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ASTM E449-18 Standard Test Methods for Analysis of Calcium Chloride Active 发布日期 :  1970-01-01 实施日期 : 

3.1 Calcium chloride is available in various forms and purities. A major use is the de-icing and dust control of roads. It is also used in the coal industry for dustproofing and freezeproofing, in foods, in electrolytic cells, and in refrigeration brines. The test methods listed in 1.2 provide procedures for analyzing calcium chloride to determine if it is suitable for its intended use.1.1 These test methods cover the analysis of calcium chloride and solutions.1.2 Procedures are given for the determination of calcium chloride, magnesium chloride, potassium chloride, sodium chloride, and calcium hydroxide. The test methods appear in the following order:  SectionsCalcium Chloride 8 to 17Magnesium Chloride, Potassium Chloride,and Sodium Chloride 18 to 28Calcium Hydroxide 29 to 361.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.1.4 Review the current Safety Data Sheet (SDS) for detailed information concerning toxicity, first aid procedures, handling, and safety precautions.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in Section 5.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Although Test Method D4017 is widely used for the determination of water in paints and related materials, this method may overcome some of the variability found in the Karl Fischer method.4.2 Control of water content is often important in controlling the performance of paints, and it is critical in determining volatile organic compound (VOC) content when VOC content is measured by difference from total volatile matter and water content as required in certain federal and state regulations.1.1 This test method describes the determination of the total water content of paints using a calcium hydride reaction test kit, or water content between 2 and 85 % water.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification covers structural insulating board for general thermal insulating, fire-resistive, and marine bulkhead applications. The structural insulating boards shall be of the following types and grades: Types I and II and Grades 1; 2; 3; 4; 5; 6; 7; and 8. Calcium silicate structural insulating board shall be composed of hydrated calcium silicate with natural or man-made fibers or fillers, or a combination thereof. The following test methods shall be performed: dimensions and density; flexural strength; compressive strength; screw holding strength; apparent thermal conductivity; combustion characteristics; and maximum use temperatures.1.1 This specification covers structural insulating board for general thermal insulating, fire-resistive, and marine bulkhead applications. The rigid, preformed structural insulating board is for use at temperatures up to 1700°F (927°C). For specific applications, the actual temperature limit shall be agreed upon between the manufacturer and the purchaser.1.2 The structural insulating board maintains its structural integrity after immersion in water.1.3 Rapid cycling over a wide temperature range is not recommended because of potential damage due to thermal shock.1.4 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.5 When the installation or use of thermal insulation materials, accessories and systems, may pose safety or health problems, the manufacturer shall provide the user appropriate current information regarding any known problems associated with the recommended use of the company's products, and shall also recommend protective measures to be employed in their safe utilization. The user shall establish appropriate safety and health practices and determine the applicability of regulatory requirements prior to use.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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3.1 These test methods compile in one place, recommended procedures for analysis of the pigment known commercially as calcium borosilicate. This pigment is used extensively in paints and the composition is important to the user and producer.1.1 These test methods cover the analysis of the pigment commercially known as calcium borosilicate.1.2 The test methods appear in the following order:Test Methods SectionsSilicon Dioxide (SiO2) 6 – 9Iron Oxide (Fe2O3) 10 – 13Boron Trioxide (B2O3) 17 – 20Calcium Oxide (CaO) 21 – 23Moisture and Volatile Matter 24Water of Hydration 25 to 26Coarse Particles 27Oil Absorption 281.3 Individual specimens may be used for the direct determinations of SiO2, B2O3, and CaO. SiO2 and Fe2O3 should be removed before the determination of the B2O3 and CaO.1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method is intended as a referee method for compliance with compositional specifications for impurity content. It is assumed that all who use this procedure will be trained analysts capable of performing common laboratory practices skillfully and safely. It is expected that work will be performed in a properly equipped laboratory and that proper waste disposal procedures will be followed. Follow appropriate quality control practices such as those described in Guide E882.1.1 This test method covers the determination of calcium and magnesium in iron ores, concentrates, and agglomerates in the mass fraction (%) range from 0.05 % to 5 % of calcium and 0.05 % to 3 % of magnesium.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Fluorspar is used as a flux in the steelmaking and glass industries, and in the manufacture of HF.5.2 This test method is intended to be used for compliance with compositional specifications for calcium fluoride content. It is assumed that all who use these procedures will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory and that proper waste disposal procedures will be followed. Appropriate quality control practices must be followed such as those described in Guide E882.1.1 This test method covers the determination of calcium fluoride in acid-grade fluorspar and other types of fluorspar that can be rendered soluble by the procedure described in the test method.