AbstractThese test methods cover the determination of the content of 5-ethylidenenorbornene (ENB) or dicyclopentadiene (DCPD) in ethylene-propylene-diene (EPDM) terpolymers. They are applicable to diene contents in the 0.1 to 10 mass % range. The different apparatus used for testing are presented in details. The methods for the preparation of the test specimen are presented in details. The precision and bias for ENB shall be prepared to meet the requirements prescribed. The precision and bias for DCPD shall be prepared to meet the requirements prescribed.1.1 These test methods cover the determination of the content of 5-ethylidenenorbornene (ENB) or Dicyclopentadiene (DCPD) in ethylene-propylene-diene (EPDM) terpolymers. They are applicable to diene contents in the 0.1 to 10 mass % range.1.2 ENB and DCPD are dienes introduced in ethylene/propylene rubbers to generate specific cure properties. Since high precision for diene content determination has become very important, a Fourier Transform Infrared Spectroscopic (FTIR) method was developed. Diene determination was performed in the past by a refractive index technique.NOTE 1: The procedures for % ENB and % DCPD differ only in the location in the infrared (IR) of the IR peak being quantified.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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1.1 This specification covers alloys of chlorinated ethylene elastomers suitable for injection molding, extrusion, blow molding, thermoforming, and other plastics processing methods.1.2 This specification allows for the use of those TECEA materials that can be recycled, regrounded, and reprocessed, provided that the requirements as stated in this specification are met. The proportions of recycled material used, as well as the nature and amount of any contaminant, however, cannot be covered practically in this specification.1.3 The properties included in this specification are those required to identify the compositions covered. There may be other requirements necessary to identify particular characteristics important to specialized application. These shall be agreed upon between the user and the supplier, by using the suffixes given in Section 5.1.4 The values stated in SI units are to be regarded as the standard. The practices, as detailed in Practice IEEE/ASTM SI 10, are incorporated herein.1.5 The following precautionary caveat pertains only to the test methods portion, Section 10, of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.Note 1--There is no similar or equivalent ISO standard.

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5.1 Presence of paper, metal, or incompatible polymer contamination in poly(ethylene terephthalate) renders the recycled polymer unfit for use in secondary product manufacturing operations. This procedure is useful for identifying different types of contamination in recycled PET flakes.1.1 This practice covers an indication of the quality of recycled transparent poly(ethylene terephthalate) by examination of a wafer or plaque formed by melting a representative sample and quenching it to prevent crystallization.1.2 Specific contaminants and impurities such as aluminum particles, dirt particles, paper, and fibers are identified in the transparent wafer. This method is only limited to contamination observable through visual methods. If there are low levels (0–200 ppm) of certain types of contamination, which are transparent and partially/wholly miscible with PET, they will not be apparent through this method.1.3 The overall color of the plaque is indicative of oxidizable contaminants such as ethylene-vinyl acetate (EVA) glue residue and the number of bubbles present in the plaque gives an indication of the moisture content of the sample.1.4 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 8.NOTE 1: There is no known ISO equivalent to this standard.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This test method covers the determination of ethylene diamine tetraacetate (EDTA) in soaps and synthetic detergents. Throughout this test method EDTA represents the hydrated disodium salt containing 2 moles of H 21.1 This test method covers the determination of ethylene diamine tetraacetate (EDTA) in soaps and synthetic detergents. Throughout this test method EDTA represents the hydrated disodium salt containing 2 moles of H2O. In the chemical literature this is frequently abbreviated to Na2H2Y4 · 2H2O.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Material Safety Data Sheets are available for reagents and materials. Review them for hazards prior to usage.

