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This specification covers austenitic stainless steel forgings for pressure and high temperature parts such as boilers, pressure vessels, and associated equipment. The grades covered here are F304, F304H, F304L, F304N, F304LN, F309H, F310, F310H, F316, F316H, F316L, F316N, F316LN, F321, F321H, F347, F347H, F348, F348H, FXM-19, FXM-11, and F46. Materials shall be produced by melting, forging, and rough machining, and shall be furnished by heat treatment in solution treated condition (solution annealing and quenching in water, oil, or a polymer water solution). Stainless steel specimens shall undergo heat and product analyses to evaluate the conformance of individual grades to specified elemental chemical compositions. Forgings shall also be examined for the adherence of each grade to required grain sizes and mechanical properties, which include tensile strength, yield strength, elongation, and reduction of area.1.1 This specification covers austenitic stainless steel forgings for boilers, pressure vessels, high temperature parts, and associated equipment.1.2 Supplementary requirements are provided for use when additional testing, inspection, or processing is required. In addition, supplementary requirements from Specification A788/A788M may be specified when appropriate.1.3 This specification includes the austenitic steel forgings that were a part of Specification A336/A336M.1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.1.5 Unless the order specifies the applicable “M” specification designation, the material shall be furnished to the inch-pound units.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test method may be used for material development, quality control, characterization, and design data generation purposes. This test method is intended to be used with ceramics whose strength is 50 MPa (~7 ksi) or greater. The test method may also be used with glass test specimens, although Test Methods C158 is specifically designed to be used for glasses. This test method may be used with machined, drawn, extruded, and as-fired round specimens. This test method may be used with specimens that have elliptical cross section geometries.4.2 The flexure strength is computed based on simple beam theory with assumptions that the material is isotropic and homogeneous, the moduli of elasticity in tension and compression are identical, and the material is linearly elastic. The average grain size should be no greater than one-fiftieth of the rod diameter. The homogeneity and isotropy assumptions in the standard rule out the use of this test for continuous fiber-reinforced ceramics.4.3 Flexural strength of a group of test specimens is influenced by several parameters associated with the test procedure. Such factors include the loading rate, test environment, specimen size, specimen preparation, and test fixtures (1-3).3 This method includes specific specimen-fixture size combinations, but permits alternative configurations within specified limits. These combinations were chosen to be practical, to minimize experimental error, and permit easy comparison of cylindrical rod strengths with data for other configurations. Equations for the Weibull effective volume and Weibull effective surface are included.4.4 The flexural strength of a ceramic material is dependent on both its inherent resistance to fracture and the size and severity of flaws in the material. Flaws in rods may be intrinsically volume-distributed throughout the bulk. Some of these flaws by chance may be located at or near the outer surface. Flaws may alternatively be intrinsically surface-distributed with all flaws located on the outer specimen surface. Grinding cracks fit the latter category. Variations in the flaws cause a natural scatter in strengths for a set of test specimens. Fractographic analysis of fracture surfaces, although beyond the scope of this standard, is highly recommended for all purposes, especially if the data will be used for design as discussed in Refs (3-5) and Practices C1322 and C1239.4.5 The three-point test configuration exposes only a very small portion of the specimen to the maximum stress. Therefore, three-point flexural strengths are likely to be greater than four-point flexural strengths. Three-point flexure has some advantages. It uses simpler test fixtures, it is easier to adapt to high temperature and fracture toughness testing, and it is sometimes helpful in Weibull statistical studies. It also uses smaller force to break a specimen. It is also convenient for very short, stubby specimens which would be difficult to test in four-point loading. Nevertheless, four-point flexure is preferred and recommended for most characterization purposes.1.1 This test method is for the determination of flexural strength of rod-shaped specimens of advanced ceramic materials at ambient temperature. In many instances it is preferable to test round specimens rather than rectangular bend specimens, especially if the material is fabricated in rod form. This method permits testing of machined, drawn, or as-fired rod-shaped specimens. It allows some latitude in the rod sizes and cross section shape uniformity. Rod diameters between 1.5 and 8 mm and lengths from 25 to 85 mm are