5.1 A large number of industrial processes involve transfer and feeding of bulk solids, and the ability of such materials to flow in a controlled manner during these operations is critical to product quality.5.2 Direct shear cells are among the most important methods for measuring the flow properties of bulk solids in industrial applications for bulk solids handling.5.3 Direct shear cells have many advantages over simpler methods of measuring bulk solids flow properties, but their operation is more complex and the procedures for their use must be carefully controlled to produce accurate and reproducible data.5.4 The three most popular direct shear cell types are: Translational (D6128), Annular (D6773), and Rotational (D6682 and D7891).5.5 From shear cell data, a wide variety of parameters can be obtained, including the yield locus representing the shear stress to normal stress relationship at incipient flow, angle of internal friction, unconfined yield strength, cohesion, and a variety of related parameters such as the flow function.5.6 In addition, these three direct shear cells can be set up with wall coupons to measure wall friction.5.7 When the shear cell data are combined with unconfined yield strength, wall friction data, and bulk density data, they can be used for bin and hopper evaluation and design.1.1 This guide covers theory and principles for obtaining reliable and accurate bulk solids flow data using a direct shear cell. It includes characteristics and limitations of the three most popular direct shear cell types: Translational (D6128), Annular (D6773), and Rotational (D6682 and D7891).1.2 Units—The values stated in SI units are to be regarded as standard. No other units of measure are included in this standard.1.3 This guide offers an organized collection of information or a series of options and does not recommend a specific course of action. This document cannot replace education or experience and should be used in conjunction with professional judgment. Not all aspects of this guide may be applicable in all circumstances. This ASTM standard is not intended to represent or replace the standard of care by which the adequacy of a given professional service must be judged, nor should this document be applied without consideration of a project’s many unique aspects. The word “Standard” in the title of this document means only that the document has been approved through the ASTM consensus process.1.4 This guide offers an organized collection of information or a series of options and does not recommend a specific course of action. This document cannot replace education or experience and should be used in conjunction with professional judgment. Not all aspects of this guide may be applicable in all circumstances. This ASTM standard is not intended to represent or replace the standard of care by which the adequacy of a given professional service must be judged, nor should this document be applied without consideration of a project’s many unique aspects. The word “Standard” in the title of this document means only that the document has been approved through the ASTM consensus process.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Test methods A and B are used to estimate the permanganate natural oxidant demand exerted by the soil or aquifer solids by determining the quantity of potassium permanganate that is consumed by naturally occurring species as a function of time. Test Method C is used to estimate the permanganate total oxidant demand exerted by soil, aquifer solids, chemical contaminants or any other reduced species by determining the quantity of potassium permanganate that is consumed by all components of the bulk aquifer as a function of time. Typically, the measurement of oxidant demand is used to screen potential sites for in situ chemical oxidation (ISCO) with permanganate (Test Methods A and C) and provide information to aid in the design of remediation systems (Test Methods B and C).5.2 While some oxidizable species react relatively quickly (that is, days to weeks), others react more slower (weeks to months). Consequently, the PNODt is expected to be some fraction of the PNODmax.5.3 For ISCO injection applications, the PNOD may overestimate the demand exerted due to mass transport related issues. For soil blending applications, the PNOD is a more accurate measure of the demand exerted due to better mass to oxidant contact.NOTE 1: The quality of the result produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/and so forth.1.1 These test methods cover the estimation of the permanganate natural oxidant demand (PNOD) through the determination of the quantity of potassium permanganate (KMnO4) that organic matter and other naturally occurring oxidizable species present in soil or aquifer solids will consume under specified conditions as a function of time. Oxidizable species may include organic constituents and oxidizable inorganic ions, such as ferrous iron and sulfides. The following test methods are included:Test Method A—48-hour Permanganate Natural Oxidant DemandTest Method B—Permanganate Natural Oxidant Demand KineticsTest Method C—Permanganate Total Oxidant Demand1.2 These test methods are limited by the reagents employed to a permanganate natural oxidant demand (PNOD) of 40 g KMnO4 per kg soil or aquifer solids after a period of 48 hours (Methods A and C) or two weeks (Method B).1.3 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.1.4 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to interpret the results of the data. It is the responsibility of the user of this standard to interpret the results obtained and to determine the applicability of these results prior to use.