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4.1 These test methods can be used for determining which EPDM polymers are evaluated in the different compounds in Test Methods D3568.4.2 Differences in ethylene sequence distribution cause differences in crystallinity and green strength at the same ethylene content. Since these are important variables in EPM and EPDM processability and end-use properties, the ethylene content of the rubber should not be used as the sole measurement to determine the suitability of a particular rubber for an intended purpose.1.1 These test methods cover the determination of the proportion of ethylene and propylene units in ethylene-propylene copolymers (EPM) and ethylene-propylenediene terpolymers (EPDM) over the range from 35 to 85 mass % ethylene. Four test methods are needed to encompass the variety of commercial polymers that contain additives or polymerized diene units that interfere with the various infrared peaks. Except when interferences are present, all four test methods should give similar results. The test methods appear in the following order:1.1.1 Pressed Film Test Methods:   SectionsTest Method A—For EPM and EPDM between 35 and 70 mass % ethylene  9 – 14Test Method B—For EPM and EPDM between 60 and 85 mass % ethylene, except for ethylene/propylene/1,4-hexadiene terpolymers 15 – 19Test Method C—For all EPM and EPDM polymers between 35 and 85 mass % ethylene, using near infrared 20 – 241.1.2 Cast Film Test Methods:Test Method D—For all EPM and EPDM polymers between 35 and 85 mass % ethylene, except for ethylene/propylene/1,4-hexadiene terpolymers 25 – 321.2 These test methods are not applicable to oil-extended EPDM unless the oil is first removed in accordance with Test Method D.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This standard provides guidance to obtain data that is the most representative of the material’s characteristics and performance. To properly evaluate EPDM, tests should be performed in accordance with specific test methods and procedures.1.1 This guide covers and provides recommendations for the selection of appropriate test methods for Ethylene Propylene Diene Terpolymer (EPDM) geomembranes used in geotechnical and geoenvironmental applications.1.2 This guide includes test methods for three different types of EPDM geomembranes including: scrim-reinforced membranes, composite membranes, and smooth, nonreinforced membranes.1.3 The test methods are divided into three categories including manufacturing quality control, optional performance tests, and seam testing.1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This test method covers the determination of ethylene oxide content in polyethoxylated nonionic surfactants. It can also be used for compounds containing propylene oxide or any compounds (glycols and glycol and polyglycol ethers and esters) which form unstable 1,2-diiodides on reaction with hydroiodic acid. The apparatus is comprised of the following: heat source which shall be an electric heater provided with a sliding rheostat or other means of heat control; flasks which shall be equipped with a standard ground-glass joint; condensers with standard joints; gas bubbler filled with dibutyl phthalate; buret; and pipet. The dual apparatus is designed to permit a sample and a blank to be run simultaneously. Reagent grade chemicals or reagents of sufficiently high purity including water, carbon dioxide or nitrogen, lubricant, dibutyl phthalate, glass beads, hydroiodic acid, hydrochloric acid, methanol, potassium dichromate, potassium iodide solution, sodium thiosulfate, and starch indicator solution shall be used in all tests. The ethylene oxide content shall be calculated from the amount of sodium thiosulfate solution required to titrate the sample and the blank, normality of sodium thiosulfate, and weight of the sample. Standard deviations for repeatability and reproducibility shall be estimated to determine the acceptability of the results.1.1 This test method covers the determination of ethylene oxide in polyethoxylated nonionic surfactants. It can also be used for compounds containing propylene oxide or any compounds (glycols and glycol and polyglycol ethers and esters) which form unstable 1,2-diiodides on reaction with hydriodic acid.NOTE 1: Compounds in which the oxyalkylene group is connected to a nitrogen cannot be entirely decomposed. This can be used to determine the percent of an ethoxylated surfactant in a mixture, if the ethylene oxide content of the ethoxylated surfactant is known.NOTE 2: This method reports results as percent ethylene oxide. If this method is applied to unknown compounds or compositions, the analyst should be aware of the possible presence of material other than ethylene oxide.NOTE 3: For use on built syndet compositions the organic active ingredient must be isolated in accordance with Test Method D2358.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Material Safety Data Sheets are available for reagents and materials. Review them for hazards prior to usage.

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4.1 High-purity ethylene is required as a feedstock for some manufacturing processes, and the presence of trace amounts of carbon dioxide and some hydrocarbons can have deleterious effects. This method is suitable for setting specifications, for use as an internal quality control tool and for use in development or research work.1.1 This test method covers the determination of carbon dioxide, methane, ethane, acetylene, and other hydrocarbons in high-purity ethylene. Hydrogen, nitrogen, oxygen, and carbon monoxide are determined in accordance with Test Method D2504. The percent ethylene is obtained by subtracting the sum of the percentages of the hydrocarbon and nonhydrocarbon impurities from 100. The method is applicable over the range of impurities from 1 to 500 parts per million volume (ppmV).1.2  This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For some specific hazard statements, see Section 6.1.3 The values stated in SI units are to be regarded as the standard. The values in parentheses are for information only.

