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5.1 Two procedures, A and B, are outlined in this test method. Procedure A is used most often for development of various beverage container designs to determine the functional characteristics of the package in regard to shelf life. Procedure B is recommended for use in beverage filling operations as a quality control tool in maintaining the desired CO2 fill pressure. A loss of CO2 will affect product taste.5.1.1 Procedure A involves the use of sensitive pressure and temperature monitoring equipment where a high degree of accuracy is essential, for example, a micro-pressure transducer and thermocouple for measuring pressure and temperature of the package in a closed system. Alternatively, this procedure may also use bottles closed with roll-on aluminum caps containing rubber septums. The septum is pierced with a hypodermic needle attached to a pressure transducer to obtain pressure readings. This procedure should be confined to laboratories that are practiced in this type of analytical testing.5.1.2 Procedure B is more widely used when measuring the carbonation level of the package due to the simplicity of the technique. A simple Manual pressure assembly or an Automated CO2 Analyzer is utilized.1.1 The objective of this test method is to determine the carbon dioxide (CO2) loss from plastic beverage containers after a specified period of storage time.1.2 Factors contributing to this pressure loss are volume expansion and the gas transport characteristics of the package, including permeation and leakage.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D1509-18(2023) Standard Test Methods for Carbon Black—Heating Loss Active 发布日期 :  1970-01-01 实施日期 : 

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4.1 This test method is used to obtain the ignition loss of a cured reinforced resin sample.NOTE 2: The basic concept of burning off of the organic matrix of a reinforced polymer composite has also been shown to be a useful method for enabling a visual examination of the fiber architecture or laminate structure of some reinforcements.4.2 If only glass fabric or filament is used as the reinforcement of an organic resin that is completely decomposed to volatile materials under the conditions of this test and the small amount of volatiles (water, residual solvent) that are potentially present are ignored, the ignition loss shall be considered to be the resin content of the sample.4.2.1 This test method does not provide a measure of resin content for samples containing reinforcing materials that lose weight under the conditions of the test or containing resins or fillers that do not decompose to volatile materials released by ignition.1.1 This test method covers the determination of the ignition loss of cured reinforced resins. This ignition loss shall be considered to be the resin content within the limitations of 4.2.1.2 The values stated in SI units are to be regarded as the standard.1.3 This standard is used to measure and describe the response of composite material to heat under controlled conditions, but does not by itself incorporate all of the factors required for fire hazard or fire assessments of the composite materials under actual fire conditions.1.4 Fire testing is inherently hazardous. Adequate safeguards for personnel and property shall be employed in conducting these tests.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.NOTE 1: There is no known ISO equivalent to this standard.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The evaporation loss is of particular importance in engine lubrication. Where high temperatures occur, portions of an oil can evaporate.5.2 Evaporation may contribute to oil consumption in an engine and can lead to a change in the properties of an oil.5.3 Many engine manufacturers specify a maximum allowable evaporation loss.5.4 Some engine manufacturers, when specifying a maximum allowable evaporation loss, quote this test method along with the specifications.5.5 The apparatuses used in Procedure C (see Annex A2) and Procedure D, also permit collection of the volatile oil vapors for determination of their physical and chemical properties. Elemental analysis of the collected volatiles may be helpful in identifying components such as phosphorous, which has been linked to premature degradation of the emission system catalyst.1.1 This test method covers four procedures for determining the evaporation loss of lubricating oils (particularly engine oils). The evaporation measured is reported as percent total loss. The test method relates to one set of operating conditions but may be readily adapted to other conditions as required.1.2 Procedure B and Procedure D that are in the main section of the test method provide equivalent results. Procedures A and C, which are in Annex A1 and Annex A2, have equivalent results. It has been determined that Procedures A and C show a slight bias when compared to Procedures B and D. Procedures B and D give slightly higher results versus Procedures A and C on formulated engine oils, while Procedures B and D give lower results versus Procedures A and C on basestocks. Thus, a correction factor is utilized to convert between the two sets of Procedures based on the fluid type.