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4.1 This guide is an educational tool for tank owners, operators, and other users and is not intended for use in certifying compliance with the Federal technical standards for underground storage tanks.4.2 The intent of this guide is to provide an overview of the general requirements. This guide is intended for users who are generally familiar with the requirements of 40 CFR Part 280. The user is advised that this guide does not contain the level of detail necessary to make the determination of whether specific equipment or services meet the detailed technical performance requirements of 40 CFR Part 280.4.3 This guide does not cover state and local requirements, that can be more stringent than the federal rules. Owners and operators are responsible for meeting federal, state, and, in some circumstances, local requirements. It is recommended that owners and operators familiarize themselves with these requirements as well.4.4 Owners or operators may use the sample checklist in Appendix X1 to assist them in determining operational conformance or they may develop their own checklist based upon this guide.4.5 This guide and accompanying appendixes are not intended to be used by state or local UST program authorities as a regulatory or administrative requirement for owners or operators. Use of this guide and appendixes by owners and operators is intended to be a voluntary educational tool for the purposes described in 4.1.1.1 This guide covers information for evaluating tank systems for operational conformance with the Federal technical standards (including the financial responsibility requirements) for underground storage tanks (USTs) found at 40 Code of Federal Register (CFR) Part 280.1.2 This guide does not address the corrective action requirements of 40 CFR Part 280.1.3 To the extent that a tank system is excluded or deferred from the federal regulations under Subpart A of 40 CFR Part 280, it is not covered by this guide.1.4 Local regulations may be more stringent than federal regulation and the reader should refer to the implementing agency to determine compliance.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Continuous opacity monitors are required to be installed at many stationary sources of air pollution by federal, state, and local air pollution control agency regulations. EPA regulations regarding the design and performance of opacity monitoring systems for sources subject to “Standards of Performance for New Stationary Sources” are found in 40 CFR 60, Subpart A General Provisions, §60.13 Monitoring Provisions, Appendix B, Performance Specification 1, and in applicable source-specific subparts. Many states have adopted these or very similar requirements for opacity monitoring systems.5.2 Regulated industrial facilities are required to report continuous opacity monitoring data to control agencies on a periodic basis. The control agencies use the data as an indirect measure of particulate emission levels and as an indicator of the adequacy of process and control equipment operation and maintenance practices.5.3 EPA Performance Specification 1 provides minimum specifications for opacity monitors and requires source owners or operators of regulated facilities to demonstrate that their installed systems meet certain design and performance specifications. Performance Specification 1 adopts this ASTM practice by reference so that manufacturers can demonstrate conformance with certain design specifications by selecting and testing representative instruments.5.4 Experience demonstrated that EPA Performance Specification 1 prior to the Aug. 10, 2000 revisions did not address all of the important design and performance parameters for opacity monitoring systems. The additional design and performance specifications included in this practice are needed to eliminate many of the performance problems that were previously encountered. This practice also provides purchasers and vendors flexibility, by designing the test procedures for basic transmissometer components or opacity monitors, or in certain cases, complete opacity monitoring systems. However, the specifications and test procedures are also sufficiently detailed to support the manufacturer’s certification and to facilitate independent third party evaluations of the procedures used.5.5 Purchasers of opacity monitoring equipment meeting all of the requirements of this practice are assured that the opacity monitoring equipment meets all of the applicable requirements of EPA Performance Specification 1 for which the manufacturer can certify conformance. Purchasers can rely on the manufacturer’s published operating range specifications for ambient temperature and supply voltage. These purchasers are also assured that the specific instrument has been tested at the point of manufacture and demonstrated to meet the manufacturer’s performance specifications for instrument response time, calibration error (based on pathlength measurements provided by the end user), optical alignment, and the spectral response performance check requirement. Conformance with the requirements of this practice ensures conformance with all of the requirements of 40 CFR 60, Appendix B, Performance Specification 1 except those requirements for which tests are required after installation.5.6 The original manufacturer, or those involved in the repair, remanufacture, or resale of opacity monitors can use this practice to demonstrate that the equipment components