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 These procedures can be used to generate microplastic particles as a simulation of microplastic particles found in the natural environment. Suitable uses may include evaluation of microplastic detection and imaging methods. Use of reference samples will support estimation of ambient and flux concentrations in drinking water, wastewater and natural environments, investigations of microplastic particle degradation, and ingestion of microplastics by animals in the contexts of food safety and human health risk assessment.1.1 This practice describes manufacturing methods to create microplastic particles from pellets of common polymers and the preparation of microplastic reference samples for calibration and proficiency evaluation of microplastic collection practices, preparation practices, and identification methods.1.2 This practice does not describe methods for controlling or characterizing the shapes of particles. The procedures have been observed to yield irregularly shaped particles, the use of which in many cases will serve to remove the analytical bias inherent with using distinctive manufactured spherical beads. Other procedures should be used if spheres or elongated fibers are desired.1.3 This practice does not describe handling procedures for waste generated when executing the procedures described herein. It is the responsibility of the user of this practice to follow applicable laws and regulations when manufacturing and disposing of microplastic particles, and to establish appropriate procedures to minimize the amount of waste generated.1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test method is used to determine the solids content of mixing water used to produce concrete when one or more of the water sources is wash water from concrete production operations or water that contains solids when batched as mixing water in concrete.4.2 The test method provides a means to determine the relationship between the density and solids content of water for compliance with solids content limits of mixing water such as in Specification C1602/C1602M.4.3 During production of concrete, the water property measured is its density, which can then be used to estimate the solids content from procedures described in this test method.4.4 To develop a correlation between the density and solids content of water, water samples should be tested that cover the range of solids concentrations anticipated during production.1.1 This test method covers the measurement of the solids content in water for use as mixing water in ready-mixed concrete and the measurement of its density. Solids content is expressed in terms of parts per million (ppm) or in terms of percent by mass of the water sample.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 The text of this standard references notes and footnotes that provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test method is useful in determining the total solids and water in analytical solutions.1.1 This test method is intended for use in determining the total solids and water in extracts of vegetable tanning materials. The test method is applicable to solutions of liquid, solid, pasty, and powdered extracts, and to extracts of raw or spent materials.1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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2.1 This test method is intended for use in determining the total solids content and the ash content of a finishing material before its use on any leather.1.1 This test method covers the total solids and ash content of finishing materials.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This practice is intended for use in collecting samples of consolidated or compacted materials from drums or similar containers, but only in compliance with a suitable work plan prepared according to Practice D5283 and Guide D4687. If the plan so provides, samples may be collected from drums not intended to be opened and from drums that are unstable, ruptured or otherwise compromised. Special handling procedures (for example, remote drum opening, overpressurized drum opening, drum deheading, etc.) are described in Drum Handling Practices at Hazardous Waste Sites.1.1 This practice covers typical equipment and methods for collecting samples of consolidated solids in drums or similar containers. These methods are adapted specifically for sampling drums having a volume of 110 U.S. gal (416 L) or less. These methods are applicable to hazardous material, product, or waste. Specific sample collection and handling requirements should be described in the site-specific work plan.1.2 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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5.1 This practice is intended for use in collecting samples of unconsolidated solid materials from drums or similar containers, including those that are unstable, ruptured, or compromised otherwise. Special handling procedures (for example, remote drum opening, overpressurized drum opening, drum deheading, etc.) are described in EPA/600/2-86/013, Drum Handling Practices at Hazardous Waste Sites.1.1 This practice covers typical equipment and methods for collecting samples of unconsolidated solids in drums or similar containers. These methods are adapted specifically for sampling drums having a volume of 110 U.S. gal (416 L) or less. These methods are applicable to