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ASTM D98-15(2021) Standard Specification for Calcium Chloride Active 发布日期 :  1970-01-01 实施日期 : 

This specification covers technical grade calcium chloride typically used for, but not limited to, dust control, stabilization, ice/snow removal, other road-conditioning purposes, acceleration of the set of concrete, and as a desiccant. Two types of calcium chloride are covered, as follows: Type S (solid), flake, pellet, or granular calcium chloride in varying concentrations; and Type L (liquid), water solutions of calcium chloride in varying concentrations. Concentrations shall be expressed as a percentage of the total. Impurities such as alkali chlorides, magnesium, and calcium hydroxide should be within specified composition limits.1.1 This specification covers calcium chloride, technical grade, typically used for, but not limited to, dust control, stabilization, ice/snow removal, other road-conditioning purposes, acceleration of the set of concrete, and as a desiccant.1.2 The values stated in SI units are to be regarded as the standard.1.3 For purposes of determining conformance to this specification, values for chemical analysis shall be rounded to the nearest 0.1 %, and values for grading shall be rounded to the nearest 1 %, in accordance with the rounding method in Practice E29.1.4 The text of this standard references notes and footnotes, which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D4288-02(2019) Standard Specification for Calcium Borosilicate Pigments Active 发布日期 :  1970-01-01 实施日期 : 

This specification covers three grades of pigment commercially known as calcium borosilicate composite pigment. The two types differ in chemical composition while the two classes of type I differ in oil absorption. The chemical composition, ignition loss, and particle size shall be tested to meet the requirements prescribed. The specific surface diameter of the pigment, oil absorption, and coarse particle shall be tested to meet the requirements prescribed.1.1 This specification covers three grades of pigment commercially known as calcium borosilicate composite pigment. The two types differ in chemical composition while the two classes of Type I differ in oil absorption.1.2 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Calcium and magnesium salts in water are the primary components of water hardness which can cause pipe or tube scaling.1.1 These test methods cover the determination of calcium and magnesium in water by complexometric titration and atomic absorption spectrometric procedures. Two test methods are included, as follows:  SectionsTest Method A—Complexometric Titration 7 – 15Test Method B—Atomic Absorption Spectrometric 16 – 251.2 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversion to inch-pound units that are provided for information only and are not considered standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in 12.2.6 and 20.6.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This test method describes procedures to be used for sampling calcium chloride, and for determining grading of solid forms of calcium chloride for comparison with the requirements of a specification, such as Specification D98.1.1 This test method covers sampling of solid and liquid forms of calcium chloride, and sieve analysis of solid form calcium chloride. Referee procedures for chemical analysis are covered in Test Methods E449.1.2 A rapid method of chemical analysis is shown in Appendix X1. This rapid method is not to be used for determining chemical compliance of calcium chloride with specification requirements, such as in Specification D98.1.3 The values stated in SI units are to be regarded as the standard.1.4 This standard does not purport to address the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.1.1.1 This appendix covers a rapid method for chemical analysis of calcium chloride.