or opacity monitoring systems provided meet, or exceed, or both, appropriate design and performance specifications.5.7 The applicable test procedures and specifications of this practice are selected to address the equipment and activities that are within the control of the manufacturer; they do not mandate testing of the opacity system data recording equipment or reporting.5.8 This practice also may serve as the basis for third party independent audits of the certification procedures used by manufacturers of opacity monitoring equipment.5.9 This practice does not address ongoing quality assurance procedures which are needed to maintain correct operation during the lifetime of the opacity monitor.1.1 This practice covers the procedure for certifying continuous opacity monitors. In the main part of this practice, it includes design and performance specifications, test procedures, and quality assurance requirements to ensure that continuous opacity monitors meet minimum design and calibration requirements, necessary in part, for accurate opacity monitoring measurements in regulatory environmental opacity monitoring applications subject to 10 % or higher opacity standards. In Annex A1, additional or alternative specifications are provided for certifying opacity monitors intended for use in applications where the opacity standard is less than 10 %, or where the user expects the opacity to be less than 10 % and elects to use the more restrictive criteria in Annex A1. In both cases, the error budgets for the opacity measurements are given in Appendix X1.1.2 This practice applies specifically to the original manufacturer, or to those involved in the repair, remanufacture, or resale of opacity monitors.1.3 Test procedures that specifically apply to the various equipment configurations of component equipment that comprise either a transmissometer, an opacity monitor, or complete opacity monitoring system are detailed in this practice.1.4 The specifications and test procedures contained in the main part of this practice have been adopted by reference by the United States Environmental Protection Agency (U.S. EPA). For each opacity monitor or monitoring system that the manufacturer demonstrates conformance to this practice, the manufacturer may issue a certificate that states that opacity monitor or monitoring system conforms with all of the applicable design and performance requirements of 40 CFR 60, Appendix B, Performance Specification 1 except those for which tests are required after installation.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This practice is intended solely for the evaluation of metallic-coated, painted metallic-coated, and painted nonmetallic-coated materials used for the manufacture of cold formed framing members.5.2 Correlation and extrapolation of corrosion performance based on exposure to the test environment provided by Practice B117 are not always predictable. Correlation and extrapolation should be considered only in cases where appropriate corroborating long-term atmospheric exposures have been conducted.5.3 This practice assesses whether coated materials not currently in Specification A1003/A1003M satisfy the required minimum corrosion characteristics.1.1 This practice covers procedures for establishing the acceptability of metallic-coated steel sheet, painted metallic-coated steel sheet, and painted nonmetallic-coated steel sheet for use as cold formed framing members.1.2 This practice shall be used to assess the corrosion resistance of different coatings on steel sheet in a laboratory test. It shall not be used as an application performance standard for the cold formed framing members.1.3 The practice shall be used to evaluate coatings under consideration for addition to Specification A1003/A1003M.1.4 The values stated in either inch-pound or SI units are to be regarded separately as standard. Within the text, the SI units are shown in brackets. The values stated in each system are not exact equivalents; therefore, each system must be used independently of the other.1.5 The text of this standard references notes and footnotes that provide explanatory material. These notes and footnotes, excluding those in tables and figures, shall not be considered as requirements of the standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This practice is intended to assist the various technical committees in the use of uniform methods of indicating the number of digits which are to be considered significant in specification limits, for example, specified maximum values and specified minimum values. This practice is also intended to be used in determining conformance with specifications when the applicable ASTM specifications or standards make a direct reference.1.1 This practice is intended to assist the various technical committees in the use of uniform methods of indicating the number of digits which are to be considered significant in specification limits, for example, specified maximum values and specified minimum values. Its aim is to outline methods which should aid in clarifying the intended meaning of specification limits with which observed values or calculated test results are compared in determining conformance with specifications.1.2 This practice is intended to be used in determining conformance with specifications when the applicable ASTM specifications or standards make direct reference to this practice.1.3 Reference to this practice is valid only when a choice of method has been indicated, that is, either absolute method or rounding method.1.4 The system of units for this practice is not specified. Dimensional quantities in the practice are presented only as illustrations of calculation methods. The examples are not binding on products or test methods treated.