recommended, but other sizes are permitted. Four-point-1/4-point as shown in Fig. 1 is the preferred testing configuration. Three-point loading is permitted. This method describes the apparatus, specimen requirements, test procedure, calculations, and reporting requirements. The method is applicable to monolithic or particulate- or whisker-reinforced ceramics. It may also be used for glasses. It is not applicable to continuous fiber-reinforced ceramic composites.FIG. 1 Four-Point-1/4-Point Flexure Loading Configuration1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This guide specifies standard specification for heavy-wall carbon and alloy steel pipe made from turned and bored forgings and is intended for high-temperature service. Heat and product analysis shall be conducted on several grades of ferritic steels, wherein the material shall conform to the required chemical composition for carbon, manganese, phosphorus, sulfur, silicon, chromium, and molybdenum. The steel pipe shall conform to the required tensile properties like tensile strength, yield strength, and elongation. Required mechanical tests for the steel pipe include transverse or longitudinal tension test, flattening test, and bend test.1.1 This specification2 covers heavy-wall carbon and alloy steel pipe (Note 1) made from turned and bored forgings and is intended for high-temperature service. Pipe ordered under this specification shall be suitable for bending and other forming operations and for fusion welding. Selection will depend on design, service conditions, mechanical properties and high-temperature characteristics.NOTE 1: The use of the word “pipe” throughout the several sections of this specification is used in the broad sense and intended to mean pipe headers, or leads.NOTE 2: The dimensionless designator NPS (nominal pipe size) has been substituted in this standard for such traditional terms as “nominal diameter,” “size,” and “nominal size.”1.2 Several grades of ferritic steels are covered. Their compositions are given in Table 1.1.3 Supplementary requirements (S1 to S7) of an optional nature are provided. Supplementary requirements S1 to S5 call for additional tests to be made, and when desired shall be so stated in the order, together with the number of such tests required as applicable.1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. Within the text, the SI units are shown in brackets. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard. The inch-pound units shall apply unless the “M” designation of this specification is specified in the order.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification covers hot- and cold-worked precipitation-hardenable nickel alloy rod, bar, forgings, and forging stock for high-temperature service. Chemical analysis shall be performed on the alloy and shall conform to the chemical composition requirement in carbon, manganese, silicon, phosphorus, sulfur, chromium, cobalt, molybdenum, columbium, tantalum, titanium, aluminum, zirconium, boron, iron, copper, and nickel. The material shall follow recommended annealing treatment, solution treatment, stabilizing treatment, and precipitation hardening treatment. Tension testing, hardness testing and stress-rupture testing shall be performed on the material and shall comply to the required tensile strength, yield strength, elongation, reduction in area, and Brinell hardness.1.1 This specification2 covers hot- and cold-worked precipitation-hardenable nickel alloy rod, bar, forgings, and forging stock for moderate or high temperature service (Table 1).1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to become familiar with all hazards including those identified in the appropriate Safety Data Sheet (SDS) for this product/material as provided by the manufacturer, to establish appropriate safety, health, and environmental practices, and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method is used to measure the apparent viscosity of thermoplastic pavement marking at elevated temperatures. Elevated temperature viscosities of thermoplastic pavement marking may be related to the properties of coatings, adhesives, and composite thermoplastics. This method is helpful in determining the flow properties which can be used in determining processability when applied to the road surface.5.2 Thermoplastic pavement markings may be applied to the road surface in several different ways. Typical methods of application are screed extrude, ribbon extrude, thin film spray, and standard spray. Proper application depends on the viscosity of the thermoplastic material at application temperatures for the method being used. Thin-line applied thermoplastic pavement marking, for example, requires a relatively lower viscosity. Screed extrude applied thermoplastic requires a higher viscosity.5.3 Materials of the type described in this procedure may be non-Newtonian, and as such, the apparent viscosity will be a function of shear rate under the conditions of test. Although the viscometer described in this test method operates under conditions of relatively low shear rate, differences in shear effect can exist depending upon the spindle and rotational speed conditions selected for the test program. Comparisons between non-Newtonian viscosity values should be