定价： 819元 / 折扣价： 697 元 加购物车

定价： 481元 / 折扣价： 409 元 加购物车

定价： 481元 / 折扣价： 409 元 加购物车

定价： 605元 / 折扣价： 515 元 加购物车

定价： 481元 / 折扣价： 409 元 加购物车

5.1 For ferromagnetic materials, magnetic particle examination is widely specified for the detection of surface and near-surface flaws such as cracks, laps, seams, and linearly oriented nonmetallic inclusions. Such examinations are included as mandatory requirements in some forging standards such as Specifications A508/A508M and A963/A963M.5.2 Use of alternating current as the power source for magnetic particle examination imposes a significant restriction on the detection of subsurface indications, so that the procedure is essentially limited to the finding of flaws that are open to the surface. Attention therefore is drawn to the need to have the component in the finish-machined condition before conducting the magnetic particle examination.5.3 The presence of residual magnetic fields in a component may be undesirable, and an advantage of the use of an ac power source for magnetic particle examination is that an acceptable level of demagnetization can be readily achieved.1.1 This practice covers a procedure for the magnetic particle examination of steel forgings using alternating current as the power source. The procedure will produce consistent results upon which acceptance standards can be based. This practice does not contain acceptance limits or recommended quality levels.1.2 Only alternating 50–60 cycle current shall be used as the electric power source for any of the magnetizing methods.1.3 When subsurface indications are sought in forgings, then dc magnetization in accordance with Practice A275/A275M should be used.1.4 The values stated in either inch-pound units or SI units are to be regarded separately as standard. Within the text, the SI units are shown in brackets. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined. Unless the order specifies the applicable “M” specification designation [SI units], the inch-pound units shall be used.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价： 590元 / 折扣价： 502 元 加购物车

4.1 The composition and sequential structure of alginate determines the functionality of alginate in an application. For instance, the gelling properties of an alginate are highly dependent upon the monomer composition and sequential structure of the polymer. Gel strength will depend upon the guluronic acid content (FG) and also the average number of consecutive guluronate moieties in G-block structures (NG>1).4.2 Chemical composition and sequential structure of alginate can be determined by 1H- and 13C-nuclear magnetic resonance spectroscopy (NMR). A general description of NMR can be found in <761> of the USP 35-NF30. The NMR methodology and assignments are based on data published by Grasdalen et al. (1979, 1981, 1983).4, 5, 6 The NMR technique has made it possible to determine the monad frequencies FM (fraction of mannuronate units) and FG (fraction of guluronate units), the four nearest neighboring (diad) frequencies FGG, FMG, FGM, FMM, and the eight next nearest neighboring (triad) frequencies FGGG, FGGM, FMGG, FMGM, FMMM, FMMG, FGMM, FGMG. Knowledge of these frequencies enables number averages of block lengths to be calculated. NG is the number average length of G-blocks, and NG>1 is the number average length of G-blocks from which singlets (-MGM-) have been excluded. Similarly, NM is the number average length of M-blocks, and NM>1 is the number average length of M-blocks from which singlets (-GMG-) have been excluded. 13C NMR must be used to determine the M-centered triads and NM>1. This test method describes only the 1H NMR analysis of alginate. Alginate can be well characterized by determining FG and NG>1.4.3 In order to obtain well-resolved NMR spectra, it is necessary to reduce the viscosity and increase the mobility of the molecules by depolymerization of alginate to a degree of polymerization of about 20 to 50. Acid hydrolysis is used to depolymerize the alginate samples. Freeze-drying, followed by dissolution in 99 % D2O, and another freeze-drying before dissolution in 99.9 % D2O yields samples with low 1H2O content. TTHA is used as a chelator to prevent traces of divalent cations to interact with alginate. While TTHA is a more effective chelator, other agents such as EDTA and citrate may be used. Such interactions may lead to line broadening and selective loss of signal intensity.4.4 Samples are analyzed at a temperature of 80 ± 1°C. Elevated sample temperature contributes to reducing sample viscosity and repositions the proton signal of residual water to an area outside that of interest.1.1 This test method covers the determination of the composition and monomer sequence of alginate intended for use in biomedical and pharmaceutical applications as well as in Tissue Engineered Medical Products (TEMPs) by high-resolution proton NMR (1H NMR). A guide for the characterization of alginate has been published as Guide F2064.1.2 Alginate, a linear polymer composed of β-D-mannuronate (M) and its C-5 epimer α-L-guluronate (G) linked by β-(1—>4) glycosidic bonds, is characterized by calculating parameters such as mannuronate/guluronate (M/G) ratio, guluronic acid content (G-content), and average length of blocks of consecutive G monomers (that is, NG>1 ). Knowledge of these parameters is important for an understanding of the functionality of alginate in TEMP formulations and applications. This test method will assist end users in choosing the correct alginate for their particular application. Alginate may have utility as a scaffold or matrix material for TEMPs, in cell and tissue encapsulation applications, and in drug delivery formulations.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