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This practice provides a means by which the purchaser can determine the conformance of geosynthetic properties as applied to the acceptance or rejection of a material in regards to a material specification.4.2 This practice has been developed with strong emphasis on practicality and the realization that all geosynthetics are subjected to a vigorous quality control program prior to shipping.NOTE 1: It is suggested that the user obtain the mean, standard deviation, and/or the coefficient of variation for given physical/mechanical properties of a product directly from the manufacturer. If this data is unavailable, it is suggested that users of this practice begin to accumulate data that can be used to estimate product averages and standard deviations for each product.NOTE 2: The risk to the purchaser of buying out-of-specification materials is minimal when conformance requirements are detailed in the purchase specification and adequate conformance testing is performed. It is the producer's responsibility to perform thorough quality control testing for all properties requiring certification. The producer's risk of rejection is minimal with the performance of this thorough quality control testing.1.1 This practice covers a procedure for determining the conformance of geosynthetic properties to standard specifications.1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 EPA regulations require Portland cement plants that burn hazardous waste to use BLDs or PMDs to provide either a relative or an absolute indication of PM concentration and to alert the plant operator of the need to inspect PM control equipment or initiate corrective action. EPA and others have not established for these applications specific design and performance specifications for these instruments. The design and performance specifications and test procedures contained in this practice will help ensure that measurement systems are capable of providing reliable monitoring data.5.2 This practice identifies relevant information and operational characteristics of BLD and PMD monitoring devices for Portland cement kiln systems. This practice will assist equipment suppliers and users in the evaluation and selection of appropriate monitoring equipment.5.3 This practice requires that tests be conducted to verify manufacturer’s published specifications for detection limit, linearity, thermal stability, insensitivity to supply voltage variations and other factors so that purchasers can rely on the manufacturer’s published specifications. Purchasers are also assured that the specific instrument has been tested at the point of manufacture and shown to meet selected design and performance specifications prior to shipment.5.4 This practice requires that the manufacturer develop and provide to the user written procedures for installation start-up, operation, maintenance, and quality assurance of the equipment. This practice requires that these same procedures are used for a field performance demonstration of the BLD or PMD monitoring equipment at a Portland cement plant.5.5 The applicable test procedures and specifications of this practice are selected to address the equipment and activities that are within the control of the manufacturer.5.6 This practice also may serve as the basis for third party independent audits of the certification procedures used by manufacturers of PMD or BLD equipment.1.1 This practice covers the procedure for certifying particulate matter detectors (PMDs) and bag leak detectors (BLDs) that are used to monitor particulate matter (PM) emissions from kiln systems at Portland cement plants that burn hazardous waste. It includes design specifications, performance specifications, test procedures, and information requirements to ensure that these continuous monitors meet minimum requirements, necessary in part, to monitor reliably PM concentrations to indicate the need for inspection or corrective action of the types of air pollution control devices that are used at Portland cement plants that burn hazardous waste.1.2 This practice applies specifically to the original manufacturer, or to those involved in the repair, remanufacture, or resale of PMDs or BLDs.1.3 This practice applies to (a) wet or dry process cement kilns equipped with electrostatic precipitators, and (b) dry process kilns, including pre-heater pre-calciner kiln systems, equipped with fabric filter controls. Some types of monitoring instruments are suitable for only certain types of applications.NOTE 1: This practice has been developed based on careful consideration of the nature and variability of PM concentrations, effluent conditions, and the type, configuration, and operating characteristics of air pollution control devices used at Portland cement plants that burn hazardous waste.1.4 This practice applies to Portland cement kiln systems subject to PM emission standards contained in 40 CFR 63, Subpart EEE.NOTE 2: The level of the PM emission limit is relevant to the design and selection of appropriate PMD and BLD instrumentation. The current promulgated PM emission standards (70 FR 59402, Oct. 12, 2005) are: (a) 65 mg/dscm at 7 % O2 (0.028 gr/dscf at 7 % O2) or approximately 