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Manufacturers of thermal insulation express the performance of their products in charts and tables showing heat gain or loss per unit surface area or unit length of pipe. This data is presented for typical insulation thicknesses, operating temperatures, surface orientations (facing up, down, horizontal, vertical), and in the case of pipes, different pipe sizes. The exterior surface temperature of the insulation is often shown to provide information on personnel protection or surface condensation. However, additional information on effects of wind velocity, jacket emittance, ambient conditions and other influential parameters may also be required to properly select an insulation system. Due to the large number of combinations of size, temperature, humidity, thickness, jacket properties, surface emittance, orientation, and ambient conditions, it is not practical to publish data for each possible case, Refs (7,8).5.2 Users of thermal insulation faced with the problem of designing large thermal insulation systems encounter substantial engineering cost to obtain the required information. This cost can be substantially reduced by the use of accurate engineering data tables, or available computer analysis tools, or both. The use of this practice by both manufacturers and users of thermal insulation will provide standardized engineering data of sufficient accuracy for predicting thermal insulation system performance. However, it is important to note that the accuracy of results is extremely dependent on the accuracy of the input data. Certain applications may need specific data to produce meaningful results.5.3 The use of analysis procedures described in this practice can also apply to designed or existing systems. In the rectangular coordinate system, Practice C680 can be applied to heat flows normal to flat, horizontal or vertical surfaces for all types of enclosures, such as boilers, furnaces, refrigerated chambers and building envelopes. In the cylindrical coordinate system, Practice C680 can be applied to radial heat flows for all types of piping circuits. In the spherical coordinate system, Practice C680 can be applied to radial heat flows to or from stored fluids such as liquefied natural gas (LNG).5.4 Practice C680 is referenced for use with Guide C1055 and Practice C1057 for burn hazard evaluation for heated surfaces. Infrared inspection, in-situ heat flux measurements, or both are often used in conjunction with Practice C680 to evaluate insulation system performance and durability of operating systems. This type of analysis is often made prior to system upgrades or replacements.5.5 All porous and non-porous solids of natural or man-made origin have temperature dependent thermal conductivities. The change in thermal conductivity with temperature is different for different materials, and for operation at a relatively small temperature difference, an average thermal conductivity may suffice. Thermal insulating materials (k < 0.85 {Btu·in}/{h·ft 2·°F}) are porous solids where the heat transfer modes include conduction in series and parallel flow through the matrix of solid and gaseous portions, radiant heat exchange between the surfaces of the pores or interstices, as well as transmission through non-opaque surfaces, and to a lesser extent, convection within and between the gaseous portions. With the existence of radiation and convection modes of heat transfer, the measured value should be called apparent thermal conductivity as described in Terminology C168. The main reason for this is that the premise for pure heat conduction is no longer valid, because the other modes of heat transfer obey different laws. Also, phase change of a gas, liquid, or solid within a solid matrix or phase change by other mechanisms will provide abrupt changes in the temperature dependence of thermal conductivity. For example, the condensation of the gaseous portions of thermal insulation in extremely cold conditions will have an extremely influential effect on the apparent thermal conductivity of the insulation. With all of this considered, the use of a single value of thermal conductivity at an arithmetic mean temperature will provide less accurate predictions, especially when bridging temperature regions where strong temperature dependence occurs.5.6 The calculation of surface temperature and heat loss or gain of an insulated system is mathematically complex, and because of the iterative nature of the method, computers best handle the calculation. Computers are readily available to most producers and consumers of thermal insulation to permit the use of this practice.5.7 Computer programs are described in this practice as a guide for calculation of the heat loss or gain and surface temperatures of insulation systems. The range of application of these programs and the reliability of the output is a primary function of the range and quality of the input data. The programs are intended for use with an “interactive” terminal. Under this system, intermediate output guides the user to make programming adjustments to the input parameters as necessary. The computer controls the terminal interactively with program-generated instructions and questions, which prompts user