylbenzene and total eight-carbon (C8) and heavier aromatics in the concentration range from 0.1 to 30 % in mineral spirits having a distillation range from 149 to 210 °C (300 to 410 °F) as determined by Test Method D86. The procedures permit the identification and calculation of concentrations of aromatic components to 0.1 volume %.1.2 It is recognized by analytical chemists that a single column gas chromatography analysis of an unknown sample is risky. In such cases, multiple and different analytical techniques must be used for absolutely positive identification, for example, several different gas chromatography columns, gas chromatography/mass spectrometer, or gas chromatography/infrared, etc. In these test methods the material is known and is clearly defined.1.3 Oxygenated compounds, if present, may interfere and cause erroneous results. Such oxygenated compounds are not normally present in mineral spirits.1.4 Three test methods are covered as follows:1.4.1 Test Method A, measurement of ethylbenzene content, C8 plus higher aromatics (except ethylbenzene), and total aromatics by means of a single packed column gas chromatographic analysis.1.4.2 Test Method B, measurement of ethylbenzene content by means of a rapid packed column gas chromatographic analysis.1.4.3 Test Method C, measurement of ethylbenzene content, C8 plus higher aromatics (except ethylbenzene) and total aromatics by means of a capillary column gas chromatographic analysis.1.5 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.6 For purposes of determining conformance of an observed or a calculated value using this test method to relevant specifications, test result(s) shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29.1.7 For hazard information and guidance, see the supplier’s Material Safety Data Sheet.1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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3.1 This test method is used to determine the quality of adhesion of the granular surfacing to the coating asphalt in a sample of mineral-surfaced roofing. The results determine compliance with the applicable specification requirements or for comparative analysis. This test method applies to “as manufactured” material and may not be applicable to material that has had weathering exposure.1.1 This test method covers the determination of granule adhesion to mineral-surfaced roofing due to abrasion.1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Thermocouples fabricated from thermocouple cable that has been contaminated by moisture or by other impurities may undergo large changes in thermoelectric properties or may fail catastrophically when exposed to high temperatures. Since such contamination usually lowers the electrical resistance between the thermoelements and the sheath substantially, measurement of the insulation resistance can provide a valuable check of insulation quality and cleanliness, and can serve as a basis for rejection of unsuitable material and unreliable components. For manufacturers in particular, low electrical insulation resistance can also be indicative of displaced thermoelements or conductors or defects in the metal sheath which will require further investigation, but all users should be aware of these potential defects when faced with an unacceptable insulation resistance measurement.5.2 This test method is primarily intended for use by manufacturers and users of mineral-insulated, metal-sheathed (MIMS) thermocouples or MIMS cables to verify that measured values of insulation resistance exceed specified minimum values, such as those listed in Specifications E235, E585/E585M, E608/E608M, E2181/E2181M, and E2821. Manufacturers and users should be aware, however, that when the insulation resistance is greater than 1 × 108 Ω, disagreement by an order of magnitude in the results obtained with this test method is not unusual. In addition, users of this test method should appreciate that the room temperature insulation resistance of both MIMS cables and of finished thermocouples will change during shipment, storage, and use if the end seals are damaged or defective. Consequently, values of insulation resistance determined by this test method may not necessarily be repeatable.1.1 This test method provides the procedures for measuring the room temperature electrical insulation resistance between the thermoelements and between the thermoelements and the sheath, of a mineral-insulated, metal-sheathed (MIMS) thermocouple or mineral-insulated, metal-sheathed (MIMS) thermocouple cable or between the conductors and between the conductors and the sheath, of mineral-insulated, metal-sheathed (MIMS) cable used for industrial resistance thermometers. It may be used to measure the insulation resistance of bulk lengths of mineral-insulated, metal-sheathed MIMS cable previously sealed against moisture intrusion or to test a thermocouple having an ungrounded measuring junction. This method cannot be used to test a thermocouple having a grounded measuring junction unless the measuring junction is removed prior to testing, after which the thermocouple may be dealt with in the same manner as a mineral-insulated, metal-sheathed (MIMS) cable.1.2 This test method applies primarily to thermocouple cables and cable used for industrial resistance thermometers conforming to Specifications E585/E585M, E2181/E2181M, and E2821 and to thermocouples conforming to Specifications E608/E608M and E2181/E2181M, but may also be applied to thermocouples or MIMS cables that are suitable for use in air, whose sheath or thermoelements or conductors are comprised of refractory metals, that are tested in a dry and chemically inert environment, and that may employ compacted ceramic insulating materials other than magnesia (MgO) or alumina (Al2O3). Users of this test method should note that specifications dealing with compacted ceramic insulating materials other than magnesia or alumina, which are described in Specification E1652, are not currently available. As a result, acceptance criteria must be agreed upon between the customer and supplier at the time of purchase, or alternatively, judgment and experience must be applied in establishing test voltage levels and acceptable insulation resistance values for these types of thermocouples and MIMS cables.1.3 This test method may be used for thermocouples or MIMS cables having an outside diameter of 0.5 mm (0.020 in.) or larger.1.4 Users of this test method should be aware that the room temperature insulation resistance of a mineral-insulated, metal-sheathed thermocouple or MIMS cable will change during shipment, storage, or use if they are not properly sealed.1.5 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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1.1 This performance specification covers mixtures of water-based latex polymer, mineral aggregates, and optional other admixtures that, when combined, create a weather-protective and aliphatic hydrocarbon-resistant coating over asphalt and other pavements. There are two variations of the coating (Class 1 and Class 2): Class 1, a standard version—typically black but can be other colors, and Class 2, designed to be a solar reflective version.1.2 Units—The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard.1.3 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements for the standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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The content of dissolved decay products in insulating oils is made up of a variety of compounds, such as peroxides, aldehydes, ketones, and organic acids. Each of them is partially adsorbed on the large surface of paper insulation leading to the premature aging of power transformers. The relative assessment of byproduct formation, therefore, can be used as an indicator of the aging of the mineral oil.1.1 This test method characterizes by spectrophotometry the relative level of dissolved decay products in mineral insulating oils of petroleum origin. While new oil is almost transparent to a monochromatic beam of light in the visible spectrum, the increasing concentration of dissolved decay products shift the absorbance curve to longer wavelengths.1.2 This test method is applicable to compare the extent of dissolved decay products for oils in service. It can assess the effectiveness of used or stored oil purification during the reclamation process, as well.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and to determine the applicability of regulatory limitations prior to use.

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4.1 Material finer than the 75-μm (No. 200) sieve can be separated from larger particles much more efficiently and completely by wet sieving than through the use of dry sieving. Therefore, when accurate determinations of material finer than 75 μm (No. 200) in fine or coarse aggregate are desired, this test method is used on the sample prior to dry sieving in accordance with Test Method C136/C136M. The results of this test method are included in the calculation in Test Method C136/C136M, and the total amount of material finer than 75 μm (No. 200) by washing, plus that obtained by dry sieving the same sample, is reported with the results of Test Method C136/C136M. Usually, the additional amount of material finer than 75 μm (No. 200) obtained in the dry sieving process is a small amount. If it is large, the efficiency of the washing operation should be checked. It could also be an indication of degradation of the aggregate.4.2 Plain water is adequate to separate the material finer than 75 μm (No. 200) from the coarser material with most aggregates. In some cases, the finer material is adhering to the larger particles, such as some clay coatings and coatings on aggregates that have been extracted from bituminous mixtures. In these cases, the fine material will be separated more readily with a wetting agent in the water.1.1 This test method covers the determination of the amount of material finer than a 75-μm (No. 200) sieve in aggregate by washing. Clay particles and other aggregate particles that are dispersed by the wash water, as well as water-soluble materials, will be removed from the aggregate during the test.1.2 Two procedures are included, one using only water for the washing operation, and the other including a