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4.1 Use this test method to obtain a quantitative value indicating the rate of moisture vapor emission from the surface of a concrete floor and whether or not that floor is acceptable to receive resilient floor covering. The moisture vapor emission rate only reflects the condition of the concrete floor at the time of the test. All concrete subfloors emit some amount of moisture in vapor form. Concrete moisture emission is a natural process driven by environmental conditions. All floor coverings are susceptible to failure from excessive moisture vapor emissions. The moisture vapor emitted from a concrete slab is measured in pounds. This measurement is the equivalent weight of water evaporating from 1000 ft2 of concrete surface in a 24-h period. The calcium chloride moisture test has been the industry standard for making this determination and is a practical, well-established and accepted test of dynamic moisture. It will produce quantified results directly applicable to flooring manufacturer's specifications. The results obtained reflect the condition of the concrete floor surface at the time of testing and may not indicate future conditions.1.1 This test method covers the quantitative determination of the rate of moisture vapor emitted from below-grade, on-grade, and above-grade (suspended) bare concrete floors.1.2 This test shall not be used to evaluate the rate of moisture vapor emitted by gypsum concrete or floors containing lightweight aggregate.1.3 This test shall not be used to evaluate moisture vapor emissions over coatings on concrete or through reactive penetrants or over patching or leveling compounds.1.4 This quantity of moisture shall be expressed as the rate of moisture vapor emission, measured in pounds of moisture over a 1000 ft2 area during a 24-h period.1.5 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This practice covers the mathematical calculation of the supersaturation of three principal sulfate scaling compounds found in industrial operations. Application of this standard practice to the prediction of scale formation in a given system, however, requires experience. The calculations tell the user if a water, or mixture of waters, is in a scaling mode. Whether or not scale will in fact form, how quickly it will form, where it will form, in what quantities, and what composition are subject to factors beyond the scope of this practice. However, based on how supersaturated a given water or mixture of waters is, an objective evaluation of the relative likelihood of scale formation can be made.NOTE 1: There are several personal computer (PC) type programs that are both available commercially and publicly that will perform these calculations.1.1 This practice covers the calculation of supersaturation of barium sulfate, strontium sulfate, and calcium sulfate dihydrate (gypsum) in brackish water, seawater, and brines in which barium, strontium, and calcium ions either coexist or exist individually in solution in the presence of sulfate ions.1.2 This practice is not applicable for calculating calcium sulfate dihydrate supersaturation if the temperatures of saline waters under investigation exceed 95°C. At temperatures above 95°C, hemianhydrate and anhydrite would be major insoluble forms.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Lubricating oils can be formulated with additives, which can act as detergents, anti-oxidants, anti-wear agents, and so forth. Some additives can contain one or more of calcium, copper, magnesium, phosphorus, sulfur, and zinc. This test method can be used to determine if the oils, additives, and additive packages meet specification with respect to content of these elements.4.2 Several additive elements and their compounds are added to the lubricating oils to give beneficial performance (Table 3).4.3 This test method can also be used to determine if lubricating oils, additives, and additive packages meet specification with respect to chlorine concentration. In this context, specification can refer to contamination.4.4 This test method is not intended for use on samples that contain some component that significantly interferes with the analysis of the elements specified in the scope.4.5 This test method can complement other test methods for lube oils and additives, including Test Methods D4628, D4927, D4951, and D5185.1.1 This test method covers the determination of calcium, chlorine, copper, magnesium, phosphorus, sulfur, and zinc in unused lubricating oils, additives, and additive packages by wavelength dispersive X-ray fluorescence spectrometry. Matrix effects are handled with mathematical corrections.1.2 For each element, the upper limit of the concentration range covered by this test method is defined by the highest concentration listed in Table 1. Samples containing higher concentrations can be analyzed following dilution.1.3 For each element, the lower limit of the concentration range covered by this test method can be estimated by the limit of detection (LOD)2 (see also 40 CFR 136 Appendix B) or limit of quantification (LOQ),2 both of which can be estimated from Sr, the repeatability standard deviation. LOD and LOQ values, determined from results obtained in the interlaboratory study on precision, are listed in Table 2.1.3.1 LOD and LOQ are not intrinsic constants of this test method. LOD and LOQ depend upon the precision attainable by a laboratory when using this test method.1.4 This test method uses regression software to determine calibration parameters, which can include influence coefficients (that is, interelement effect coefficients) (Guide E1361), herein referenced as alphas. Alphas can also be determined from theory using relevant software.1.5 Setup of this test method is intended for persons trained in the practice of X-ray spectrometry. Following setup, this test method can be used routinely.1.6 The values stated in either SI units or angstrom (Å) units are to be regarded separately as standard.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 There are existing lime-based flue gas desulfurization units in operation that require a method to measure the oxides available for sulfur dioxide absorption. Dissolved magnesium oxide varies among limes depending on the limestone sources and calcination conditions.1.1 This test method covers analysis of magnesian, dolomitic and high-calcium limes for total neutralizing capability and dissolved major oxides. Dissolved calcium and magnesium are the major species that neutralize acid under the conditions of the test.1.2 The test conditions are chosen to measure the acid-neutralizing capacity of both calcium hydroxide and magnesium hydroxide contained in slaked lime. By controlling the neutralization pH at 6, magnesium hydroxide and magnesium oxide are titrated in addition to calcium hydroxide fraction.1.3 This test method also determines the fraction of Mg ions present in the lime that will dissolve under lime flue gas desulfurization (FGD) conditions. Because the Mg2+ ion alters FGD performance, it is important to know its concentration.1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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