定价： 0元 / 折扣价： 0 元

4.1 The degree of deacetylation of chitosan salts is an important characterization parameter since the charge density of the chitosan molecule is responsible for potential biological and functional effects.4.2 The degree of deacetylation (% DDA) of water-soluble chitosan salts can be determined by 1H nuclear magnetic resonance spectroscopy (1H NMR). Several workers have reported on the NMR determination of chemical composition and sequential arrangement of monomer units in chitin and chitosan. The test method described is primarily based on the work of Vårum et al. (1991),5 which represents the first publication on routine determination of chemical composition in chitosans by solution state 1H NMR spectroscopy. This test method is applicable for determining the % DDA of chitosan chloride and chitosan glutamate salts. It is a simple, rapid, and suitable method for routine use. Quantitative 1H NMR spectroscopy reports directly on the relative concentration of chemically distinct protons in the sample, consequently, no assumptions, calibration curves or calculations other than determination of relative signal intensity ratios are necessary.4.3 In order to obtain well-resolved NMR spectra, depolymerization of chitosans to a number average degree of polymerization (DPn) of ~15 to 30 is required. This reduces the viscosity and increases the mobility of the molecules. Although there are several options for depolymerization of chitosans, the most convenient procedure is that of nitrous acid degradation in deuterated water. The reaction is selective, stoichiometric with respect to GlcN, rapid, and easily controlled (Allan & Peyron, 1995).6 The reaction selectively cleaves after a GlcN-residue, transforming it into 2,5-anhydro-D-mannose (chitose), consequently, depletion of GlcN after depolymerization is expected. On the other hand, the chitose unit displays characteristic 1H NMR signals the intensity of which may be estimated and utilized in the calculation of % DDA, eliminating the need for correction factors. Using the intensity of the chitose signals, the number average degree of polymerization can easily be calculated as a control of the depolymerization.4.4 Samples are equilibrated and analyzed at a temperature of 90 ± 1°C. Elevated sample temperature contributes to reducing sample viscosity and repositions the proton signal of residual water to an area outside that of interest. While samples are not stored at 90°C but only analyzed at this elevated temperature, the NMR tubes should be sealed with a stopper to avoid any evaporation. At a sample pH* of 3.8-4.3 (see 6.1.5 below), artifactual deacetylation of the sample does not occur during the short equilibration and analysis time.4.5 A general description of NMR can be found in <761> of the USP 35-NF30.1.1 This test method covers the determination of the degree of deacetylation in chitosan and chitosan salts intended for use in biomedical and pharmaceutical applications as well as in Tissue Engineered Medical Products (TEMPs) by high-resolution proton NMR (1H NMR). A guide for the characterization of chitosan salts has been published as Guide F2103.1.2 The test method is applicable for determining the degree of deacetylation (% DDA) of chitosan chloride and chitosan glutamate salts and is valid for % DDA values from 50 up to and including 99. It is simple, rapid, and suitable for routine use. Knowledge of the degree of deacetylation is important for an understanding of the functionality of chitosan salts in TEMP formulations and applications. This test method will assist end users in choosing the correct chitosan for their particular application. Chitosan salts may have utility in drug delivery applications, as scaffold or matrix material, and in cell and tissue encapsulation applications.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价： 590元 / 折扣价： 502 元 加购物车