made only for measurements made with similar viscometers under conditions of equivalent shear. For this method, “torpedo” spindles are recommended. Spindles considered torpedo spindles are ~1-in. long and come in many diameters with a 45° conical bottom. A diameter that is half the diameter of the thimbles used is recommended. If large glass beads are used in the pavement marking formulation, a smaller diameter spindle may be needed so the beads do not cause an impedance of the spindle due to a jamming between the inside wall of the thimble and the spindle.1.1 This test method covers the sample preparation and testing procedure needed to determine the apparent viscosity of a thermoplastic pavement marking formulation at elevated temperatures to the specimen.1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are customary units and are provided as a courtesy to the user.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价: 590元 / 折扣价: 502 加购物车

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This specification contains reference tables that give temperature-electromotive force (emf) relationships for types B, E, J, K, N, R, S, T, and C thermocouples. These are the thermocouple types most commonly used in industry. Thermocouples and matched thermocouple wire pairs are normally supplied to the tolerances on initial values of emf versus temperature. Color codes for insulation on thermocouple grade materials, along with corresponding thermocouple and thermoelement letter designations are given. Four types of tables are presented: general tables, EMF versus temperature tables for thermocouples, EMF versus temperature tables for thermoelements, and supplementary tables.1.1 This specification contains reference tables (Tables 8 to 25) that give temperature-electromotive force (emf) relationships for Types B, C, E, J, K, N, R, S, and T thermocouples.2 These are the thermocouple types most commonly used in industry. The tables contain all of the temperature-emf data currently available for the thermocouple types covered by this standard and may include data outside of the recommended upper temperature limit of an included thermocouple type.1.2 In addition, the specification includes standard and special tolerances on initial values of emf versus temperature for thermocouples (Table 1), thermocouple extension wires (Table 2), and compensating extension wires for thermocouples (Table 3). Users should note that the stated tolerances apply only to the temperature ranges specified for the thermocouple types as given in Tables 1, 2, and 3, and do not apply to the temperature ranges covered in Tables 8 to 25.1.3 Tables 4 and 5 provide insulation color coding for thermocouple and thermocouple extension wires as customarily used in the United States.1.4 Recommendations regarding upper temperature limits for the thermocouple types referred to in 1.1 are provided in Table 6.1.5 Tables 26 to 45 give temperature-emf data for single-leg thermoelements referenced to platinum (NIST Pt-67). The tables include values for Types BP, BN, JP, JN, KP (same as EP), KN, NP, NN, TP, and TN (same as EN).1.6 Tables for Types RP, RN, SP, and SN thermoelements are not included since, nominally, Tables 18 to 21 represent the thermoelectric properties of Type RP and SP thermoelements referenced to pure platinum. Tables for the individual thermoelements of Type C are not included because materials for Type C thermocouples are normally supplied as matched pairs only.1.7 Polynomial coefficients which may be used for computation of thermocouple emf as a function of temperature are given in Table 7. Coefficients for the emf of each thermocouple pair as well as for the emf of most individual thermoelements versus platinum are included. Coefficients for type RP and SP thermoelements are not included since they are nominally the same as for types R and S thermocouples, and coefficients for type RN or SN relative to the nominally similar Pt-67 would be insignificant. Coefficients for the individual thermoelements of Type C thermocouples have not been established.1.8 Coefficients for sets of inverse polynomials are given in Table 46. These may be used for computing a close approximation of temperature (°C) as a function of thermocouple emf. Inverse functions are provided only for thermocouple pairs and are valid only over the emf ranges specified.1.9 This specification is intended to define the thermoelectric properties of materials that conform to the relationships presented in the tables of this standard and bear the letter designations contained herein. Topics such as ordering information, physical and mechanical properties, workmanship, testing, and marking are not addressed in this specification. The user is referred to specific standards such as Specifications E235, E574, E585/E585M, E608/E608M, E1159, or E2181/E2181M for guidance in these areas.1.10 The temperature-emf data in this specification are intended for industrial and laboratory use.1.11 Thermocouple color codes per IEC 584–3 are given in Appendix X1.1.12 The values stated in either SI units or inch-pound units are to be regarded separately as standard.1.12.1 The values stated in brackets are not conversions to the values they succeed and therefore shall be used independently of