hazardous material, product, or waste. Specific sample collection and handling requirements should be described in the site-specific work plan.1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Most organic liquids and solids will ignite in a pressurized oxidizing gas atmosphere if heated to a sufficiently high temperature and pressure. This procedure provides a numerical value for the temperature at the onset of ignition under carefully controlled conditions. Means for extrapolation from this idealized situation to the description, appraisal, or regulation of fire and explosion hazards in specific field situations, are not established. Ranking of the ignition temperatures of several materials in the standard apparatus is generally in conformity with field experience.4.2 The temperature at which material will ignite spontaneously (AIT) will vary greatly with the geometry of the test system and the rate of heating. To achieve good interlaboratory agreement of ignition temperatures, it is necessary to use equipment of approximately the dimensions described in the test method. It is also necessary to follow the described procedure as closely as possible.4.3 The decomposition and oxidation of some fully fluorinated materials releases so little energy that there is no clear-cut indication of ignition. Nor will there be a clear indication of ignition if a sample volatilizes, distilling to another part of the reaction vessel, before reaching ignition temperature.1.1 This test method covers the determination of the temperature at which liquids and solids will spontaneously ignite. These materials must ignite without application of spark or flame in a high-pressure oxygen-enriched environment.1.2 This test method is intended for use at pressures of 2.1 MPa to 20.7 MPa [300 psi to 3000 psi]. The pressure used in the description of the method is 10.3 MPa [1500 psi], and is intended for applicability to high pressure conditions. The test method, as described, is for liquids or solids with ignition temperature in the range from 60 °C to 500 °C [140 °F to 932 °F].NOTE 1: Test Method G72/G72M normally utilizes samples of approximately 0.20 ± 0.03-g mass, a starting pressure of 10.3 MPa [1500 psi] and a temperature ramp rate of 5 °C/min. However, Autogenous Ignition Temperatures (AIT) can also be obtained under other test conditions. Testing experience has shown that AIT testing of volatile liquids can be influenced by the sample pre-conditioning and the sample mass. This will be addressed in the standard as Special Case 1 in subsection 8.2.2. Testing experience has also shown that AIT testing of solid or non-volatile liquid materials at low pressures (that is, < 2.1 MPa) can be significantly influenced by the sample mass and the temperature ramp rate. This will be addressed in the standard as Special Case 2, in subsection 8.2.3. Since the AIT of a material is dependent on the sample mass/configuration and test conditions, any departure from the standard conditions normally used for Test Method G72/G72M testing should be clearly indicated in the test report.1.3 This test method is for high-pressure pure oxygen. The test method may be used in atmospheres from 0.5 % to 100 % oxygen.1.4 An apparatus suitable for these requirements is described. This test method could be applied to higher pressures and materials of higher ignition temperature. If more severe requirements or other oxidizers than those described are desired, care must be taken in selecting an alternative safe apparatus capable of withstanding the conditions.1.5 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Reliable, controlled flow of bulk solids from bins and hoppers is essential in almost every industrial facility. Unfortunately, flow stoppages due to arching and ratholing are common. Additional problems include uncontrolled flow (flooding) of powders, segregation of particle mixtures, usable capacity which is significantly less than design capacity, caking and spoilage of bulk solids in stagnant zones, and structural failures.5.2 By measuring the flow properties of bulk solids, and designing bins and hoppers based on these flow properties, most flow problems can be prevented or eliminated (1).35.3 For bulk solids with a significant percentage of particles (typically, one third or more) finer than about 6 mm (1/4 in.), the unconfined yield strength is governed by the fines (−6 mm fraction). For such bulk solids, strength and wall friction tests may be performed on the fine fraction only.NOTE 1: The quality of the result produced by this standard is dependent on the competence of personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself ensure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors. Practice D3740 was developed for agencies engaged in the testing or inspection (or both) of soil and rock. As such it is not totally applicable to agencies performing this standard. However, users of this standard should recognize that the framework of Practice D3740 is appropriate for evaluating the quality of an agency performing this standard. Currently there is no known qualifying national authority that inspects agencies that perform this standard.1.1 This test method covers the apparatus and procedures for measuring the unconfined yield strength of bulk solids during both continuous flow and after storage at rest. In addition, measurements of internal friction, bulk density, and wall friction on various wall surfaces are included.1.2 This test method covers operation of the manually-controlled Schulze Ring Shear Tester. An automated