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1.1 This test method covers the gravimetric determination of phthalic anhydride in alkyd resins and esters that contain dibasic acids such as maleic, fumaric, adipic, and sebacic, which would interfere if Test Method D 563 was used.1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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3.1 This guide uses a weight-loss method of wear determination for the polymeric components used with hip joint prostheses, using serum or demonstrated equivalent fluid for lubrication, and running under a dynamic load profile representative of the human hip-joint forces during walking (1,2).5 The basis for this weight-loss method for wear measurement was originally developed (3) for pin-on-disk wear studies (see Practice F732) and has been extended to total hip replacements (4,5) femoral-tibial knee prostheses (6), and to femoropatellar knee prostheses (6,7).3.2 While wear results in a change in the physical dimensions of the specimen, it is distinct from dimensional changes due to creep or plastic deformation, in that wear generally results in the removal of material in the form of polymeric debris particles, causing a loss in weight of the specimen.3.3 This guide for measuring wear of the polymeric component is suitable for various simulator devices. These techniques can be used with metal, ceramic, carbon, polymeric, and composite counter faces bearing against a polymeric material (for example, polyethylene, polyacetal, and so forth). This weight-loss method, therefore, has universal application for wear studies of total hip replacements that feature polymeric bearings. This weight-loss method has not been validated for high-density material bearing systems, such as metal-metal, carbon-carbon, or ceramic-ceramic. Progressive wear of such rigid bearing combinations generally has been monitored using a linear, variable-displacement transducers or by other profilometric techniques.1.1 This guide describes a laboratory method using a weight-loss technique for evaluating the wear properties of materials or devices, or both, which are being considered for use as bearing surfaces of human-hip-joint replacement prostheses. The hip prostheses are evaluated in a device intended to simulate the tribological conditions encountered in the human hip joint, for example, use of a fluid such as bovine serum, or equivalent pseudosynovial fluid shown to simulate similar wear mechanisms and debris generation as found in vivo, and test frequencies of 1 Hz or less.1.2 Since the hip simulator method permits the use of actual implant designs, materials, and physiological load/motion combinations, it can represent a more physiological simulation than basic wear-screening tests, such as pin-on-disk (see Practice F732) or ring-on-disk (see ISO 6474).1.3 It is the intent of this guide to rank the combination of implant designs and materials with regard to material wear-rates, under simulated physiological conditions. It must be recognized, however, that there are many possible variations in the in vivo conditions, a single laboratory simulation with a fixed set of parameters may not be universally representative.1.4 The reference materials for the comparative evaluation of candidate materials, new devices, or components, or a combination thereof, shall be the wear rate of extruded or compression-molded, ultra-high molecular weight (UHMW) polyethylene (see Specification F648) bearing against standard counter faces [stainless steel (see Specification F138); cobalt-chromium-molybdenum alloy (see Specification F75); thermomechanically processed cobalt chrome (see Specification F799); alumina ceramic (see Specification F603)], having typical prosthetic quality, surface finish, and geometry similar to those with established clinical history. These reference materials will be tested under the same wear conditions as the candidate materials.