the preceding values.1.12.2 The values given in parentheses are conversions of the values they succeed.1.12.3 Combining values from the two systems may result in non-conformance with the standard.1.13 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.14 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification covers hot- and cold-worked precipitation hardenable cobalt-containing alloys (UNS R30155 and UNS R30816) rod, bar, forgings, and forging stock for high temperature service. The material shall conform to the required chemical composition for carbon, manganese, silicon, phosphorus, sulfur, chromium, nickel, molybdenum, columbium, tantalum, iron, cobalt, and nitrogen. The materials shall conform to the required tensile and hardness properties such namely tensile strength, yield strength, alongation and Brinell hardness. The alloys shall also conform to the required stress-rupture properties. Dimensions such as diameter, thickness, or width, out-of-round, corners, cut lengths, straightness for cold-worked and hot-worked rod and bar shall be measured.1.1 This specification covers hot- and cold-worked precipitation hardenable cobalt-containing alloys (UNS R30155 and UNS R30816)2 rod, bar, forgings, and forging stock for high-temperature service.1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to become familiar with all hazards including those identified in the appropriate Safety Data Sheet (SDS) for this product/material as provided by the manufacturer, to establish appropriate safety, health, and environmental practices, and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价: 515元 / 折扣价: 438 加购物车

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5.1 Materials undergo an increase in molecular mobility at the glass transition seen as a sigmoidal step increase in the heat capacity. This mobility increase may lead to kinetic events such as enthalpic recovery, chemical reaction or crystallization at temperatures near the glass transition. The heat flow associated with the kinetic events may interfere with the determination of the glass transition.5.2 The glass transition is observed in differential scanning calorimetry as a sigmoidal or step change in specific heat capacity.5.3 MTDSC provides a test method for the separation of the heat flow due to heat capacity and that associated with kinetic events making it possible to determine the glass transition in the presence of interfering kinetic event.5.4 These test methods are useful in research and development, quality assurance and control and specification acceptance.5.5 Other methods for assigning the glass transition temperature include differential scanning calorimetry (Test Method E1356), thermomechanical analysis (Test Method E1545) and dynamic mechanical analysis (Test Method E1640).1.1 These test methods describe the assignment of the glass transition temperature of materials using modulated temperature differential scanning calorimetry (MTDSC) over the temperature range from –120 °C to +600 °C. The temperature range may be extended depending upon the instrumentation used.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价: 590元 / 折扣价: 502 加购物车

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4.1 These test methods for the chemical analysis of metals and alloys are primarily intended as referee methods to test such materials for compliance with compositional specifications, particularly those under the jurisdiction of Committee B02 on Nonferrous Metals and Alloys. It is assumed that all who use these test methods will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory under appropriate quality control practices such as those described in Guide E882.1.1 These test methods describe the chemical analysis of nickel, cobalt, and high-temperature alloys having chemical compositions within the following limits:  Element Composition Range, %    Aluminum   0.005 to 7.00      Beryllium   0.001 to 0.05      Boron   0.001 to 1.00      Calcium   0.002 to 0.05      Carbon   0.001 to 1.10      Chromium   0.10 to 33.00      Cobalt   0.10 to 75.00      Copper   0.01 to 35.00      Iron   0.01 to 50.00      Lead   0.001 to 0.01      Magnesium   0.001 to 0.05      Manganese   0.01 to 3.0      Molybdenum   0.01 to 30.0      Niobium (Columbium)   0.01 to 6.0       Nickel   0.10 to 98.0      Nitrogen   0.001 to 0.20      Phosphorus   0.002 to 0.08      Sulfur   0.002 to 0.10      Silicon   0.01 to 5.00      Tantalum   0.005 to 1.00      Tin   0.002 to 0.10      Titanium   0.01 to 5.00      Tungsten   0.01 to 18.00      Vanadium   0.01 to 3.25      Zinc   0.001 to 0.01      Zirconium   0.01 to 2.50    1.2 The test methods in this standard are contained in the sections indicated as follows:Aluminum, Total by the 8-Quinolinol Gravimetric Method (0.20 % to 7.00 %) 53 to 60Chromium by the Atomic Absorption Spectrometry Method (0.018 % to 1.00 %) 91 to 100Chromium by the Peroxydisulfate Oxidation—Titration Method (0.10 % to 33.00 %) 101 to 109Cobalt by the Ion-Exchange-Potentiometric Titration Method (2 % to 75 %) 25 to 32Cobalt by the Nitroso-R-Salt Spectrophotometric Method (0.10 % to 5.0 %) 33 to 42Copper by Neocuproine Spectrophotometric Method (0.010 % to 10.00 %) 43 to 52Iron by the Silver Reduction Titrimetric Method (1.0 % to 50.0 %) 