30 mg/acm (0.013 gr/acf) for “existing sources” and (b) 5.3 mg/dscm at 7 % O2 (0.0023 gr/dscf at 7 % O2) or approximately 2.5 mg/acm (0.001 gr/acf) for “new sources.” On March 23, 2006 (71 FR 14665), EPA proposed to revise the PM standard for new cement plants to 15.9 mg/dscm at 7 % O2 (0.0069 gr/dscf at 7 % O2), or about 6–9 mg/acm (0.0026–0.0039 gr/acf). The emission standards may change in future rulemakings, so users of this practice should check the current regulations. Some types of monitoring instruments are not suitable for use over the range of emissions encountered at both new and existing sources.1.5 The specifications and test procedures contained in this practice exceed those of the United States Environmental Protection Agency (USEPA). For each monitoring device that the manufacturer demonstrates conformance to this practice, the manufacturer may issue a certificate that states that monitoring device conforms with all of the applicable design and performance requirements of this practice and also meets all applicable requirements for PMDs or BLDs at 40 CFR 63, Subpart EEE, which apply to Portland cement plants.NOTE 3: 40 CFR 63.1206 (c)(8) and (9) requires that BLDs and PMDs “be certified by the manufacturer to be capable of detecting particulate matter emissions at concentrations of 1.0 milligrams per actual cubic meter unless you demonstrate under §63.1209(g), that a higher detection limit would routinely detect particulate matter loadings during normal operations.” This practice includes specific procedures for determination and reporting of the detection limit for each PMD or BLD model.1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This practice provides a means whereby the parties can resolve disputes over specification conformance for those product properties which can be tested and expressed numerically.4.1.1 This practice can be used to ensure that such properties are correctly stated on labels or in other descriptions of the product.4.1.2 This practice can be implemented in those cases where a supplier uses an in-house or a commercial testing laboratory to sample and test a product prior to releasing the product to a shipper (intermediate receiver) and the ultimate receiver also uses an in-house or commercial testing laboratory to sample and test the product upon arrival at the destination. The ATV would still be determined according to 8.3.4.2 This practice can be applied in the determination of tolerances from specification limits based on a mutually agreed probability between parties for making the conformance to specification decision if the true value of a property is sufficiently close to the specification limit. Such tolerances are bounded by an acceptance limit (AL). If the ATV value determined by applying this practice falls on the AL or on the acceptable side of the AL, the product property can be considered to have met the specification; otherwise it shall be considered to have failed to meet the specification.4.3 Application of this practice requires the AL be determined prior to actual commencement of testing. Therefore, the degree of criticality of the specification, as determined by the Probability of Acceptance (P value) that is required to calculate the AL, shall have been mutually agreed upon between both parties prior to execution of actual product testing.4.3.1 This agreement should include a decision as to whether the ATV is to be determined by the absolute or rounding-off method of Practice E29, as therein defined.4.3.1.1 If the rounding-off method is to be used, the number of significant digits to be retained must also be agreed upon.4.3.1.2 These decisions must also be made in the case where only one party is involved, as in the case of a label.4.3.1.3 In the absence of such an agreement, this practice recommends the ATV be rounded in accordance with the rounding-off method in Practice E29 to the number of significant digits that are specified in the governing specification.4.4 This practice is designed to be suitable for reference in contracts governing the transfer of petroleum products and lubricants from a supplier to a receiver.4.5 As a prerequisite for acceptance for lab test results to be used in this practice, the following conditions shall be satisfied:4.5.1 Site precision (R′) as defined in Practice D6299 for the appropriate test method(s) from each lab, as substantiated by control charts meeting the requirement of D6299 from in-house quality control programs, for property typical of the product in dispute, should have a TPI > 1.2 for methods with Precision Ratio <4 and TPI > 2.4 for methods with Precision Ratio ≥4 (see Practice D6792 for TPI explanation).4.5.2 Each lab shall be able to demonstrate, by way of results from interlaboratory exchange programs, a lack of a systemic bias relative to exchange averages for the appropriate test method(s) as per methodology outlined in Guide D7372.4.5.3 In the event that the site precision of laboratories from two parties are statistically different as confirmed by the F-test (see Annex A4), then, for the purpose of establishing the ATV, each laboratory's test result shall be inversely weighted in accordance with laboratory's demonstrated variance.4.6 It is recommended that this practice be conducted under the guidance of a qualified statistician.1.1 This practice covers guidelines and statistical methodologies with which two parties (see Note 1) can compare and combine independently obtained test results to obtain an