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This test method has been evaluated in accordance with Practice E1601 and Guide E1763. Unless otherwise noted in the precision and bias section, the lower limit in the scope of each method specifies the lowest analyte content that may be analyzed with acceptable error (defined as a nominal 5 % risk of obtaining a 50 % or larger relative difference in results on the same test sample in two laboratories).1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM E1229-21 Standard Specification for Calcium Hypochlorite Active 发布日期 :  1970-01-01 实施日期 : 

This specification covers technical-grade calcium hypochlorite in granular form. Sampled specimens shall be tested and conform accordingly to chemical and physical requirements such as available chlorides, moisture content, and particle sizes through a U.S. 14 and U.S. 100 mesh.1.1 This specification covers technical-grade calcium hypochlorite in granular form.1.2 The following applies to all specified limits in this specification: for purposes of determining conformance with this specification, an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29.1.3 Units—The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.1.4 Review the current Safety Data Sheets (SDS) for detailed information concerning toxicity, first aid procedures, handling and safety precautions.1.5 The following safety hazards caveat pertains only to the test methods listed in Sections 3 – 5. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test method may be used to confirm the stated calcium or zinc content of pure liquid calcium or zinc driers soluble in toluene-alcohol and manufactured for use by the coatings industry.1.1 This test method covers a titrimetric determination of calcium in liquid calcium driers and zinc in liquid zinc driers that can be dissolved in a toluene-alcohol mixture and utilizes the disodium salt of ethylenediaminetetraacetic acid dihydrate (EDTA).1.2 This test method is not applicable to drier blends.1.3 All cations that can be titrated with EDTA in alkaline media interfere and must not be present in the sample.1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The tensile test method is recommended for tension testing of calcium phosphate/substrate or porous metal coating/substrate combinations and can provide information on the adhesive or cohesive strength of coatings under (uniaxial) tensile stress.5.2 The test method may be useful for comparative evaluation of adhesive or cohesive strengths of a variety of types of coatings. Coatings may be applied using a variety of methods, including, but not limited to, plasma-spraying and sintering. Information developed using this test method may be useful for certain quality control and design purposes.5.3 The test should not be considered to provide an intrinsic value for utilization directly in making calculations such as determining the ability of a coating to withstand specified environmental stresses.5.4 Processing variables such as substrate preparation prior to coating, surface texture, coating technique variables or postcoating heat treatment variables may introduce a significant effect on the results of the tension test. The specimen being evaluated must be representative of the actual end-use coating.1.1 This test method covers tension testing of calcium phosphate and metallic porous coatings adhering to dense metal substrates at ambient temperatures. It assesses the degree of adhesion of coatings to substrates, or the internal cohesion of a coating in tension normal to the surface plane.1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM F1501-95 Test Method for Tension Testing of Calcium Phosphate Coatings (Withdrawn 2000) Withdrawn, Replaced 发布日期 :  1970-01-01 实施日期 : 

1.1 This test method covers tension testing of continuous calcium phosphate coatings adhering to dense metal substrates at ambient temperatures. It assesses the degree of adhesion of coatings to substrates, or the internal cohesion of a coating in tension, normal to the surface plane. 1.2 The values stated in SI units are to be regarded as the standard. The inch-pound units given in parentheses are for information only. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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This specification covers brick made principally from sand and lime and intended for use in brick masonry. Two grades of brick are covered: grade SW - brick intended for use where exposed to temperature below freezing in the presence of moisture, grade MW - brick intended for use where exposed to temperature below freezing but unlikely to be saturated with eater. The brick shall conform to the physical requirements for the grade specified, as prescribed. All units shall be sound and free of cracks or other defects that interfere with the proper placement of the unit or significantly impair the strength or permanence of the construction.1.1 This specification covers brick made principally from sand and lime and intended for use in brick masonry. Two grades of brick are covered:1.1.1 Grade SW—Brick intended for use where exposed to temperature below freezing in the presence of moisture.NOTE 1: As a typical example, brick used for foundation courses and parapets in the northeastern quarter of the United States should conform to Grade SW.1.1.2 Grade MW—Brick intended for use where exposed to temperature