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5.1 This practice is intended for use in collecting samples of single and multilayered liquids, with or without solids, from drums or similar containers, including those that are unstable, ruptured, or otherwise compromised. Special handling procedures (for example, remote drum opening, over-pressurized drum opening, drum deheading, etc.) are described in Drum Handling Practices at Hazardous Waste Sites.1.1 This practice covers typical equipment and methods for collecting samples of single or multilayered liquids, with or without solids, in drums or similar containers. These methods are adapted specifically for sampling drums having a volume of 110 gal (416 L) or less. These methods are applicable to hazardous material, product, or waste. Specific sample collection and handling requirements should be described in the site-specific work plan.1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in 7.2.4, 7.2.7.1, and Notes 1 and 2.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Many microplastic particles enter the environment, including ambient waters and drinking water supplies, via wastewater sources resulting from both industrial processes and consumer products. The presence of high percentages of organic particles, including cellulose material originating from toilet paper and chitin-based materials originating from insect exoskeletons, makes visual identification and subsequent quantification of microplastic particles in wastewater difficult.5.2 This test method, associated sampling Practice D8332, and preparation Practice D8333 provide a standardized approach for the preparation of water and, particularly, wastewater samples. The isolation of microplastic particles from interfering contaminants by Practice D8333 enables positive identification and, therefore, quantification of microplastic particles.5.3 Using this test method, microplastic particles are characterized in terms of size, shape, and quantity, allowing for the enumeration of subsequent particle count for a given volume of sample. The method does not provide qualitative identification of plastic composition.1.1 This test method covers the determination of microplastic particle size distribution, shape characterization, and number concentration (particle counts) in sample extracts containing particles between 5 µm and 100 µm. Light is transmitted through a flow cell containing particles in liquid medium. The particles create shadows as they pass through the field of vision of a camera, producing a multitude of images. The images are then used to measure size, shape, and concentration.1.2 This test method is used as a complementary technique for microplastic particle and fiber polymer identification methods infrared microscopy and gas chromatography/mass spectroscopy pyrolysis.1.3 This test method requires that samples are collected according to Practice D8332 and prepared according to Practice D8333 prior to use.1.4 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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2.1 Nonvolatile matter determination is useful as a quality control test, when used in conjunction with other tests, to assure specification compliance.1.1 This test method covers the determination of nonvolatile matter (total solids) in a water-emulsion, organic solvent-based liquid and paste floor polishes, and polymer-emulsion-type floor polishes.1.2 This test method recognizes that the products may contain material that will slowly volatilize or change chemically with a resulting change in weight of the nonvolatile matter. Therefore, since drying to constant weight is impractical, specific drying times have been selected.1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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The spontaneous heating value of a substance is a measure of the ability of that substance to undergo self-heating reactions while supported by cellulosic or other fibrous material in air. It is an index of the autoignition tendency of the substance under such conditions.1.1 This test method covers the non-adiabatic determination of the spontaneous heating values (SHV) of liquids and solids. It is applicable to substances that are not completely volatile at the test temperature. Spontaneous heating values obtained by this test method are qualitative indications of the degree of self-heating that may be expected to occur upon exposure of the sample to air at the test temperature.1.2 Values obtained by this method are applicable to liquids and solids supported on cellulosic surfaces. They are not applicable to liquids on metal surfaces, on contaminated surfaces, or at pressures above atmospheric.1.3 Spontaneous heating values determined by the present test method are regarded only as qualitative measurements of self-heating which occurs under the conditions of the test. The test method does not purport to produce a quantitative measure of the enthalpy of reaction of the sample with air at a given test temperature. Such data can be obtained by the use of an adiabatic calorimeter. The existence, under the test conditions, of a positive temperature difference between the sample and the reference is evidence of a thermochemical reaction in the sample.1.4 The magnitude of the measured temperature difference is a semiquantitative indication of the enthalpy and rate of that reaction. Since factors such as heat loss from the sample to the bath and quenching of the reaction due to too rapid consumption of oxygen affect the amount and duration of the measured heat effect, care must be taken not to attribute too much quantitative significance to the test results. It is sufficient, for the purpose of this test, to determine whether or not the sample is capable of undergoing a self-heating reaction of sufficient magnitude and rapidity to produce a detectable thermal effect. The spontaneous heating value (SHV) can be lower than the test temperature. A negative result does not preclude spontaneous heating initiating at a temperature higher than the test temperature.1.5 This standard should be used to measure and describe the response of materials, products, or assemblies to heat and flame under controlled conditions and should not be used to describe or appraise the fire-hazard or fire-risk of materials, products, or assemblies under actual fire conditions. However, results of this test may be used as elements of a fire-hazard assessment or a fire-risk assessment which takes into account all of the factors which are pertinent to an assessment of the fire hazard or fire risk of a particular end use.1.6 The values stated in SI units are to be regarded as the standard. In cases where materials, products or equipment are available in inch-pound units only, SI units are omitted.