118 to 125Manganese by the Metaperiodate Spectrophotometric Method (0.05 % to 2.00 %) 8 to 17Molybdenum by the Ion Exchange—8-Hydroxyquinoline  Gravimetric Method (1.5 % to 30 %) 110 to 117Molybdenum by the Thiocyanate Spectrophotometric Method (0.01 % to 1.50 %) 79 to 90Nickel by the Dimethylglyoxime Gravimetric Method (0.1 % to 84.0 %) 61 to 68Niobium by the Ion Exchange—Cupferron Gravimetric Method (0.5 % to 6.0 %) 126 to 133Silicon by the Gravimetric Method (0.05 % to 5.00 %) 18 to 24Tantalum by the Ion Exchange—Pyrogallol Spectrophotometric Method (0.03 % to 1.0 %) 134 to 142Tin by the Solvent Extraction-Atomic Absorption Spectrometry Method (0.002 % to 0.10 %) 69 to 781.3 Other test methods applicable to the analysis of nickel alloys that may be used in lieu of or in addition to this method are E1019, E1834, E1835, E1917, E1938, E2465, E2594, E2823.1.4 Some of the composition ranges given in 1.1 are too broad to be covered by a single method, and therefore, these test methods contain multiple methods for some elements. The user must select the proper test method by matching the information given in the scope and interference sections of each test method with the composition of the alloy to be analyzed.1.5 Units—The values stated in SI units are regarded as standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific caution and hazard statements are given in Section 7 and in 13.4, 15.1.1, 15.1.2, 21.2, 22.3, 57.3, 84.2, 114.5, 115.14, 130.4, 130.5, 138.5, and 138.6.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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1.1 This specification covers a coextruded polyethylene composite pressure pipe with a butt welded aluminum tube reinforcement between the inner and outer layers. The inner and outer polyethylene layers are bonded to the aluminum tube by a melt adhesive. Included is a system of nomenclature for the polyethylene-aluminum-polyethylene of raised temperature (PE-RT/AL/PE-RT) pipes, the requirements and test methods for materials, the dimensions and strengths of the component tubes and finished pipe, adhesion tests, and the burst and sustained pressure performance. Also given are the requirements and methods of marking. The pipe covered by this specification is intended for use in air conditioning and refrigeration (ACR) line set systems.1.2 This specification relates only to composite pipes incorporating a butt welded aluminum tube having both internal and external polyethylene layers. The welded aluminum tube is capable of sustaining internal pressures. Pipes consisting of metallic layers not butt welded together and plastic layers other than polyethylene are outside the scope of this specification.1.3 The dimensions in this specification are ID controlled to match that of ACR Copper Tube so that the flowrate and volume remains the same on a size-for-size basis.1.4 Specifications for fittings for use with pipe meeting the requirements of this specification are given in Annex A1.1.5 This specification excludes crosslinked polyethylene-aluminum-crosslinked polyethylene pipes (see Specification F1281).1.6 This specification tests the pipe for service at 60 °C ± 2 °C (140 °F ± 3 °F) or 82 °C ± 2 °C (180 °F ± 3 °F).1.7 Units—The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价: 590元 / 折扣价: 502 加购物车

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4.1 This test method may be used for material development, quality control, characterization, and design data generation purposes. This test method is intended to be used with ceramics whose strength is 50 MPa (~7 ksi) or greater.4.2 The flexure stress is computed based on simple beam theory with assumptions that the material is isotropic and homogeneous, the moduli of elasticity in tension and compression are identical, and the material is linearly elastic. The average grain size should be no greater than one-fiftieth of the beam thickness. The homogeneity and isotropy assumption in the standard rule out the use of this test for continuous fiber-reinforced ceramics.4.3 Flexural strength of a group of test specimens is influenced by several parameters associated with the test procedure. Such factors include the loading rate, test environment, specimen size, specimen preparation, and test fixtures. Specimen sizes and fixtures were chosen to provide a balance between practical configurations and resulting errors, as discussed in MIL-STD-1942(MR) and Refs (1, 2).4 Specific fixture and specimen configurations were designated in order to permit ready comparison of data without the need for Weibull-size scaling.4.4 The flexural strength of a ceramic material is dependent on both its inherent resistance to fracture and the size and severity of flaws. Variations in these cause a natural scatter in test results for a sample of test specimens. Fractographic analysis of fracture surfaces, although beyond the scope of this standard, is highly recommended for all purposes, especially if the data will be used for design as discussed in MIL-STD-1942(MR) and Refs (2-5) and Practices C1322 and C1239.4.5 The three-point test configuration exposes only a very small portion of the specimen to the maximum stress. Therefore, three-point flexural strengths are likely to be much greater than four-point flexural