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3.1 These test methods are intended mainly for referee purposes but may be used for quality control of masterbatch production. They may also be used in research and development work and for comparison of different rubber samples in a standard formula.3.2 These test methods may also be used to obtain values for customer acceptance of rubber.1.1 These test methods cover the standard materials, test formula, mixing procedures, and test methods for the evaluation and production control of pigmented types of styrene-butadiene rubbers (SBR). This includes the pigmented SBR oil masterbatches.1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM C1362-09 Standard Test Method for Flow of Freshly Mixed Hydraulic Cement Concrete (Withdrawn 2014) Withdrawn, No replacement 发布日期 :  1970-01-01 实施日期 : 

This test method permits a rapid assessment of the flow and consistency of freshly mixed concrete (see Note 1).This test method also provides information on the change in flow and consistency, with time, of concrete containing superplasticizer admixtures.This test method can be used to measure the uniformity characteristics of flow and consistency of freshly mixed concrete and its change with time.Note 1—This test method may not be appropriate for use in evaluating gap-graded aggregate concrete.1.1 This test method covers determination of the flow of a sample of freshly mixed concrete, either in the field or in the laboratory.1.2 This test method is applicable to concrete having coarse aggregate up to 37.5 mm in size. If the coarse aggregate is larger than 37.5 mm in size, the test method is applicable when the fraction of concrete larger than 37.5 mm is removed in accordance with Practice C 172.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 The text of this standard references notes and footnotes that provide explanatory information. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. (Warning—Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure. )

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3.1 This test method covers the determination of the air content of freshly mixed concrete. The test determines the air content of freshly mixed concrete exclusive of any air that may exist inside voids within aggregate particles. For this reason, it is applicable to concrete made with relatively dense aggregate particles and requires determination of the aggregate correction factor (see 6.1 and 9.1).3.2 This test method and Test Method C138/C138M and C173/C173M provide pressure, gravimetric, and volumetric procedures, respectively, for determining the air content of freshly mixed concrete. The pressure procedure of this test method gives substantially the same air contents as the other two test methods for concretes made with dense aggregates.3.3 The air content of hardened concrete may be either higher or lower than that determined by this test method. This depends upon the methods and amount of consolidation effort applied to the concrete from which the hardened concrete specimen is taken; uniformity and stability of the air bubbles in the fresh and hardened concrete; accuracy of the microscopic examination, if used; time of comparison; environmental exposure; stage in the delivery, placement and consolidation processes at which the air content of the unhardened concrete is determined, that is, before or after the concrete goes through a pump; and other factors.1.1 This test method covers determination of the air content of freshly mixed concrete from observation of the change in volume of concrete with a change in pressure.1.2 This test method is intended for use with concretes and mortars made with relatively dense aggregates for which the aggregate correction factor can be satisfactorily determined by the technique described in Section 6. It is not applicable to concretes made with lightweight aggregates, air-cooled blast-furnace slag, or aggregates of high porosity. In these cases, Test Method C173/C173M should be used. This test method is also not applicable to nonplastic concrete such as is commonly used in the manufacture of pipe and concrete masonry units.1.3 The text of this test method references notes and footnotes that provide explanatory information. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of this standard.1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. (Warning—Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure.2)1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D2901-99 Standard Test Method for Cement Content of Freshly Mixed Soil-Cement (Withdrawn 2006) Withdrawn, No replacement 发布日期 :  1970-01-01 实施日期 : 

1.1 This test method covers determination of the cement content of samples of freshly-mixed soil-cement. 1.2 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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5.1 This test method provides a procedure for determining the density and void content of freshly mixed pervious concrete.5.2 This test method is applicable to pervious concrete mixtures containing coarse aggregate with a nominal maximum size of 25 mm [1 in.] or smaller.5.3 The measured fresh density may be used as verification of mixture proportions.5.4 This method uses a standard consolidation procedure to measure fresh density and void content of a pervious concrete mixture as delivered. Test results are not intended to represent the density and void content of the in-place pervious concrete. This method shall not be used to determine the in-place void content or yield of the pervious concrete.5.5 The fresh density and void content calculated from this test method may be different when comparing the results from Procedure A with Procedure B. Results are only comparable when obtained using the same procedure (Procedure A or B).1.1 This test method covers determining the density of freshly mixed pervious concrete under standardized conditions and gives formulas for calculating the void content of pervious concrete. Test results are not intended to represent the in-place density and void content.1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. (Warning—Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure.2)1.4 The text of this test method references notes and footnotes that provide explanatory information. These notes and footnotes (excluding those in tables) shall not be considered as requirements of this test method.