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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4.1 Solids (nonvolatile matter) determinations of polishes, resin solutions, and wax emulsions take 2 to 4 h in accordance with Test Method D2834, not counting preparation time.4.2 Curves of solids/refractive index provide a means for determining solids in a matter of minutes.4.3 This practice is particularly useful for quality control and in process control for the production of polishes and polish components.1.1 This practice covers the use of a refractometer for determining the nonvolatile matter (total solids) in floor polishes. This practice is also applicable to resin solutions and wax emulsions used in floor polishes.1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Pyrolysis liquid can be produced to various char concentrations. Increasing pyrolysis solids content can affect the pyrolysis liquid biofuel handling, atomization and storage stability in a negative manner.1.1 This test method describes a filtration procedure for determining the pyrolysis solids content of pyrolysis liquid. It is intended for the analysis of pyrolysis liquid with all ranges of pyrolysis solids concentrations.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Material Safety Data Sheets are available for reagents and materials. Review them for hazards prior to usage. For specific warning statements, see 7.2, 7.3, and 7.4.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Corrosion products, in the form of particulate and dissolved metals, in the steam and water circuits of electricity generating plants are of great concern to power plant operators. Aside from indicating the extent of corrosion occurring in the plant, the presence of corrosion products has deleterious effects on plant integrity and efficiency. Deposited corrosion products provide sites at which chemicals, which are innocuous at low levels, may concentrate to corrosive levels and initiate under-deposit corrosion. Also, corrosion products in feedwater enter the steam generating components where deposition on heat transfer surfaces reduces the overall efficiency of the plant.5.2 Most plants perform some type of corrosion product monitoring. The most common method is to sample for long time periods, up to several days, after which laboratory analysis of the collected sample gives the average corrosion product level over the collection time period. This methodology is referred to as integrated sampling. With the more frequent measurements in the on-line monitor, a time profile of corrosion product transport is obtained. Transient high corrosion product levels can be detected and measured, which cannot be accomplished with integrated sampling techniques. With this newly available data, plant operators may begin to correlate periods of high corrosion product levels with controllable plant operating events. In this way, operators may make more informed operational decisions with respect to corrosion product generation and transport.1.1 This test method covers the operation, calibration, and data interpretation for an on-line corrosion product (metals) monitoring system. The monitoring system is based on x-ray fluorescence (XRF) analysis of metals contained on membrane filters (for suspended solids) or resin membranes (for ionic solids). Since the XRF detector is sensitive to a range of emission energy, this test method is applicable to simultaneous monitoring of the concentration levels of several metals including titanium, vanadium, chromium, manganese, iron, cobalt, nickel, copper, zinc, mercury, lead, and others in a flowing sample. A detection limit below 1 ppb can be achieved for most metals.1.2 This test method includes a description of the equipment comprising the on-line metals monitoring system, as well as, operational procedures and system specifications.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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1.1 This specification describes the required properties and test methods for a one or two-component, cold liquid-applied elastomeric-type membrane comprised of silyl-terminated polyether polymer, silyl-terminated polyurethane polymer, or a blend of the two polymers for waterproofing building decks and walls subjected to hydrostatic pressure in building areas to be occupied by personnel, vehicles, or equipment. This specification applies only to a membrane system that will be covered with a separate wearing course, traffic course, or backfill.NOTE 1: See Guides C898/C898M and C1471/C1471M for proper application of membrane.1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Methods such as D3273 Standard Test Method for Resistance to Growth of Mold on the Surface of Interior Coatings in an Environmental Chamber and D3274 Standard Test Method for Evaluating the Degree of Surface Disfigurement of Paint Films by Fungal or Algal Growth or Soil or Dirt Accumulation provide means for assessing mold and algal staining on paints.5.2 This test method provides a technique for evaluating antimicrobials in or on polymeric solids against staining by Streptomyces species, bacteria and should assist in the prediction of performance of treated articles under actual field conditions.5.3 Conditioning of the specimens, such as exposure to leaching, weathering, and heat treatment, may have significant effects on performance of antimicrobials against staining. Determination of these effects is not included in this test method.1.1 This test method is intended to assess susceptibility of flat two dimensional vinyl films and other solid polymer products as well as products that may directly contact vinyl to pink-staining by the actinomycete bacteria Streptomyces species. This test method may not be suitable for highly textured or porous substrates.1.2 This test method is not suitable for evaluating dark-pigmented test samples.1.3 A knowledge of microbiological techniques is recommended for these procedures.1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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4.1 This guide is divided into two sections which provide design and specification guidelines for the use of a cold liquid-applied elastomeric membrane with integral wearing surface for waterproofing building decks in building areas to be occupied by personnel, vehicles, or equipment.4.2 The intent of Sections 5 – 11, Design Considerations, is to provide information and design guidelines where a waterproofing membrane with integral wearing surface is to be used. The