below freezing but unlikely to be saturated with water.NOTE 2: As a typical example, brick exposed in the face of the wall other than parapet or foundations, or brick intended for structures located in regions of the United States characterized by less severe frost action or by drier climate than is found in the northeastern quarter of the United States should conform to Grade MW.1.1.3 When the term brick is used in this specification, it is understood to mean brick or solid masonry units.1.2 If brick having a particular color, texture, finish, or uniformity is desired, these features shall be specified separately by the purchaser.1.3 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.1.4 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 In-vitro osteoblast differentiation assays are one approach to screen progenitor stem cells for their capability to become osteoblasts. The extent of calcium deposits or mineralized matrix that form in vitro may be an indicator of differentiation to a functional osteoblast; however, expression of osteogenic genes or proteins is another important measurement to use in conjunction with this assay to determine the presence of an osteoblast.5.2 This practice provides a technique for staining, imaging, and quantifying the fluorescence intensity and area related to the mineralization in living cell cultures using the non-toxic calcium-chelating dye, XO. The positively stained area of mineralized deposits in cell cultures is an indirect measure of calcium content. It is important to measure the intensity to ensure that the images have not been underexposed or overexposed. Intensity and area do not correlate directly to calcium content.5.3 XO enables the monitoring of calcium deposits repeatedly throughout the life of the culture without detriment to the culture. There is no interference on subsequent measurements of the mineralized area due to dye accumulation from repeated application (1).3 Calcium deposits that have been previously stained may appear brighter, but this does not impact the area measurement. Calcein dyes may also be used for this purpose (1) but require a different procedure for analysis than XO (that is, concentration and filter sets) and are thus not included here. Alizarin Red and Von Kossa are not suitable for use with this procedure on living cultures since there is no documentation supporting their repeated use in living cultures without deleterious effects.5.4 The practice may be applied to cultures of any cells capable of producing calcium deposits. It may also be used to document the absence of mineral in cultures where the goal is to avoid mineralization.5.5 During osteoblast differentiation assays, osteogenic supplements are provided to induce or assist with the differentiation process. If osteogenic supplements are used in excess, a calcium deposit that is not osteoblast-mediated and is referred to as dystrophic, pathologic, or artifactual may occur in the cell cultures (2). For example, when higher concentrations of beta-glycerophosphate are used in the medium to function as a substrate for the enzyme alkaline phosphatase secreted by the cells, there is a marked increase in free phosphate, which then precipitates with Ca++ ions in the media to form calcium phosphate crystals independently of the differentiation status of the progenitor cell. Alkaline phosphatase production is associated with progenitor cell differentiation, and is frequently stimulated by dexamethasone addition to the medium, which enhances the formation of calcium deposits. These kinds of calcium/mineral deposits are thus considered dystrophic, pathologic, or artifactual because they were not initiated by a mature osteoblast. The measurement obtained by using this practice may thus result in a potentially false interpretation of the differentiation status of osteoprogenitor cells if used in isolation without gene or protein expression data (3, 4).5.6 Due to the possibility of artifactual calcium deposits during mineralization assays (2-4), gene expression analysis or protein analysis techniques demonstrating the RNA message or the presence of osteocalcin and bone sialoprotein are recommended for use in conjunction with the calcium deposit quantification procedure described here in order to confirm the presence of mature osteoblasts that are in the process of secreting a mineralizing matrix.5.7 The deposition of a mineralized substance in the culture dish does not confirm that the cells being cultured are capable of forming bone in vivo.5.8 The pattern of mineralized matrix deposition in the culture dish will vary, depending on the number of times the cells have been passaged (that is, first passage primary cells versus cells that have been passaged several times, including cell lines). First passage primary cells typically form relatively large nodules of osteoprogenitor cells that differentiate and mineralize, while cells that have been passaged many times lead to the formation of diffuse, dispersed mineral throughout the culture dish. This practice is independent of the pattern of mineralization and can be used to analyze mineralized matrix in both primary cells and cell lines.5.9 Since some cells proliferate slower than others and since some of the cell culture surfaces being tested may affect proliferation of the cells, the data can be normalized to total cell number. Since reduced proliferation typically reduces mineralization, normalization to cell number typically does not influence the outcomes. Total DNA content can be determined as an indirect measure of cell number. There are several commercially available kits for this purpose. Since DNA analysis is a destructive, toxic assay, additional cell cultures must be prepared if this assay