wetting agent to assist the loosening of the material finer than the 75-μm (No. 200) sieve from the coarser material. Unless otherwise specified, Procedure A (water only) shall be used.1.3 The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard.NOTE 1: Sieve size is identified by its standard designation in Specification E11. The alternative designation given in parentheses is for information only and does not represent a different standard sieve size.1.4 The text of this standard refers to notes and footnotes that provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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1.1 This specification covers rerefined previously used mineral insulating liquid of petroleum origin for reuse as an insulating and cooling medium in new and existing power and distribution electrical apparatus, such as transformers, regulators, reactors, liquid filled circuit breakers, switchgear, and attendant equipment.1.2 This specification is intended to define a rerefined mineral insulating liquid that is functionally interchangeable and miscible with existing mineral insulating liquids, is compatible with existing apparatus, and with appropriate field maintenance2 will satisfactorily maintain its functional characteristics in its application in electrical equipment. This specification applies only to rerefined mineral insulating liquid as received prior to any processing. Liquids that undergo treatment in-situ are not covered by this specification.1.3 Formulated rerefined mineral insulating liquids may contain additives such as inhibitors, passivators, pour point depressants, flow modifiers, gassing tendency modifiers, and other compounds. This specification will address some of these but not all. It is the responsibility of the supplier to disclose information concerning the presence of all known additives and their concentration to the user.1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This guide provides a method to determine the thermal performance of low-density blanket-type insulation. It may be used for the purposes of quality assurance, certification, or research.4.2 The thermal resistance of low-density insulation depends significantly on the density, the thickness, and thermal conductivity. Typical low-density, mineral-fiber insulation for buildings may vary in density from one specimen to the next.4.3 Thermal tests are time-consuming in comparison with density and thickness measurements. Low-density insulation material is produced in large quantities. A typical lot would be a truckload or the amount necessary to insulate a house.4.4 The relatively low unit cost of this product and the relatively high cost of thermal resistance testing makes it cost-effective to test only a small percentage of the product area. It is recommended that there be a determination of the density that is representative of a lot by the measurement of the average density of a statistically representative sampling.4.5 A fewer number of thermal measurements are then made to determine the apparent thermal conductivity at the previously determined representative density. The essential significance of this guide is that a large lot of variable material is best characterized by: (a) determining the representative density, and by (b) determining the thermal property at this representative density with a small number of thermal measurements.4.6 Building insulation products are commonly manufactured in thicknesses ranging from 19 to 330 mm (0.75 to 13 in.) inclusive. Experimental work has verified that there is a dependence of λapp on thickness for some low density materials.4.7 The upper limit of test thickness for specimens evaluated using Test Methods C177, C518, and C1114 is established based upon the apparatus design, overall dimensions, expected thermal resistivity level and desired target accuracy. The testing organization is responsible for applying these restrictions when evaluating a product to ensure that the results meet applicable product labels and any existing regulatory requirements (2).4.8 Extrapolation of the apparent thermal conductivity or the thermal resistance beyond the ranges of thickness or density of products tested is not valid.1.1 This guide describes the calculation and interpolation of a thermal resistance value for low-density blanket-type insulation material at a particular density and thickness having been selected as representative of the product. It requires measured values of this average density and thickness, as well as apparent thermal conductivity values determined by either Test Method C177, C518, or C1114.1.2 This guide applies to a density range for mineral-fiber material of roughly 6.4 to 48 kg/m3 (0.4 to 3.0 lb/ft3). It is primarily intended to apply to low-density, mineral-fiber mass insulation batts and blankets, exclusive of any membrane facings. Apparent thermal conductivity data for these products are commonly reported at a mean temperature of 23.9°C (75°F) and a hot-to-cold plate temperature difference of 27.8°C (50°F) or 22.2°C (40°F).1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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