intent of the remaining sections is to provide minimum guide specifications for the use of the purchaser and the seller in contract documents.4.3 Where the state of the art is such that criteria for a particular condition is not as yet firmly established or has numerous variables that require consideration, reference is made to the applicable portion of Sections 5 – 11 that covers the particular area of concern. Section 16 describes the repair, rehabilitation, and replacement of the membrane.1.1 This guide describes the design and installation of cold liquid-applied elastomeric waterproofing membrane systems that have an integral wearing surface. The cold liquid-applied elastomeric waterproofing membrane (membrane) to which this guide refers is specified in Specification C957/C957M.1.2 Concrete Slab-on-Grade—Waterproofing the upper surface of a concrete slab-on-grade presents special problems due to the possibility of negative hydrostatic pressure causing loss of bond to the substrate. Consideration of these problems is beyond the scope of this guide. Consult the membrane manufacturer for recommendations when this situation exists.1.3 The committee having jurisdiction for this guide is not aware of any similar ISO standard.1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see 15.4.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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The use of sound speed values to determine changes in the elastic constants due to applied or residual stress requires that such measurements be of high precision and low bias. For that reason, special evaluation tests to determine a representative precision and bias for the specific technique, method, and equipment setup used are given. Speed of sound is a measure that depends on the accurate measurements of length of path of travel and transit time or other related parameters such as frequency, etc. Both measurements are subject to certain interpretations and assumptions and are highly dependent on laboratory expertise. This practice provides a means of checking overall technique. This practice shall be used when it is necessary to assess the systematic and random errors associated with a particular speed of sound measurement in a solid medium. It can be used to check both equipment performance and measurement technique for these errors. It can also be used to study inherent errors in a particular method. It can also be used to assess proposed corrections to sound speed measurements such as the phase corrections of Papadakis (3, 4). The resultant precision and bias determined by the use of the described block represents a more ideal situation than the same measurement performed in practice, in the field. Thus, the error for the specific field measurement may be larger than indicated by this test. This test represents the best error condition for a given technique and practice. 1.1 This practice provides a means for evaluating both systematic and random errors for ultrasonic speed-of-sound measurement systems which are used for evaluating material characteristics associated with residual stress and which may also be used for nondestructive measurements of the dynamic elastic moduli of materials. Important features and construction details of a reference block crucial to these error evaluations are described. This practice can be used whenever the precision and bias of sound speed values are in question.1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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5.1 Reliable, controlled flow of bulk solids from bins and hoppers is essential in almost every industrial facility. Unfortunately, flow stoppages due to arching and ratholing are common. Additional problems include uncontrolled flow (flooding) of powders, segregation of particle mixtures, useable capacity which is significantly less than design capacity, caking and spoilage of bulk solids in stagnant zones, and structural failures.5.2 By measuring the flow properties of bulk solids, and designing bins and hoppers based on these flow properties, most flow problems can be prevented or eliminated.5.3 For bulk solids with a significant percentage of particles (typically, one third or more) finer than about 6 mm, the cohesive strength is governed by the fines (-6-mm fraction). For such bulk solids, cohesive strength and wall friction tests may be performed on the fine fraction only.NOTE 1: The quality of the result produced by this test method is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this test method are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors. Practice D3740 was developed for agencies engaged in the testing and/or inspection of soil and rock. As such it is not totally applicable to agencies performing this test method. However, users of this test method should recognize that the framework of Practice D3740 is appropriate for evaluating the quality of an agency performing this test method. Currently there is no known qualifying national authority that inspects agencies that perform this test method.1.1 This method 2covers the apparatus and procedures for measuring the cohesive strength of bulk solids during both continuous flow and after storage at rest. In addition, measurements of internal friction, bulk density, and wall friction on various wall surfaces are included.1.2 This standard is not applicable to testing bulk solids that do not reach the steady state requirement within the travel limit of the shear cell. It is difficult to classify ahead of time which bulk solids cannot be tested, but one example may be those consisting of highly elastic particles.1.3 The most common use of this information is in the design of storage bins and hoppers to prevent flow stoppages due to arching and ratholing, including the slope and smoothness of hopper walls to provide mass flow. Parameters for structural design of such equipment also may be derived from this data.1.4 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.1.4.1 The procedures used to specify how data are collected/recorded or calculated, in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user's objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analysis methods for engineering design.1.5 Units—The values stated in SI units are to be regarded as standard. No other units of measure are included in this standard1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The comparative method of measurement of thermal conductivity is especially useful for engineering materials including ceramics, polymers, metals and alloys, refractories, carbons, and graphites including combinations and other composite forms of each.5.2 