5.1 This test method was developed for evaluating the ac magnetic properties of laminated cores made from flat-rolled magnetic materials.5.2 The reproducibility and repeatability of this test method are such that this test method is suitable for design, specification acceptance, service evaluation, and research and development.1.1 This test method covers the determination of several ac magnetic properties of laminated cores made from flat-rolled magnetic materials.1.2 This test method covers test equipment and procedures for the determination of impedance permeability and exciting power from voltage and current measurements, and core loss from wattmeter measurements. These tests are made under conditions of sinusoidal flux.1.3 This test method covers tests for two general categories (1 and 2) of cores based on size and application.1.4 Tests are provided for power and control size cores (Category 1) operating at inductions of 10 to 15 kG [1.0 to 1.5 T] and at frequencies of 50, 60, and 400 Hz.1.5 Procedures and tests are provided for coupling and matching type transformer cores (Category 2) over the range of inductions from 100 G [0.01 T] or lower to 10 kG [1.0 T] and above at 50 to 60 Hz or above when covered by suitable procurement specifications.1.6 This test method also covers tests for core loss and ac impedance permeability under incremental test conditions (ac magnetization superimposed on dc magnetization) for the above core types and at inductions up to those that cause the ac exciting current to become excessively distorted or reach values that exceed the limits of the individual test equipment components.1.7 This test method shall be used in conjunction with Practice A34/A34M and Terminology A340. It depends upon these designated documents for detailed information which will not be repeated in this test method.1.8 The values and equations stated in customary (cgs-emu and inch-pound) or SI units are to be regarded separately as standard. Within this standard, SI units are shown in brackets. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with this standard.1.9 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.10 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价： 646元 / 折扣价： 550 元 加购物车

5.1 This test method provides an easy, accurate, and reproducible method for determination of shielding factors (attenuation ratios) in simple alternating magnetic fields.5.2 Since the sensing or pickup coil is of finite size, the measured shielding factor tends to be the average value for the space enclosed by the coil. Due care is required when interpreting results when the coil is located near an opening in the shield.5.3 This test method is suitable for design, specification acceptance, service evaluation, quality assurance, and research purposes on magnetic shields.5.4 Provided geometrically identical shields are compared, this test method is also suitable for evaluation and grading of magnetic shielding materials.1.1 This test method covers the means for determining the performance quality of a magnetic shield when placed in a magnetic field of alternating polarity.1.2 This test method provides a means of evaluating and grading magnetic shielding materials to determine their suitability for use in the production of magnetic shields.1.3 This test method shall be used in conjunction with and shall conform to the requirements of Practice A34/A34M.1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价： 590元 / 折扣价： 502 元 加购物车

4.1 This test method is suitable for magnet specification, acceptance, service evaluation, quality control in magnet production, research and development, and design.4.2 When a test specimen is cut or fabricated from a larger magnet, the magnetic properties measured on it are not necessarily exactly those of the original sample, even if the material is in the same condition. In such instances, the test results must be viewed in context of part performance history.4.3 Tests performed in general conformity to this test method and even on the same specimen, but using different test systems, may not yield identical results. The main source of discrepancies are variations between the different test systems in the geometry of the region surrounding the sample, such as, size and shape of the electromagnet pole caps (see Annex A1 and Appendix X1), air gaps at the specimen end faces, and especially the size and location of the measuring devices for H and B or for their corresponding flux values (Hall-effect probes, inductive sensing coils). Also important is the method of B calibration, for example, a volt-second calibration of the fluxmeter alone versus an overall system calibration using a physical reference sample. The method of B and H sensing should be indicated in test reports (see Section 9).1.1 This test method covers how to determine the magnetic characteristics of magnetically hard materials (permanent magnets), particularly their initial magnetization, demagnetization, and recoil curves, and such quantities as the residual induction, coercive field strength, knee field, energy product, and recoil permeability. This test method is suitable for all materials processed into bulk magnets by any common fabrication technique (casting, sintering, rolling, molding, and so forth), but not for thin films or for magnets that are very small or of unusual shape. Uniformity of composition, structure, and properties throughout the magnet volume is necessary to obtain repeatable results. Particular attention is paid to the problems posed by modern materials combining very high coercivity with high saturation induction, such as the rare-earth magnets, for which older test methods (see Test Method A341/A341M) are unsuitable. An applicable international standard is IEC Publication 60404-5.1.2 The magnetic system (circuit) in a device or machine generally comprises flux-conducting and nonmagnetic structural members with air gaps in addition to the permanent magnet. The system behavior depends on properties and geometry of all these components and on the operating temperature. This test method describes only how to measure the properties of the permanent magnet material. The basic test method incorporates the magnetic specimen in a magnetic circuit with a closed flux path. Test methods using ring samples or frames composed entirely of the magnetic material to be characterized, as commonly used for magnetically soft materials, are not applicable to permanent magnets.1.3 This test method shall be used in conjunction with Practice A34/A34M.1.4 The values and equations stated in customary (cgs-emu or inch-pound) or SI units are to be regarded separately as standard. Within this test method, SI units are shown in brackets except for the sections concerning calculations where there are separate sections for the respective unit systems. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with this test method.1.5 The names and symbols of magnetic quantities used in this test method, summarized in Table 1, are those generally accepted by the industry.1.6 This test method is useful for magnet materials having Hci values between about 100 Oe and 35 kOe [8 kA/m and 2.8 MA/m], and Br values in the approximate range from 500 G to 20 kG [50 mT to 2 T]. High-coercivity rare-earth magnet test specimens may require much higher magnetizing fields than iron-core electromagnets can produce. Such samples must be premagnetized externally and transferred into the measuring yoke. Typical values of the magnetizing fields, Hmag, required for saturating magnet materials are shown in Table A2.1.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价： 646元 / 折扣价： 550 元 加购物车