response. This facilitates problem solution and increases the probability of successful computer runs.5.8 The user of this practice may wish to modify the data input and report sections of the computer programs presented in this practice to fit individual needs. Also, additional calculations may be desired to include other data such as system costs or economic thickness. No conflict exists with such modifications as long as the user verifies the modifications using a series of test cases that cover the range for which the new method is to be used. For each test case, the results for heat flow and surface temperature must be identical (within resolution of the method) to those obtained using the practice described herein.5.9 This practice has been prepared to provide input and output data that conforms to the system of units commonly used by United States industry. Although modification of the input/output routines could provide an SI equivalent of the heat flow results, no such “metric” equivalent is available for some portions of this practice. To date, there is no accepted system of metric dimensions for pipe and insulation systems for cylindrical shapes. The dimensions used in Europe are the SI equivalents of American sizes (based on Practice C585), and each has a different designation in each country. Therefore, no SI version of the practice has been prepared, because a standard SI equivalent of this practice would be complex. When an international standard for piping and insulation sizing occurs, this practice can be rewritten to meet those needs. In addition, it has been demonstrated that this practice can be used to calculate heat transfer for circumstances other than insulated systems; however, these calculations are beyond the scope of this practice.1.1 This practice provides the algorithms and calculation methodologies for predicting the heat loss or gain and surface temperatures of certain thermal insulation systems that can attain one dimensional, steady- or quasi-steady-state heat transfer conditions in field operations.1.2 This practice is based on the assumption that the thermal insulation systems can be well defined in rectangular, cylindrical or spherical coordinate systems and that the insulation systems are composed of homogeneous, uniformly dimensioned materials that reduce heat flow between two different temperature conditions.1.3 Qualified personnel familiar with insulation-systems design and analysis should resolve the applicability of the methodologies to real systems. The range and quality of the physical and thermal property data of the materials comprising the thermal insulation system limit the calculation accuracy. Persons using this practice must have a knowledge of the practical application of heat transfer theory relating to thermal insulation materials and systems.1.4 The computer program that can be generated from the algorithms and computational methodologies defined in this practice is described in Section 7 of this practice. The computer program is intended for flat slab, pipe and hollow sphere insulation systems.1.5 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 A radiation-hardness assurance program requires a methodology for relating radiation-induced changes in materials exposed to a variety of particle species over a wide range of energies, including those encountered in spacecraft and in terrestrial environments as well as those produced by particle accelerators and nuclear fission and fusion reactors.4.2 A major source of radiation damage in electronic and photonic devices and materials is the displacement of atoms from their normal lattice site. An appropriate exposure parameter for such damage is the damage energy calculated from NIEL by means of Eq 2. Other analogous measures, which may be used to characterize the irradiation history that is relevant to displacement damage, are damage energy per atom or per unit mass (displacement kerma, when the primary particles are neutral), and displacements per atom (dpa). See Terminology E170 for definitions of those quantities.4.3 Each of the quantities mentioned in the previous paragraph should convey similar information, but in a different format. In each case the value of the derived exposure parameter depends on approximate nuclear, atomic, and lattice models, and on measured or calculated cross sections. If consistent comparisons are to be made of irradiation effects caused by different particle species and energies, it is essential that these approximations be consistently applied.4.4 No correspondence should be assumed to exist between damage energy as calculated from NIEL and a particular change in a material property or device parameter. Instead, the damage energy should be used as a parameter which describes the exposure. It may be a useful correlation variate, even when different particle species and energies are included. NIEL should not be reported as a measure of damage, however, unless its correlation with a particular damage modality has been demonstrated in that material or device.4.5 NIEL is a construct that depends on a model of the particle interaction processes in a material, as well as the cross section for each type of interaction. It is essential, when using NIEL as a correlation