Proper design of a guarded-longitudinal system is difficult and it is not practical in a method of this type to try to establish details of construction and procedures to cover all contingencies that might offer difficulties to a person without technical knowledge concerning theory of heat flow, temperature measurements, and general testing practices. Standardization of this test method is not intended to restrict in any way the future development by research workers of new or methods or improved procedures. However, new or improved techniques must be thoroughly tested. Requirements for qualifying an apparatus are outlined in Section 10.1.1 This test method describes a steady state technique for the determination of the thermal conductivity, λ, of homogeneous-opaque solids (see Notes 1 and 2). This test method is applicable to materials with effective thermal conductivities in the range 0.2 < λ < 200 W/(m·K) over the temperature range between 90 K and 1300 K. It can be used outside these ranges with decreased accuracy.NOTE 1: For purposes of this technique, a system is homogeneous if the apparent thermal conductivity of the specimen, λA, does not vary with changes of thickness or cross-sectional area by more than ±5 %. For composites or heterogeneous systems consisting of slabs or plates bonded together, the specimen should be more than 20 units wide and 20 units thick, respectively, where a unit is the thickness of the thickest slab or plate, so that diameter or length changes of one-half unit will affect the apparent λA by less than ±5 %. For systems that are non-opaque or partially transparent in the infrared, the combined error due to inhomogeneity and photon transmission should be less than ±5 %. Measurements on highly transparent solids must be accompanied with infrared absorption coefficient information, or the results must be reported as apparent thermal conductivity, λA.NOTE 2: This test method may also be used to evaluate the contact thermal conductance/resistance of materials and composites.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 These test methods are intended as a quick and reliable procedure for measuring the titanium dioxide pigment content of aqueous slurries. Included with the pigment content in the percent solids are the various nonvolatile additives used in preparing a stable slurry. Because the aluminum and silica oxide treatments on the more highly treated titanium dioxide pigments may change somewhat with prolonged drying, in the oven method the solids of the slurry are considered dry after heating at 105°C for 60 to 65 min. The high temperature associated with the infrared moisture analyzer may also effect a change in the aluminum and silica oxide treatment on highly treated TiO2 products. Therefore, care in selection of time and temperature are critical to obtain accurate results with the infrared method. With the short duration of test associated with the microwave drying system, overdrying is not a concern.1.1 These test methods cover the determination of the weight percent of solids in aqueous slurries of titanium dioxide pigments by either the use of a gravity-convection oven (Method A), infrared radiation moisture analyzer (Method B), or a microwave drying system (Method C).1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This test standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The specific gravity value is used in many phase relation equations to determine relative volumes of particle, water, and gas mixtures.5.2 The term soil particle typically refers to a naturally occurring mineral grain that is not readily soluble in water. Therefore, the specific gravity of soils that contain extraneous matter (such as cement, lime, and the like) or water-soluble material (such as salt) must be corrected for the precipitate that forms on the test specimen after drying. If the precipitate has a specific gravity less than the parent soil grains, the uncorrected test result will be too low. If the precipitate has a higher specific gravity, then the uncorrected test value will be too high.5.3 Heating during drying may diagenetically alter the structure of some clay minerals.3 Therefore caution should be exercised if the mineral composition of a clay test specimen is going to be determined after drying. It is possible to dry the test specimen at a lower temperature. However, the effect on water content4 and hence specific gravity should be investigated. In addition, some materials other than clay may be affected by drying at 110°C, such as gypsum, soils containing organics, fly ash containing residual coal, island sands. Test Method D2216 includes recommendations for drying gypsum using a lower temperature, such as 60°C.NOTE 1: The quality of the result produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing. Users of this standard are cautioned that compliance with Practice D3740 does not in itself ensure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.1.1 This test method covers the determination of the specific gravity of soil solids by means of a gas pycnometer. Particle size is limited by the dimensions of the test specimen container of the particular pycnometer being used.1.2 Test Method D854 may be used instead of or in conjunction with this test method for performing specific gravity tests on soils. Note that Test Method D854 does not require the specialized test apparatus needed by this test method. However, Test Method D854 may not be used if the test specimen contains matter that can readily dissolve in water, whereas this test method does not have that limitation.1.3 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.1.3.1 For purposes of comparing a measured or calculated value(s) with specified limits, the measured or calculated value(s) shall be rounded to the nearest decimal or significant digits in the specified limits.1.3.2 The procedures used to specify how data are collected/recorded and calculated in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that should generally be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analysis methods for engineering design.1.4 Units—The values stated in SI units are to be regarded as standard. The values given in parentheses are provided for information only and are not considered standard.1.4.1 The gravitational system of inch-pound units is used when dealing with inch-pound units. In this system, the pound (lbf) represents a unit of force (weight), while the unit for mass is slugs. The converted slug unit is not given, unless dynamic (F = ma) calculations are involved.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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