This test method is useful for measuring the wall thickness of plastic vessels and other plastic structures where the geometry of the equipment does not permit direct measurement by conventional methods, such as micrometers, calipers, and rulers. This test method is not limited to plastics and can be used for all nonmagnetic materials. It provides for a rapid and accurate thickness measurement, without the need for drilling and repair of holes.Accuracies are not affected by density variations, permitting the measurement of composites made up of a variety of materials of varying densities. By placement of the magnetic source on the mold surface, thickness measurements can be made during and after fabrication of plastic products to verify thickness and adherence to specifications.1.1 This test method covers the measurement of thickness of any nonmagnetic material by means of a digital magnetic intensity instrument.Note 1The instrument on which this test method is based is no longer sold or serviced.1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.1.2 There is no similar or equivalent ISO standard.

定价： 0元 / 折扣价： 0 元

This test method covers the procedures for the standard practice of performing magnetic particle examination of continuous grain flow crankshaft forgings intended for medium speed diesel engines. Crankshafts shall be divided into four zones of decreasing operational stress, each of which have been designated its own set of acceptance criteria. Zone 1, which consists of the major critical areas, includes the crankpin journals, main bearing journals, and oil holes. Zone 2, which consists of the minor critical areas, includes the balance of the fillet radii of the crankpin and main bearing journals not included in Zone 1. Zone 3, which comprises the journal running surfaces, includes the remainder of the crankpin and main bearing journal surfaces not covered by Zones 1 and 2. Finally, Zone 4 comprises all other remaining areas, including the crankpin web surfaces, and flange faces and periphery. Dimpling technique may be used to remove unwanted visual or magnetic particle indications.1.1 This specification covers the magnetic particle examination of forged continuous grain flow (CGF) crankshafts intended for medium speed diesel engines.1.2 For the purpose of magnetic particle indication assessment, the crankshaft is divided into four zones of decreasing operational stress. Acceptance criteria have been set for each zone.1.3 The engines to which these crankshafts are fitted are commonly used for diesel electric locomotives, marine propulsion, and power generation. Engines fueled by natural gas also fall into this medium speed category.1.4 Specification A983/A983M is a product specification that covers the manufacture of CGF crankshafts.1.5 The values stated in either inch-pound units or SI units are to be regarded separately as standard. Within the text, the SI units are shown in brackets. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价： 515元 / 折扣价： 438 元 加购物车

4.1 This test method is suitable for the measurement of the electrical resistivity of specimens of soft magnetic materials.4.2 The reproducibility and repeatability of this test method are such that it is suitable for design, specification acceptance, service evaluation, quality assurance, and research and development.1.1 This test method covers the measurement of electrical resistivity of strip or bar specimens of soft magnetic alloys.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价： 515元 / 折扣价： 438 元 加购物车

This specification deals with soft magnetic manganese zinc ferrite core materials for high frequency power transformer and filter inductor applications. Standard types of both power transformer and filter inductor material are defined. For power transformer use, there are five types defined by their maximum core loss density and minimum saturation flux density. For filter inductor materials, three types are defined based on their inductance permeability. Apart from magnetic property requirements, dimensional tolerances and workmanship requirements are defined in this specification.1.1 This specification covers the requirements to which the specified grades of soft magnetic manganese zinc (MnZn) ferrite materials shall conform. Cores made from these materials are used primarily in transformers and inductors.1.2 Frequency—MnZn ferrite cores are primarily used for frequencies in the range of 10 kHz to 1 MHz. Many inductors have a DC component as well.1.3 Magnetic Flux Density—Applications consist of two main categories, high and low magnetic flux density.1.3.1 High Magnetic Flux Density—Transformers used for power conversion. Inductors or chokes used in high current applications.1.3.2 Low Magnetic Flux Density—Transformers, inductors, chokes used for signal conditioning.1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to customary (cgs-emu and inch-pound) units, which are provided for information only and are not considered standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价： 515元 / 折扣价： 438 元 加购物车