parameter, to ensure that consistent modeling parameters and nuclear data are used to calculate the NIEL value for each irradiation.4.6 Damage energy deposited in materials can be calculated directly, without the use of NIEL, using the Monte Carlo codes mentioned in 3.2.4.7, if all the particles involved in atomic displacement are tracked. The utility of the NIEL concept arises in cases where some particles, especially recoiling heavy ions, do not need to be tracked. In the NIEL representation, these are treated instead by means of infinite homogeneous medium solutions of the type originated by Lindhard et al. (10).1.1 This practice describes a procedure for characterizing particle irradiations of materials in terms of non-ionizing energy loss (NIEL). NIEL is used in published literature to characterize both charged and neutral particle irradiations.1.2 Although the methods described in this practice apply to any particles and target materials for which displacement cross sections are known (see Practice E521), this practice is intended for use in irradiations in which observed damage effects may be correlated with atomic displacements. This is true of some, but not all, radiation effects in electronic and photonic materials.1.3 Procedures analogous to this one are used for calculation of displacements per atom (dpa) in charged particle irradiations (see Practice E521) or neutron irradiations (see Practice E693).1.4 Guidance on calculation of dpa from NIEL is provided.1.5 Procedures related to this one are used for calculation of 1-MeV equivalent neutron fluence in electronic materials (see Practice E722), but in that practice the concept of damage efficiency, based on correlation of observed damage effects, is included.1.6 Guidance on conversion of NIEL in silicon to monoenergetic neutron fluence in silicon (see Practice E722), and vice versa, is provided.1.7 The application of this standard requires knowledge of the particle fluence and energy distribution of particles whose interaction leads to displacement damage.1.8 The correlation of radiation effects data is beyond the scope of this standard. A comprehensive review (1)2 of displacement damage effects in silicon and their correlation with NIEL provides appropriate guidance that is applicable to semiconductor materials and electronic devices.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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2.1 Weight loss represents the amount of combustibles and volatiles of the material at various temperatures between 315°C (600°F) and 815°C (1499°F). This procedure should not be used to determine percent of binder content.1.1 This test method covers the determination of gasket material weight loss upon exposure to elevated temperatures.1.2 This test method may include hazardous materials, operations, and equipment.1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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The calculated cost of property loss and destruction in combination with the cost of overages presents a logical foundation for the development of alternative models which can be used to evaluate the effectiveness of property management systems and provide relevant information to management useful for the distribution of resources to the task of property utilization and control.The understanding of an organization’loss, destruction and overage cost of inventory is a necessary prerequisite to the development of cost effective systems for the management of movable, durable assets.The costing model used in this standard assumes that individual categories of property represent a range of realized costs to an organization and that these loss or destruction costs can range from significant to minimal.The use of overage is a necessary corollary to the model since there can be significant costs associated with the inventory and control of unneeded assets.1.1 This practice covers the assignment of a value to categories and complete populations of lost or destroyed property assets for the purpose of determining the composite cost of all such losses on a periodic basis. This practice does not address the valuation of individual property assets.1.2 The reason for assigning a loss or destruction value is to establish an economic basis for the allocation of resources to manage property efficiently and in a cost effective manner.1.3 The direct cost of lost, damaged or destroyed (LDD) property has little to do with the acquisition, book or market value of such assets. While in many organizations, the value of LDD property is reflected at acquisition cost in the General Ledger accounts this approach is only appropriate for the financial reporting of property assets.1.4 The calculation of the cost of loss or destruction of property for the purposes of computing a necessary factor to be used in the equation applied under Practice E 2219 is to be based upon the consideration of both the risk of an inventory shortage as well as the benefits of inventory control and overage management.1.5 The valuation of property for the purposes of management and control is to be based upon the consideration of both the risk of an inventory shortage and benefits of inventory management as contained in this standard.