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Low operating temperature fuel cells such as proton exchange membrane fuel cells (PEMFCs) require high purity hydrogen for maximum material performance and lifetime. Measurement of particulates in hydrogen is necessary for assuring a feed gas of sufficient purity to satisfy fuel cell and internal combustion system needs as defined in SAE J2719. The particulates in hydrogen fuel for fuel cell vehicles (FCV) and gaseous hydrogen powered internal combustion engine vehicles may adversely affect pneumatic control components, such as valves, or other critical system components. Therefore, the concentration of particulates in the hydrogen fuel should be limited as specified by ISO 14687-2, SAE J2719, or other hydrogen fuel quality specifications.5.2 Although not intended for application to gases other than hydrogen fuel, techniques within this test method can be applied to gas samples requiring determination of particulate concentration.1.1 This test method is primarily intended for gravimetric determination of particulate concentration in hydrogen intended as a fuel for fuel cell or internal combustion engine powered vehicles. This test method describes operating and quality control procedures required to obtain data of known quality satisfying the requirements of SAE J2719. This test method can be applied to other gaseous samples requiring determination of particulates provided the user’s data quality objectives are satisfied.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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3.1 This practice uses a weight-loss method of wear determination for the polymeric components or materials used in human joint prostheses, using serum or demonstrated equivalent fluid for lubrication, and running under a load profile representative of the appropriate human joint application (1,2) .4 The basis for this weight-loss method for wear measurement was originally developed (3) for pin-on-disk wear studies (Practice F732) and has been extended to total hip replacements (4, 5, ISO 14242–2, and Guide F1714), and to femoro-tibial knee prostheses (6 and ISO 14243–2), and to femoro-patellar knee prostheses (6,7).3.2 While wear results in a change in the physical dimensions of the specimen, it is distinct from dimensional changes due to creep or plastic deformation, in that wear results in the removal of material in the form of polymeric debris particles, causing a loss in weight of the specimen.3.3 This practice for measuring wear of the polymeric component is suitable for various simulator devices. These techniques can be used with metal, ceramic, carbon, polymeric, and composite counter faces bearing against a polymeric material (for example, polyethylene, polyacetal, and so forth). Thus, this weight-loss method has universal application for wear studies of human joint replacements which feature polymeric bearings. This weight-loss method has not been validated for non-polymeric material bearing systems, such as metal-metal, carbon-carbon, or ceramic-ceramic. Progressive wear of such rigid bearing combinations has generally been monitored using linear, variable-displacement transducers, or by other profilometric techniques.1.1 This practice describes a laboratory method using a weight-loss (that is, mass-loss; see X1.4) technique for evaluating the wear properties of polymeric materials or devices which are being considered for use as bearing surfaces of human joint replacement prostheses. The test specimens are evaluated in a device intended to simulate the tribological conditions encountered in the human joint; for example, use of a fluid such as bovine serum, or equivalent pseudosynovial fluid shown to simulate similar wear mechanisms and debris generation found in vivo.1.2 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The NVR determined by this test method is that amount that can reasonably be expected to exist on hardware exposed in environmentally controlled areas.5.2 The evaporation of the solvent at or near room temperature is to quantify the NVR that exists at room temperature.5.3 Numerous other methods are being used to determine NVR. This test method is not intended to replace methods used for other applications.1.1 This test method covers the determination of nonvolatile residue (NVR) fallout in environmentally controlled areas used for the assembly, testing, and processing of spacecraft.1.2 The NVR of interest is that which is deposited on sampling plate surfaces at room temperature: it is left to the user to infer the relationship between the NVR found on the sampling plate surface and that found on any other surfaces.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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1.1 This test method covers the determination of nonvolatile residue (NVR) fallout in environmentally controlled areas used for the assembly, testing, and processing of spacecraft. 1.2 The NVR of interest is that which is deposited on sampling plate surfaces at room temperature: it is left to the user to infer the relationship between the NVR found on the sampling plate surface and that found on any other surfaces. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. 1.4 The values stated in SI units are to be regarded as the standard.