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This specification covers a general classification system for crosslinkable ethylene plastics compounds. Two types of compounds are covered, namely, mechanical types in which mechanical strength properties are of prime importance in applications, and electrical types in which electrical insulating or conducting properties also are of prime importance in applications. These compounds shall be classified as: Type I; Type II; and Grade A. Tests shall be performed to determine the properties in accordance with the following test methods: conditioning; test conditions; ultimate elongation; elongation retention after aging; apparent modulus of rigidity; brittleness temperature; dielectric constant; dissipation factor; and degree of crosslinking.1.1 This specification covers a general classification system for crosslinkable ethylene plastics compounds (Note 1). The requirements specified herein are not necessarily applicable for use as criteria in determining suitability for the end use of a fabricated product.NOTE 1: It is to be noted that this specification describes materials that are available commercially in their uncrosslinked form. Therefore, they are crosslinkable compounds despite the fact that measurement of the parameters used for their classification and specification will usually be carried out after curing has been effected.1.2 Two types of compounds are covered, namely, mechanical types in which mechanical strength properties are of prime importance in applications, and electrical types in which electrical insulating or conducting properties also are of prime importance in applications.1.3 The parameters used to classify and specify the mechanical types are ultimate elongation, elongation retention after aging, apparent modulus of rigidity, and brittleness temperature.1.4 The parameters used to classify and specify the electrical types are ultimate elongation, elongation retention after aging, apparent modulus of rigidity, brittleness temperature, dielectric constant, dissipation factor, and volume resistivity.1.5 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.6 The following safety hazards caveat pertains only to the test methods portion, Section 7, of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.NOTE 2: There is no known ISO equivalent to this standard.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Ethylene oxide is a major industrial chemical with production volume ranked in the top 25 chemicals produced in the United States. It is used in the manufacture of a great variety of products as well as being a sterilizing agent and fumigant.5.2 This test method provides a means of determining exposure levels of ETO in the working environment at the presently recommended exposure guidelines.5.2.1 OSHA Permissible Exposure Limit (PEL) 1 ppm, 15-min excursion limit 5 ppm (CFR, Part 1910, Subpart Z, Section 1910.1047).35.2.2 ACGIH Threshold Limit Value (TLV) 1 ppm (1.8 mg/m3), suspected human carcinogen.41.1 This test method covers a method of collecting and analyzing samples to determine the amount of ethylene oxide (ETO) present in workplace atmospheres.1.2 This test method can be used to provide a time-weighted average (TWA) over the concentration range from 0.2 to 4 ppm (v).1.3 This test method can be used to determine 15-min excursions (STEL) ranging from 1 to 25 ppm (v).1.4 The values stated in SI units are to be regarded as the standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See Section 9 for specific safety hazards.