strengths. Three-point flexure has some advantages. It uses simpler test fixtures, it is easier to adapt to high temperature and fracture toughness testing, and it is sometimes helpful in Weibull statistical studies. However, four-point flexure is preferred and recommended for most characterization purposes.4.6 This method determines the flexural strength at ambient temperature and environmental conditions. The flexural strength under ambient conditions may or may not necessarily be the inert flexural strength.NOTE 7: time dependent effects may be minimized through the use of inert testing atmosphere such as dry nitrogen gas, oil, or vacuum. Alternatively, testing rates faster than specified in this standard may be used. Oxide ceramics, glasses, and ceramics containing boundary phase glass are susceptible to slow crack growth even at room temperature. Water, either in the form of liquid or as humidity in air, can have a significant effect, even at the rates specified in this standard. On the other hand, many ceramics such as boron carbide, silicon carbide, aluminum nitride, and many silicon nitrides have no sensitivity to slow crack growth at room temperature and the flexural strength in laboratory ambient conditions is the inert flexural strength.1.1 This test method covers the determination of flexural strength of advanced ceramic materials at ambient temperature. Four-point-1/4-point and three-point loadings with prescribed spans are the standard as shown in Fig. 1. Rectangular specimens of prescribed cross-section sizes are used with specified features in prescribed specimen-fixture combinations. Test specimens may be 3 by 4 by 45 to 50 mm in size that are tested on 40-mm outer span four-point or three-point fixtures. Alternatively, test specimens and fixture spans half or twice these sizes may be used. The method permits testing of machined or as-fired test specimens. Several options for machining preparation are included: application matched machining, customary procedure, or a specified standard procedure. This method describes the apparatus, specimen requirements, test procedure, calculations, and reporting requirements. The test method is applicable to monolithic or particulate- or whisker-reinforced ceramics. It may also be used for glasses. It is not applicable to continuous fiber-reinforced ceramic composites.1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 The useful life of photovoltaic modules may depend on their ability to withstand repeated temperature cycling with varying amounts of moisture in the air. These test methods provide procedures for simulating the effects of cyclic temperature and humidity environments. An extended duration damp heat procedure is provided to simulate the effects of long term exposure to high humidity.4.2 The durations of the individual environmental tests are specified by use of this test method; however, commonly used durations are 50 and 200 thermal cycles, 10 humidity-freeze cycles, and 1000 h of damp heat exposure, as specified by module qualification standards such as IEC 61215 and IEC 61646. Longer durations can also be specified for extended duration module stress testing.4.3 Mounting—Test modules are mounted so that they are electrically isolated from each other, and in such a manner to allow free air circulation around the front and back surfaces of the modules.4.4 Current Biasing: 4.4.1 During the thermal cycling procedure, test modules are operated without illumination and with a forward-bias current equal to the maximum power point current at standard reporting conditions (SRC, see Test Methods E1036) flowing through the module circuitry.4.4.2 The current biasing is intended to stress the module interconnections and solder bonds in ways similar to those that are believed to be responsible for fill-factor degradation in field-deployed modules.4.5 Effects of Test Procedures—Data generated using these test methods may be used to evaluate and compare the effects of simulated environment on test specimens. These test methods require determination of both visible effects and electrical performance effects.4.5.1 Effects on modules may vary from none to significant changes. Some physical changes in the module may be visible when there are no apparent electrical changes in the module. Similarly, electrical changes may occur with no visible changes in the module.4.5.2 All conditions of measurement, effects of cycling, and any deviations from this test method must be described in the report so that an assessment of their significance can be made.4.6 Sequencing—If these test methods are performed as part of a combined sequence with other environmental or non-environmental tests, the results of the final electrical tests (6.2) and visual inspection (6.3) determined at the end of one test may be used as the initial electrical tests and visual inspection for the next test; duplication of these tests is not necessary unless so specified.1.1 These test methods provide procedures for stressing photovoltaic modules in simulated temperature and humidity environments. Environmental testing is used to simulate aging of module materials on an accelerated basis.1.2 Three individual environmental test procedures are defined by these test methods: a thermal