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5.1 The NVR obtained by this test method is that amount which is available for release by wipers in normal use.5.2 Evaporation of the solvent at the stated temperature is to quantify the NVR that can be expected to exist at room temperature, since the slight difference between room temperature and test temperature has not been shown to result in significant variances.5.3 This test method may be more aggressive than necessary for the evaluation of wipers that will be restricted to dry use only.5.4 Numerous other methods are being used to determine NVR. This test method is not intended to replace test methods used for other applications.1.1 This test method covers the determination of solvent extractable nonvolatile residue (NVR) from wipers used in assembly, cleaning, or testing of spacecraft, but not from those used for analytical surface sampling of hardware.1.2 The NVR of interest is that which can be extracted from cleanroom wipers using a specified solvent that has been selected for its extractive qualities. Alternative solvents may be selected, but since their use may result in different values being generated, they must be identified in the procedure data sheet.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3.1 Exception—The inch-pound units are included for information only.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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1.1 This practice covers procedures for use in the calibration of volumetric instruments that include glassware, plasticware, and laboratory standards that are in common use in chemical, analytical, clinical, and calibration laboratories. It is based on the gravimetric determination of the quantity of pure water, either contained or delivered at a calibration temperature, and the conversion of this value to a volume at a given reference temperature, normally 20 °C by means of suitable equations. Calibration using mercury is excluded. Calibration may be performed using alternative gravimetric methodology, if it is demonstrated and documented that the results obtained are equivalent to those obtained using the methodology described herein. Alternative reference temperatures and associated equations are provided.1.2 This practice is intended to encompass volume capacity instruments between the limits of 0.1 cm3 and 10 000 cm3. Typical volumetric instruments falling within the purview of this practice are burettes graduated “to deliver,” graduated cylinders, volumetric flasks, measuring and dilution pipettes, transfer and capacity pipettes such as those in Specification E694, specific gravity flasks such as those used in several ASTM standards, and metallic volumetric standards such as those used in legal metrology.1.3 The procedures are not recommended for calibration of volumetric instruments with capacities below 0.1 cm3, such as microglassware without incorporating evaporation corrections; evaporation methods and corrections are not provided. Capacities given in 1.2 are not intended to be maximum capacity limitations; volumes greater than 10 000 cm3 may be calibrated with this procedure. Maximum capacity limitations are based on available equipment, standards, adequate quantities of pure water, and the ability to safely handle large volumetric instruments.1.4 This standard may be used for the calibration of volumetric instruments made from materials of glass, plastic, various stable metals, or any other stable materials provided appropriate volumetric coefficients of expansions are available.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method provides a means for resin producers and users as well as solvent and varnish manufacturers to rate various types of resins for solubility by assigning a numerical dilutability value. This percent dilutability value can be used to differentiate resin types for end users and can be utilized as a quality control tool by resin manufacturers.5.2 When running a series of these tests, the same lot or batch of dilution solvent must be used throughout to ensure reproducible results.1.1 This test method covers both volumetric and gravimetric determination of resin solution dilutability which gives a numerical value for the overall solubility of the resin expressed as percent dilutability.1.2 This test method is applicable only if the test solution is of sufficient clarity to allow accurate visual judgement of the end point and of low enough viscosity for efficient mixing to take place.1.3 This test method is primarily for, but not limited to, resins used in the printing ink industry.1.4 The percent solvent tolerance of a resin can be determined using this test method if the solvent in the resin solution and the dilution solvent are the same.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The function of these test methods is to define the percent of binder and retroreflective optics or non-retroreflective particles in the composition of the thermoplastic pavement marking as defined by the applicable specification for the manufacture of a specific thermoplastic pavement marking. The subsequent sample, as a result of ashing can be used to later test for the presence of titanium dioxide, lead chromate and possibly organic pigments.1.1 These test methods cover procedures for the gravimetric analysis of the binder and hydrochloric Acid (HCL) insoluble particles in white and yellow thermoplastic pavement markings. The HCL insoluble particles can be retroreflective optics, such as glass beads or some other type of retroreflective optic, or non-retroreflective particles such as silica sand, or a combination of any two or more of these materials.1.2 This standard does not address the physical separation and the individual quantification of each component when a mixture of two or more HCL insoluble materials is present. Rather it requires the user to visually evaluate the HCL insoluble material (obtained from following this test method) and report the types of materials present.1.3 This standard does not purport to address the titanium dioxide or lead chromate pigment measurement (after ashing) which is detailed in Test Methods D1394 and D126.1.4 This standard will attempt to address the interference of organic pigments with the binder results.1.5 The analytical procedures appear in the following order:  SectionsPercent Binder 10Percent Retroreflective Optics or Non-Retroreflective Particles 111.6 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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