version of this tester is also available. Its method of testing bulk solids is similar in principle to that described in this test method.1.3 The most common use of this information is in the design of storage bins and hoppers to prevent flow stoppages due to arching and ratholing, including the slope and smoothness of hopper walls to provide mass flow. Parameters for structural design of such equipment may also be derived from this data. Another application is the measurement of the flowability of bulk solids, for example, for comparison of different products or optimization.1.4 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.1.4.1 The procedures used to specify how data are collected/recorded or calculated in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives: and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analysis methods for engineering design.1.5 Units—The values stated in SI units are to be regarded as standard. No other units of measure are included in this standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method may be used as an aid to design geotextile container systems that contain fine-grained, high water content slurries such as dredged materials to meet special environmental or operational requirements. This test is often used to demonstrate the efficacy of geotextile dewatering to regulatory agencies in determining the amount of dredged material sediment passing through a geotextile and the flow rate for specific high water content materials.5.2 The designer can use this test method to assess the quantity of fine-grained dredged material sediment that may pass through the geotextile container into the environment.5.3 This test method is intended for evaluation of a specific material, as the results will depend on the specific high water content slurry and geotextile evaluated and the location of the geotextile container below or above water. It is recommended that the user or a design representative perform the test because geotextile manufacturers are not typically equipped to handle or test fine-grained slurries.5.4 This test method provides a means of evaluating geotextile containers with different dredged materials or high water content materials under various conditions. The number of times this test is repeated depends on the users and the test conditions.5.5 This test method may not simulate site conditions and the user is cautioned to carefully evaluate how the results are applied.1.1 This test method is used to determine the flow rate of water and suspended solids through a geosynthetic permeable closed bag used to contain high water content slurry such as dredged material.1.2 The results for the water and sediment that pass through the geotextile bag are shown as liters of water per time period, and the percent total suspended solids in milligrams per liter or parts per million.1.3 The flow rate is the average rate of passage of a quantity of solids and water through the bag over a specific time period.1.4 This test method requires several pieces of specified equipment such as an integrated water sampler, analytical balance, geotextile bag, stand clear PVC pipes, testing frame, and clean containers to collect the decant water and a representative sample of high water content material from the proposed dredge area or slurry source.1.5 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Moisture is a ubiquitous and variable component of any biomass sample. Moisture is not considered a structural component of biomass and can change with storage and handling of biomass samples. The determination of the total solids content allows for the correction of biomass samples to an oven-dried solids mass that is constant for a particular sample.4.2 This procedure is not suitable for biomass samples that visibly change on heating to 105 °C, for example, unwashed acid-pretreated biomass still containing free acid.4.3 Some materials that contain large amount of free sugars or proteins will caramelize or brown under direct infrared heating elements used in Test Method B. Total solids in these materials should be done by Test Method A.1.1 This test method covers the determination of the amount of total solids remaining after drying a sample. Materials suitable for this procedure include samples prepared in accordance with Practice E1757 and extractive-free material prepared in accordance with Test Method E1690. For particulate wood fuels, Test Method E871 should be used.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Designers and installers of waterproofing systems may consult this guide for a discussion of important elements of the use of cold liquid-applied waterproofing membranes and associated elements of construction. This guide is not intended to serve as a specification for waterproofing installation.4.2 Long-term performance of waterproofing with a separate wearing course is important because of the substantial difficulty in determining the location of leakage and in removing overlying materials to make repairs.4.3 Refer to Guide C1471/C1471M for application on below grade walls and vertical surfaces.1.1 This guide describes the use of a high solids content, cold liquid-applied elastomeric waterproofing membrane that meets the criteria in Specification C836/C836M, in a waterproofing system subject to hydrostatic pressure for building decks over occupied space where the membrane is covered with a separate protective wearing course.1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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