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1.1 This practice describes a microwave oven practice used to dissolve glass samples that may contain nuclear wastes. The resulting solutions are then used to determine metals and radionuclides in support of glass vitrification plant operations and materials development programs. This practice can be used to dissolve production glass samples, vitrified melter feeds, and sludges.1.2 This practice is introduced to provide the user with an alternative means to Test Methods C 169 for dissolution of waste containing glass in shielded facilities. Test Methods C 169 is not practical for use in such facilities and with radioactive materials.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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ASTM C94/C94M-24 Standard Specification for Ready-Mixed Concrete Active 发布日期 :  1970-01-01 实施日期 : 

This specification covers ready-mixed concrete manufactured and delivered to a purchaser in freshly mixed and unhardened state as hereinafter specified. Requirements for quality of concrete shall be either as hereinafter specified or as specified by the purchase. In any case where the requirements of the purchaser differ from these in this specification, the purchaser's specification shall govern. In the absence of designated applicable materials specifications, materials specifications specified shall be used for cementitious materials, hydraulic cement, supplementary cementitious materials, cementitious concrete mixtures, aggregates, air-entraining admixtures, and chemical admixtures. Except as otherwise specifically permitted, cement, aggregate, and admixtures shall be measured by mass. Mixers will be stationary mixers or truck mixers. Agitators will be truck mixers or truck agitators. Test methods for compression, air content, slump, temperature shall be performed. For s strength test, at least two standard test specimens shall be made.1.1 This specification covers ready-mixed concrete as defined in 3.2.2 (Note 1). Requirements for quality of ready-mixed concrete shall be either as stated in this specification or as ordered by the purchaser. When the purchaser’s requirements, as stated in the order, differ from those in this specification, the purchaser’s requirements shall govern. This specification does not cover the placement, consolidation, curing, or protection of the concrete after delivery to the purchaser.NOTE 1: Concrete produced by volumetric batching and continuous mixing is covered in Specification C685/C685M. Fiber-reinforced concrete is covered in Specification C1116/C1116M.1.2 As used throughout this specification the producer manufactures ready-mixed concrete and the purchaser buys ready-mixed concrete.1.3 The values stated in either SI units, shown in brackets, or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.1.4 The text of this specification references notes and footnotes that provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the specification.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. (Warning—Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged use.2)1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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AbstractThese practices cover three standard technique for dissolving glass samples containing radioactive, nuclear, and mixed wastes. These techniques used together or independently will produce solutions that can be analyzed by inductively coupled plasma atomic emission spectroscopy (ICP-AES), inductively coupled plasma mass spectrometry (ICP-MS), atomic absorption spectrometry (AAS), radiochemical methods and wet chemical techniques for major components, minor components and radionuclides. The practices for dissolving silicate matrix samples each require the sample to be initially dried and ground to a fine powder. The first practice involves the mixing and fusion of the sample with sodium tetraborate (Na2B4O7) and sodium carbonate (Na2CO4) in a muffle for a given amount of time and temperature. The sample is then cooled, dissolved in hydrochloric acid, and diluted to appropriate volume for analyses. The second practice, on the other hand, involves the fusion of the sample with potassium hydroxide (KOH) or sodium peroxide (Na2O2) using an electric bunsen burner, dissolving the fused sample in water and dilute HCl, and making to volume for analyses. Finally, the third practice involves the dissolution of the sample using a microwave oven. The ground sample is digested in a microwave oven using a mixture of hydrofluoric (HF) and nitric (HNO3) acids. Boric acid is added to the resulting solution to complex excess fluoride ions.1.1 These practices cover techniques suitable for dissolving glass samples that may contain nuclear wastes. These techniques used together or independently will produce solutions that can be analyzed by inductively coupled plasma atomic emission spectroscopy (ICP-AES), inductively coupled plasma mass spectrometry (ICP-MS), atomic absorption spectrometry (AAS), radiochemical methods and wet chemical techniques for major components, minor components and radionuclides.1.2 One of the fusion practices and the microwave practice can be used in hot cells and shielded hoods after modification to meet local operational requirements.1.3 The user of these practices must follow radiation protection guidelines in place for their specific laboratories.1.4 Additional information relating to safety is included in the text.1.5 The dissolution techniques described in these practices can be used for quality control of the feed materials and the product of plants vitrifying nuclear waste materials in glass.1.6 These practices are introduced to provide the user with an alternative means to Test Methods C169 for dissolution of waste containing glass in shielded facilities. Test Methods C169 is not practical for use in such facilities and with radioactive materials.1.7 The ICP-AES methods in Test Methods C1109 and C1111 can be used to analyze the dissolved sample with additional sample preparation as necessary and with matrix effect considerations. Additional information as to other analytical methods can be found in Test Method C169.1.8 Solutions from this practice may be suitable for analysis using ICP-MS after establishing laboratory performance criteria and verification that the criteria can be met. For example, Test Methods C1287 or C1637 may be used with additional sample preparation as necessary and appropriate matrix effect considerations.1.9 The values stated in SI units are to be regarded as standard. Units in parentheses are for information only.1.10 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Sections 10, 20, and 30.1.11 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method is useful for determining the expansion and bleeding characteristics of freshly mixed fluid hydraulic cement grout commonly used in PA concrete and cementitious post-tensioning tendon grouts.