cycling procedure, a humidity-freeze cycling procedure, and an extended duration damp heat procedure. Electrical biasing is utilized during the thermal cycling procedure to simulate stresses that are known to occur in field-deployed modules.1.3 These test methods define mounting methods for modules undergoing environmental testing, and specify parameters that must be recorded and reported.1.4 These test methods do not establish pass or fail levels. The determination of acceptable or unacceptable results is beyond the scope of these test methods.1.5 Any of the individual environmental tests may be performed singly, or may be combined into a test sequence with other environmental or non-environmental tests, or both. Certain pre-conditioning tests such as annealing or light soaking may also be necessary or desirable as part of such a sequence. The determination of any such sequencing and pre-conditioning is beyond the scope of this test method.1.6 These test procedures are limited in duration and therefore the results of these tests cannot be used to determine photovoltaic module lifetimes.1.7 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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The forest products finishing industry has encountered difficulties in measuring the temperature of painted surfaces prior to, during, and after the curing process. The use of thermocouples is not entirely satisfactory because the thermocouple wires tend to conduct heat away too rapidly from the area where the temperature is being measured. Infrared radiation thermometers that are simple to operate can circumvent this difficulty. After calibration they are aimed at the surface, switched on, and the temperature read directly from an indicating gage. Note 1—Temperature-sensitive crayons, papers, and pellets may be successfully used to measure only the highest temperature reached by painted surfaces during the curing cycle. There are several different types of infrared radiation thermometers, including those based on lead sulfide or thermistor sensors and those that are simple thermal voltaic transducers. As such they respond to different wavelengths of infrared radiation and have different areas of applicability. Only instruments that have been evaluated are included in this practice.1.1 This practice is intended to serve as a guide in measuring with infrared instruments the temperature during the curing process of coatings applied to wood products. 1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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5.1 There are many underground structures that are constructed for permanent or long-term use. Often, these structures are subjected to a relatively constant load. Creep tests provide quantitative parameters for stability analysis of these structures.5.2 The deformation and strength properties of rock cores measured in the laboratory usually do not accurately reflect large-scale in situ properties, because the latter are strongly influenced by joints, faults, inhomogeneities, weakness planes, and other factors. Therefore, laboratory test results of intact specimens shall be utilized with proper judgment in engineering applications.NOTE 1: The statements on precision and bias contained in this test method; the precision of this test method is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing. Users of this test method are cautioned that compliance with Practice D3740 does not in itself assure reliable testing. Reliable testing depends on many factors; Practice D3740 provides a means of evaluating some of these factors.1.1 These test methods cover the creep behavior of intact weak and hard rock core in fixed states of stress at ambient (room) or elevated temperatures. For creep behavior at lower temperatures refer to Test Method D5520. The methods specify the apparatus, instrumentation, and procedures necessary to determine the strain as a function of time under sustained load at constant temperature and when applicable, constant humidity.1.1.1 Hard rocks are considered those with a maximum axial strain at failure of less than 2 %. Weak rocks include such materials as salt, potash, shale, and weathered rock, which often exhibit very large strain at failure.1.2 This standard consists of three methods that cover the creep capacity of core specimens.1.2.1 Method A—Creep of Hard Rock Core Specimens in Uniaxial Compression at Ambient or Elevated Temperature.1.2.2 Method B—Creep of Weak Rock Core Specimens in Uniaxial Compression at Ambient or Elevated Temperature.1.2.3 Method C—Creep of Rock Core Specimens in Triaxial Compression at Ambient or Elevated Temperature.1.3 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.1.4 The procedures used to specify how data are collected/recorded and calculated in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to commensurate with these considerations. It is beyond the scope of these test methods to consider significant digits used in analysis methods for engineering design.1.5 Units—The values stated in SI units are to be regarded as the standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and to determine the applicability of regulatory limitations prior to use. For specific precautionary statements, see Section 7.