is used.1.1 This practice defines a method for the estimation of calcium content at multiple time points in living cell cultures that have been cultured under conditions known to promote mineralization. The practice involves applying a fluorescent calcium-chelating dye that binds to the calcium phosphate mineral crystals present in the live cultures followed by image analysis of fluorescence microscopy images of the stained cell cultures. Quantification of the positively stained areas provides a relative measure of the calcium content in the cell culture plate. A precise correlation between the image analysis parameters and calcium content is beyond the scope of this practice.1.2 Calcium deposition in a secreted matrix is one of several features that characterize bone formation (in vitro and in vivo), and is therefore a parameter that may indicate bone formation and osteoblast function (that is, osteoblastic differentiation). Calcium deposition may, however, be unrelated to osteoblast differentiation status if extensive cell death occurs in the cell cultures or if high amounts of osteogenic medium components that lead to artifactual calcium-based precipitates are used. Distinguishing between calcium deposition associated with osteoblast-produced mineralized matrix and that from pathological or artifactual deposition requires additional structural and chemical characterization of the mineralized matrix and biological characterization of the cell that is beyond the scope of this practice.1.3 The parameters obtained by image analysis are expressed in relative fluorescence units or area percentage (area%), for example, fraction of coverage of the area analyzed.1.4 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM A495-06(2020) Standard Specification for Calcium-Silicon Alloys Active 发布日期 :  1970-01-01 实施日期 : 

This specification covers a standard grade of calcium-silicon, a standard grade of calcium-manganese-silicon, a standard grade of calcium-silicon-barium and a standard grade of ferro-calcium-silicon. The material shall conform to the requirements as to chemical composition specified.1.1 This specification covers a standard grade of calcium-silicon, a standard grade of calcium-manganese-silicon, a standard grade of calcium-silicon-barium, and a standard grade of ferro-calcium-silicon.1.2 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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A1.3 A1.3.1 This test method provides analytical procedures to determine the major chemical constituents of limestone (see Note 1). The percentages of specific constituents that determine a material’s quality or fitness for use are of significance depending upon the purpose or end use of the material. Results obtained may be used in relation to specification requirements.NOTE A1.1: This test method can be applied to other calcareous materials if provisions are made to compensate for known interferences.AbstractThis specification covers ground calcium carbonate (GCC, a type of ground limestone) and other finely divided aggregate mineral filler (AMF) materials for use in concrete mixtures. It defines the types of GCC and AMF materials for use in concrete. If concrete in service is subject to sulfate exposure, fillers derived from ground limestone should not be used unless mitigation methods are used.1.1 This specification applies to ground calcium carbonate (GCC is a type of ground limestone) and other finely divided aggregate mineral filler (AMF) materials for use in concrete mixtures. The specification defines the types of GCC and AMF materials for use in concrete.1.2 If concrete in service is subject to sulfate exposure, fillers derived from ground limestone should not be used unless mitigation methods are used.NOTE 1: American Concrete Institute (ACI) technical documents 201.2R, 318, 332, and 350 contain useful information and code requirements dealing with sulfate exposure in service. Soluble sulfate in water can be determined in accordance with Test Method D516 or Test Method D4130. Percent sulfate by mass in soil can be determined by Test Method C1580.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.NOTE 2: Sieve size is identified by its standard designation in Specification E11. The alternative designation given in parentheses is for information only and does not represent a different standard sieve size.1.4 The text of this standard references notes and footnotes, which provide explanatory information. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification covers prefaced concrete and calcium silicate masonry units with the exposed-to-view-in-place surfaces are coated with resin, resin and inert filler, or cement and inert filler during manufacture. The coatings are intended to produce smooth resinous tile facing. Facings should be tested according to the prescribed procedures and should meet the requirements for resistance to crazing, cracking, or spalling, resistance to chemicals, adhesion, abrasion, surface-burning characteristics, color, tint, texture, and soiling and cleansability.1.1 This specification covers prefaced concrete and calcium silicate masonry units with the finished face(s) covered at the point of manufacture with resin, resin and inert filler, or cement and inert filler to produce a smooth tile-like surface feature. This specification does not address, and therefore is not applicable to, ground-face concrete masonry units that are manufactured by grinding a thin layer off the surface of a concrete masonry unit to expose aggregates within and polishing to produce a smooth, architectural finish.1.2 The text of this specification references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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