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5.1 Rock for erosion control consists of individual pieces of natural quarried stone or large boulders and cobbles. The ability of these individual pieces of stone to resist deterioration due to weathering action affects the stability of the integral placement of rock for erosion control and hence, the stability of construction projects, structures, shorelines, and stream banks.5.2 Deterioration of stone in this test is one indicator that similar samples exposed to wet/dry and freeze/thaw cycles may break down in a water-soaked environment condition in service.5.3 This test method was developed to be used in conjunction with additional test methods listed in Practice D4992. This test method provides a quantitative value indicating potential resistance to weathering; however, the results of this test method are not to be used as the sole basis for the determination of rock durability.NOTE 1: The quality of the result produced by this standard is dependent upon the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluation some of those factors.1.1 This test method covers the testing for and quantitative determination of the presence of swelling clays of the smectite group in rock for erosion control. The test particles are intended to be representative of erosion control rock and its durability. The test is appropriate for breakwater stone, armor stone, riprap and gabion sized rock materials.1.2 Ethylene glycol is one of the materials that react with swelling clays to form an organoclay complex having a larger basal spacing than that of the clay mineral itself. Rock containing swelling clay of the smectite group will be expected to undergo expansive breakdown upon soaking in ethylene glycol. If the amount, distribution, state of expansion, and ability to take up glycol is such as to cause such breakdown to occur, it may be expected that similar breakdown may occur of similar rock samples exposed, for longer times, to wetting and drying or freezing and thawing in a water-soaked condition in service.1.3 The prepared size of the rock specimens may eliminate some of the internal features present in the gross structure. The test specimens may not be representative of the quality of the larger rock samples used in construction. Careful examination of the rock source and proper sampling are essential in minimizing this limitation.1.3.1 The test is time intensive and requires over two weeks to complete the sample preparation, testing and analysis portions of the procedure.1.4 The use of reclaimed concrete and materials other than natural rock is beyond the scope of this test method.1.5 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard. Reporting of test results in units other than SI shall not be regarded as nonconformance with this standard.1.5.1 The gravitational system of inch-pound units is used when dealing with inch-pound units. In this system, the pound (lbf) represents a unit of force (weight), while the unit for mass is slugs. The slug unit is not given unless dynamic (F=ma) calculations are involved.1.5.2 The SI units presented for apparatus are substitutions of the inch-pound units, other similar SI units should be acceptable providing they meet the technical requirements established by the inch-pound apparatus.1.5.3 It is common practice in the engineering/construction profession to concurrently use pounds to represent both a unit of mass (lbm) and force (lbf). This practice implicitly combines two separate systems of units: the absolute and the gravitational systems. It is scientifically undesirable to combine the use of two separate sets of inch-pound units within a single standard. As stated, this standard includes the gravitational system of inch-pound units and does not use/present the slug unit for mass. However, the use of balances or scales recording pounds of mass (lbm) or recording density in lbm/ft3 shall not be regarded as nonconformance with this standard.1.5.4 Calculations are done using only one set of units; either SI or gravitational inch pound. Other units are permissible provided appropriate conversion factors are used to maintain consistency of units throughout the calculations, and similar significant digits or resolution, or both are maintained.1.6 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026, unless superseded by this standard.1.6.1 For purposes of comparing measured or calculated value(s) with specified limits, the measured or calculated value(s) shall be rounded to the nearest decimal or significant digits in the specified limits.1.6.2 The procedures used to specify how data are collected/recorded or calculated, in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analytical methods for engineering design.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 DPGBE and EGBE have a variety of residential and industrial applications such as cleaning formulations, surface coatings, inks, and cosmetics. These analytes may be released into the environment at levels that may be harmful to aquatic life.5.2 This test method has been investigated for use with reagent and sea water.1.1 This test method covers the determination of dipropylene glycol monobutyl ether (DPGBE) and ethylene glycol monobutyl ether (EGBE) in sea water by direct injection using liquid chromatography (LC) and detection with tandem mass spectrometry (MS/MS). These analytes are qualitatively and quantitatively determined by this test method. This test method adheres to selected reaction monitoring (SRM) mass spectrometry.1.2 The detection verification level (DVL) and reporting range for DPGBE and EGBE are listed in Table 1.1.2.1 The DVL is required to be at a concentration at least 3 times below the reporting limit (RL) and have a signal/noise ratio greater than 3:1. Fig. 1 and Fig. 2 display the signal/noise ratio of the single reaction monitoring (SRM) transition.FIG. 1 Detection Verification Level Signal/Noise RatioFIG. 2 Reporting Level (Calibration Standard) Signal/Noise Ratio1.2.2 The reporting limit is the concentration of the Level 1 calibration standard as shown in Table 4 for DPGBE and EGBE, taking into account the 20 % sample preparation dilution factor.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Separation and identification of stabilizers used in the manufacture of polyethylene are necessary in order to correlate performance properties with polymer composition.5.2 The BHT extraction procedure is made effective by the insolubility of the polymer sample in solvents generally used for gas chromatographic analysis.1.1 This test method describes a procedure for the determination of butylated hydroxy toluene (BHT) (2,6-di-t-butyl-4-methyl-hydroxybenzene) in polymers of ethylene and ethylene-vinyl acetate (EVA) copolymers by solvent extraction followed by gas chromatographic analysis. Detection of the compound is achieved by flame ionization, and quantitative analysis is obtained by use of internal or external standards, as described in Practices E260, E355, and E594.1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 9.NOTE 1: There is no known ISO equivalent for this test method.

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1.1 This specification covers the requirements for a prediluted aqueous ethylene glycol base low-silicate engine coolant (50 volume percent minimum) for cooling systems of heavy-duty engines. When used without further dilution, this product will function effectively during both summer and winter to provide protection from corrosion, freezing at least to -36.7°C (-34.0°F), and boiling at least to 108°C (226°F). 1.2 Prediluted coolant meeting this specification requires both an initial charge of a supplemental coolant additive (SCA) and regular maintenance doses of an SCA to continue the protection in certain operating heavy-duty engine cooling systems, particularly those of the wet cylinder liner-in-block design. The SCA additions are defined by and are the primary responsibility of the engine or vehicle manufacturer. If they provide no instructions, follow the SCA supplier's recommended instructions. 1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

定价： 0元 / 折扣价： 0 元

1.1 This specification covers flexible sheet made from ethylene propylene diene terpolymer (EPDM) geomembrane intended for use in geotechnical and geoenvironmental applications. The tests and property limits used to characterize the sheet are values to ensure minimum quality for the intended use. The vulcanized rubber sheet may be non-reinforced, fabric or scrim reinforced.1.2 In-place geomembrane design criteria, such as field seaming strength and material compatibility, among others, are factors that must be considered but are beyond the scope of this specification.1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价： 590元 / 折扣价： 502 元 加购物车