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5.1 Thermocouples fabricated from thermocouple cable that has been contaminated by moisture or by other impurities may undergo large changes in thermoelectric properties or may fail catastrophically when exposed to high temperatures. Since such contamination usually lowers the electrical resistance between the thermoelements and the sheath substantially, measurement of the insulation resistance can provide a valuable check of insulation quality and cleanliness, and can serve as a basis for rejection of unsuitable material and unreliable components. For manufacturers in particular, low electrical insulation resistance can also be indicative of displaced thermoelements or conductors or defects in the metal sheath which will require further investigation, but all users should be aware of these potential defects when faced with an unacceptable insulation resistance measurement.5.2 This test method is primarily intended for use by manufacturers and users of mineral-insulated, metal-sheathed (MIMS) thermocouples or MIMS cables to verify that measured values of insulation resistance exceed specified minimum values, such as those listed in Specifications E235, E585/E585M, E608/E608M, E2181/E2181M, and E2821. Manufacturers and users should be aware, however, that when the insulation resistance is greater than 1 × 108 Ω, disagreement by an order of magnitude in the results obtained with this test method is not unusual. In addition, users of this test method should appreciate that the room temperature insulation resistance of both MIMS cables and of finished thermocouples will change during shipment, storage, and use if the end seals are damaged or defective. Consequently, values of insulation resistance determined by this test method may not necessarily be repeatable.1.1 This test method provides the procedures for measuring the room temperature electrical insulation resistance between the thermoelements and between the thermoelements and the sheath, of a mineral-insulated, metal-sheathed (MIMS) thermocouple or mineral-insulated, metal-sheathed (MIMS) thermocouple cable or between the conductors and between the conductors and the sheath, of mineral-insulated, metal-sheathed (MIMS) cable used for industrial resistance thermometers. It may be used to measure the insulation resistance of bulk lengths of mineral-insulated, metal-sheathed MIMS cable previously sealed against moisture intrusion or to test a thermocouple having an ungrounded measuring junction. This method cannot be used to test a thermocouple having a grounded measuring junction unless the measuring junction is removed prior to testing, after which the thermocouple may be dealt with in the same manner as a mineral-insulated, metal-sheathed (MIMS) cable.1.2 This test method applies primarily to thermocouple cables and cable used for industrial resistance thermometers conforming to Specifications E585/E585M, E2181/E2181M, and E2821 and to thermocouples conforming to Specifications E608/E608M and E2181/E2181M, but may also be applied to thermocouples or MIMS cables that are suitable for use in air, whose sheath or thermoelements or conductors are comprised of refractory metals, that are tested in a dry and chemically inert environment, and that may employ compacted ceramic insulating materials other than magnesia (MgO) or alumina (Al2O3). Users of this test method should note that specifications dealing with compacted ceramic insulating materials other than magnesia or alumina, which are described in Specification E1652, are not currently available. As a result, acceptance criteria must be agreed upon between the customer and supplier at the time of purchase, or alternatively, judgment and experience must be applied in establishing test voltage levels and acceptable insulation resistance values for these types of thermocouples and MIMS cables.1.3 This test method may be used for thermocouples or MIMS cables having an outside diameter of 0.5 mm (0.020 in.) or larger.1.4 Users of this test method should be aware that the room temperature insulation resistance of a mineral-insulated, metal-sheathed thermocouple or MIMS cable will change during shipment, storage, or use if they are not properly sealed.1.5 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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