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ASTM C172/C172M-17 Standard Practice for Sampling Freshly Mixed Concrete Active 发布日期 :  1970-01-01 实施日期 : 

3.1 This practice is intended to provide standard requirements and procedures for sampling freshly mixed concrete from different containers used in the production or transportation of concrete. The detailed requirements as to materials, mixtures, air content, temperature, number of specimens, slump, interpretation of results, and precision and bias are in specific test methods.1.1 This practice covers procedures for obtaining representative samples of fresh concrete as delivered to the project site on which tests are to be performed to determine compliance with quality requirements of the specifications under which the concrete is furnished (Note 1). The practice includes sampling from stationary, paving and truck mixers, and from agitating and nonagitating equipment used to transport central-mixed concrete and from continuous mixing equipment as described in Specification C685/C685M.1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.NOTE 1: Composite samples are required by this practice, unless specifically excepted by procedures governing the tests to be performed such as tests to determine uniformity of consistency and mixer efficiency. Procedures used to select the specific test batches are not described in this practice, but it is recommended that random sampling be used to determine overall specification compliance.1.3 This practice also covers the procedures to be used for preparing a sample of concrete for further testing where it is desirable or necessary to remove the aggregate larger than a designated size. This removal of larger aggregate particles is preferably accomplished by wet-sieving.1.4 The text of this standard references notes and footnotes which provide explanatory material and shall not be considered as requirements of the practice.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. (Warning—Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure.2)1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test method covers the determination of the air content of freshly mixed concrete. It measures the air contained in the mortar fraction of the concrete, but is not affected by air that may be present inside porous aggregate particles.4.1.1 Therefore, this is the appropriate test to determine the air content of concretes containing lightweight aggregates, air-cooled slag, and highly porous or vesicular natural aggregates.4.2 This test method requires the addition of sufficient isopropyl alcohol, when the meter is initially being filled with water, so that after the first or subsequent rollings little or no foam collects in the neck of the top section of the meter. If more foam is present than that equivalent to 2 % air above the water level, the test is declared invalid and must be repeated using a larger quantity of alcohol. Addition of alcohol to dispel foam any time after the initial filling of the meter to the zero mark is not permitted.4.3 The air content of hardened concrete may be either higher or lower than that determined by this test method. This depends upon the methods and amounts of consolidation effort applied to the concrete from which the hardened concrete specimen is taken; uniformity and stability of the air bubbles in the fresh and hardened concrete; accuracy of the microscopic examination, if used; time of comparison; environmental exposure; stage in the delivery, placement and consolidation processes at which the air content of the unhardened concrete is determined, that is, before or after the concrete goes through a pump; and other factors.1.1 This test method covers determination of the air content of freshly mixed concrete containing any type of aggregate, whether it be dense, cellular, or lightweight.1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The inch-pound units are shown in brackets. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.1.3 The text of this standard references notes and footnotes that provide explanatory information. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. (Warning—Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure.2)1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification covers cold-mixed, cold-laid and recycled cold-mixed, cold-laid bituminous paving mixtures for base, binder, leveling, and surface courses. The following shall conform to the specified requirements: coarse and fine aggregates, mineral filler, bitumen, and composition of bituminous paving mixtures. The equipment for mixing shall be one of the following: central plant, travel plant, and grand or drag. The mixing operations are detailed and includes: (1) aggregate storage, (2) old bituminous pavement, (3) preparation of bitumen, (4) preparation and handling of mineral aggregates, (5) preparation and handling of bitumen aggregates for recycling, (6) preparation of mixture, and (7) mixing plant inspection. The tests methods that shall be used to determine the properties are sieve analysis of aggregates, sieve analysis of mineral filler, determination of bitumen content, specific gravity of coarse aggregate, specific gravity of coarse aggregate, plasticity index, and percentage of coated particles.1.1 This specification covers cold-mixed, cold-laid and recycled cold-mixed, cold-laid asphalt paving mixtures for base, binder, leveling, and surface courses.1.2 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Mixed oxide, a mixture of uranium and plutonium oxides, is used as a nuclear-reactor fuel in the form of pellets. The plutonium content may be up to 10 weight %, and the diluent uranium may be of any 235U enrichment. In order to be suitable for use as a nuclear fuel, the material must meet certain criteria for combined uranium and plutonium content, effective fissile content, and impurity content as described in Specification C833.4.1.1 The material is assayed for uranium and plutonium to determine whether the plutonium content is as specified by the purchaser, and whether the material contains the minimum combined uranium and plutonium contents specified on a dry weight basis.4.1.2 Determination of the isotopic content of the plutonium and uranium in the mixed oxide is made to establish whether the effective fissile content is in compliance with the purchaser's specifications.4.1.3 Impurity content is determined to ensure that the maximum concentration limit of certain impurity elements is not exceeded. Determination of impurities is also required for calculation of the equivalent boron content (EBC) as described in Practice C1233.4.2 Fitness for Purpose of Safeguards and Nuclear Safety Applications—Methods intended for use in safeguards and nuclear safety applications shall meet the requirements specified by Guide C1068 for use in such applications.1.1 These test methods cover procedures for the chemical, mass spectrometric, and spectrochemical analysis of nuclear-grade mixed oxides, (U, Pu)O2, powders and pellets to determine compliance with specifications.1.2 The analytical procedures appear in the following order:  SectionsUranium in the Presence of Pu by Potentiometric Titration   2Plutonium by Controlled-Potential Coulometry   2Plutonium by Amperometric Titration with Iron (II)   2Nitrogen by Distillation Spectrophotometry Using Nessler Reagent  8 to 15Carbon (Total) by Direct Combustion-Thermal Conductivity  16 to 26Total Chlorine and Fluorine by Pyrohydrolysis  27 to 34Sulfur by Distillation-Spectrophotometry  35 to 43Moisture by the Coulometric, Electrolytic Moisture Analyzer  44 to 51Isotopic Composition by Mass Spectrometry   3Rare Earths by Copper Spark Spectroscopy  52 to 59Trace Impurities by Carrier Distillation Spectroscopy  60 to 68Impurities by Spark-Source Mass Spectrography  69 to 75Total Gas in Reactor-Grade Mixed Dioxide Pellets    4Tungsten by Dithiol-Spectrophotometry  76 to 84Rare Earth Elements by Spectroscopy  85 to 88Plutonium-238 Isotopic Abundance by Alpha Spectrometry   5Americium-241 in Plutonium by Gamma-Ray SpectrometryUranium and Plutonium Isotopic Analysis by Mass Spectrometry  89 to 97Oxygen-to-Metal Atom Ratio by Gravimetry  98 to 1051.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. (For specific safety precaution statements, see Sections 6, 13.2.5, 41.7, and 93.6.1.)