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5.1 Manufacturers of radiant barriers express the performance of their products in terms of the total hemispherical emittance. The purpose of a radiant barrier is to decrease the radiation heat transfer across the attic air space, and hence, to decrease the heat loss or gain through the ceiling below the attic. The amount of decrease in heat flow will depend upon a number of factors, such as weather conditions, amount of mass or reflective insulation in the attic, solar absorptance of the roof, geometry of the attic and roof, and amount and type of attic ventilation. Because of the infinite combinations of these factors, it is not practical to publish data for each possible case.5.2 The calculation of heat loss or gain of a system containing radiant barriers is mathematically complex, and because of the iterative nature of the method, it is best handled by computers.5.3 Computers are now widely available to most producers and consumers of radiant barriers to permit the use of this practice.5.4 The user of this practice may wish to modify the data input to represent accurately the structure. The computer program also may be modified to meet individual needs. Also, additional calculations may be desired, for example, to sum the hourly heat flows in some fashion to obtain estimates of seasonal or annual energy usages. This might be done using the hourly data as inputs to a whole-house model, and by choosing house balance points to use as cutoff points in the summations.1.1 This practice covers the estimation of heat gain or loss through ceilings under attics containing radiant barriers by use of a computer program. The computer program included as an adjunct to this practice provides a calculational procedure for estimating the heat loss or gain through the ceiling under an attic containing a truss or rafter mounted radiant barrier. The program also is applicable to the estimation of heat loss or gain through ceilings under an attic without a radiant barrier. This procedure utilizes hour-by-hour weather data to estimate the hour-by-hour ceiling heat flows. The interior of the house below the ceiling is assumed to be maintained at a constant temperature. At present, the procedure is applicable to sloped-roof attics with rectangular floor plans having an unshaded gabled roof and a horizontal ceiling. It is not applicable to structures with flat roofs, vaulted ceilings, or cathedral ceilings. The calculational accuracy also is limited by the quality of physical property data for the construction materials, principally the insulation and the radiant barrier, and by the quality of the weather data.1.2 Under some circumstances, interactions between radiant barriers and HVAC ducts in attics can have a significant effect on the thermal performance of a building. Ducts are included in an extension of the computer model given in the appendix.1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test method provides a quantitative measure of the susceptibility to intergranular corrosion of Al-Mg and Al-Mg-Mn alloys. The nitric acid dissolves a second phase, an aluminum-magnesium intermetallic compound (βAl-Mg), in preference to the solid solution of magnesium in the aluminum matrix. When this compound is precipitated in a relatively continuous network along grain boundaries, the effect of the preferential attack is to corrode around the grains, causing them to fall away from the specimens. Such dropping out of the grains causes relatively large mass losses of the order of 25 mg/cm2 to 75 mg/cm2 (160 mg/in.2 to 480 mg/in.2), whereas, samples of intergranular-resistant materials lose only about 1 mg/cm2 to 15 mg/cm2 (10 mg/in.2 to 100 mg/in.2). When the βAl-Mg compound is randomly distributed, the preferential attack can result in intermediate mass losses. Metallographic examination is required in such cases to establish whether or not the loss in mass is the result of intergranular attack.4.2 The precipitation of the second phase in the grain boundaries also gives rise to intergranular corrosion when the material is exposed to chloride-containing natural environments, such as seacoast atmospheres or sea water. The extent to which the alloy will be susceptible to intergranular corrosion depends upon the degree of precipitate continuity in the grain boundaries. Visible manifestations of the attack may be in various forms such as pitting, exfoliation, or stress-corrosion cracking, depending upon the morphology of the grain structure and the presence of sustained tensile stress.31.1 This test method, also known as the Nitric Acid Mass Loss Test (NAMLT), covers a procedure for constant immersion intergranular corrosion testing of 5XXX series aluminum alloys.1.2 This test method is applicable only to wrought products.1.3 This test method covers type of specimen, specimen preparation, test environment, and method of exposure.1.4 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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