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5.1 The aniline point (or mixed aniline point) is useful as an aid in the characterization of pure hydrocarbons and in the analysis of hydrocarbon mixtures. Aromatic hydrocarbons exhibit the lowest, and paraffins the highest values. Cycloparaffins and olefins exhibit values that lie between those for paraffins and aromatics. In homologous series the aniline points increase with increasing molecular weight. Although it occasionally is used in combination with other physical properties in correlative methods for hydrocarbon analysis, the aniline point is most often used to provide an estimate of the aromatic hydrocarbon content of mixtures.1.1 These test methods cover the determination of the aniline point of petroleum products and hydrocarbon solvents. Test Method A is suitable for transparent samples with an initial boiling point above room temperature and where the aniline point is below the bubble point and above the solidification point of the aniline-sample mixture. Test Method B, a thin-film method, is suitable for samples too dark for testing by Test Method A. Test Methods C and D are for samples that may vaporize appreciably at the aniline point. Test Method D is particularly suitable where only small quantities of sample are available. Test Method E describes a procedure using an automatic apparatus suitable for the range covered by Test Methods A and B.1.2 These test methods also cover the determination of the mixed aniline point of petroleum products and hydrocarbon solvents having aniline points below the temperature at which aniline will crystallize from the aniline-sample mixture.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 WARNING—Mercury has been designated by many regulatory agencies as a hazardous substance that can cause serious medical issues. Mercury, or its vapor, has been demonstrated to be hazardous to health and corrosive to materials. Use caution when handling mercury and mercury-containing products. See the applicable product Safety Data Sheet (SDS) for additional information. The potential exists that selling mercury or mercury-containing products, or both, is prohibited by local or national law. Users must determine legality of sales in their location.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific warning statements are given in Section 7.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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