Assigned Test Value (ATV) for the purpose of resolving a dispute over product property conformance with specification.NOTE 1: Application of this practice is usually, but not limited to, between supplier and receiver of a product.1.2 This practice defines a technique for establishing an Acceptance Limit (AL) and Assigned Test Value (ATV) to resolve the dispute over a property conformance with specification by comparing the ATV to the AL.1.3 This practice applies only to those test methods which specifically state that the repeatability and reproducibility values conform to the definitions herein.1.4 The statistical principles and methodology outlined in this practice can also be used to obtain an ATV for specification conformance decision when multiple results are obtained for the same batch of product within a single laboratory. For this application, site precision (R') as defined in Practice D6299 shall be used in lieu of test method published reproducibility (R).1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D5063-90(2012) Standard Guide for Use of Certification of Coating Conformance Form (Withdrawn 2021) Withdrawn, No replacement 发布日期 :  1970-01-01 实施日期 : 

This guide for certification of coating conformance form provides procurement information concerning products being furnished in accordance with a specific coating specification and additional requirements contained in the purchase order. The certification form is divided into four headings: General Type and Description(I), Buyer Information(II), Seller Information (III), and Certification (IV). The first heading consists of the following information: generic type, manufacturer's designation, specification number, formula number, component number, component identification, and color. The second heading consists purchase order number, release number, part number, item number, and stock number. The third heading consists of seller's representative, batch number, lot number, date of manufacture, and date of certification expiration. The last heading is a paragraph describing the certification.1.1 This certification of coating conformance form provides procurement information concerning products being furnished in accordance with a specific coating specification and additional requirements contained in the purchase order (see Fig. 1).CERTIFICATION OF COATING CONFORMANCE FORM Number:Date:I. GENERAL TYPE AND DESCRIPTION: Generic Type: Manufacturer's Designation: Specification Number: Formula Number: Number of Components: Component Identification (if applicable): Color:II. BUYER INFORMATION: Name and Address: Purchase Order Number: Release Number (if applicable): Part Number (if applicable): Item Number (if applicable): Stock Number (if applicable):III. SELLER INFORMATION: Name and Address: Seller's Representative: (Include Telephone Number) Batch Number: Lot No.: Date of Manufacture: Date of Expiration of Certification:IV. CERTIFICATION:This is to certify that the above material being furnished has been manufactured in accordance with the specification and meets all specification requirements contained in the above purchase order. NAME AND TITLE SIGNATURE DATEFIG. 1 Certification Form1.2 The completed form can be utilized to help evaluate the acceptability of the paint being furnished.

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5.1 This test method demonstrates conformity of a dynamic mechanical analyzer at an isothermal temperature of 21 °C.5.2 Dynamic mechanical analysis experiments often use linear temperature change. This test method does not address the effect of that change in temperature on the loss modulus.5.3 This test method may be used in research and development, specification acceptance, and quality control or assurance.1.1 This test method describes the performance confirmation or measurement of conformance for the loss modulus scale of a commercial or custom-built dynamic mechanical analyzer (DMA) at 21 °C using ultra-high molecular weight polyethylene as a reference material.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 The dimensional, shape, and surface tolerances of rock core test specimens are important for determining rock properties of intact specimens. This is especially true for strong rocks, greater than 7250 psi (50 MPa) and for rock specimens that will be tested in stiff testing load frames without a spherical seat where non-uniform loading could occur. Dimensional and surface tolerance checks are required in the test methods listed in Section 2.1. To simplify test procedures in laboratories, the parts of those procedures that are common to the test methods in Section 2.1 are given in this standard.4.2 This procedure is applicable to all the standards listed in Section 2.1; however, specimens for Test Method D2936 do not need to be machined or to meet the specified tolerances for flatness and parallelism.4.3 The moisture condition of the specimen at the time of the sample preparation can have a significant effect upon the strength and deformation characteristics of the rock. Good practice generally dictates that laboratory tests be made upon a specimens’ representative of field conditions. Thus, it follows that the field moisture condition of the specimen should be preserved until the time of the test. In some instances, however, there may be reasons for testing specimens at other moisture contents, from saturation to dry. In any case, the moisture content of the test specimen should be tailored to the problem at hand.NOTE 3: Discussions on moisture content are common in many rock testing standards but professional judgement will be needed to both handle and report this issue. For example, when obtaining the samples or preparing the specimens, water or some other cooling agent may be required or used. Therefore, the moisture in the specimen or samples may not be what it was in situ; this applies to both water chemistry and quantity of fluids. This issue should be addressed, and a plan put in place for each step from the sampling to the testing phase in a manner that records/reports what steps were advised to successfully prepare testable samples. Usually a compromise between preserving in-situ conditions, costs, conditions outside the control of the laboratory and obtaining testable specimens is required. For example, loss of moisture that leads to the samples or specimens falling apart may be of greater concern than testing with in situ water or at the in situ water content or both.4.4 Excess moisture will affect the adhesion of resistance strain gages, if used, and the accuracy of their performance. Adhesives used to bond the rock to steel end caps and fixtures for attaching specimens to actuators and crosshead of the load frame in the direct tension test (D2936) will also be affected adversely by excess moisture.NOTE 4: The quality of the result produced by these practices is dependent upon the competence of the personnel performing it and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing and sampling. Users of these practices are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.1.1 These practices specify procedures for preparing rock test specimen of rock core from drill core obtained in the field or from block samples for strength and deformation testing and for determining the conformance of the test specimen dimensions with tolerances established by this practice. Cubical, rectangular, or other shapes are not covered by this practice. However, some of the information contained within this practice and in standard Test Method C170 may still be of use to preparing other test specimen shapes.1.2 Rock is a complex engineering material that can vary greatly as a function of lithology, stress history, weathering, moisture content and chemistry, and other natural geologic processes. As such, it is not always possible to obtain or prepare rock core specimens that satisfy the desirable tolerances given in this practice. Most commonly, this situation presents itself with weaker, more porous, and poorly cemented rock types and rock types containing significant or weak (or both) structural features. For rock types which are difficult to prepare, all reasonable efforts should be made to prepare a specimen in accordance with this practice and for the intended test procedure. However, when it has been determined by trial and error that this is not possible, prepare the rock specimen to the closest tolerances practicable and consider this to be the best effort (Note 1) and report it as such and if allowable or necessary for the intended test, capping the ends of the specimen as discussed in this practice is permitted.NOTE 1: Best effort in surface preparation refers to the use of a well-maintained, suitable surface grinder, lathe or lapping machine and any required ancillary equipment are utilized by an experienced operator and in which a reasonable number of attempts has been made to meet the tolerances required in this procedure.1.3 This practices covers some, but not all of the curatorial issues that should be implemented. For curatorial issues that should be followed before and during specimen preparation refer to Practices D5079 and to the specific test standards in 2.1 for which the specimens are being prepared.1.4 This practice also prescribes tolerance checks on the length-to-diameter ratio, straightness of the elements on the cylindrical surface, the flatness of the end bearing surfaces, and the perpendicularity of the end surfaces with the axis of the core.NOTE 2: This practice does not purport to cover all the issues that will or could be encountered that may control the quality of the specimen preparation required. Each laboratory may have their own issues, especially for different compression load frames or rock types. For example, stiff testing frames versus traditional load frames and loading platens with or without spherical seating. Specimens for a stiff testing load frame with no spherical seat may need to have more stringent requirements depending on the type of rock being tested. This procedure has tried to show the methods and QA that may be involved while keeping in mind those materials that are difficult to work with and for which the specimens will still be suitable to be tested. The available literature and input on this subject from D18.12 members were considered as much as possible for this standard.21.5 The requirement for specifying the moisture condition and volume of the test specimen is also stated. However, the requirements in the specific test standards in 2.1 should be followed too.1.6 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026, unless superseded by this standard.1.6.1 The practices/procedures used to specify how data are collected/recorded and calculated in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analysis methods for engineering design.1.7 Units—The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard. Add if appropriate, “Reporting of test results in units other than inch-pound shall not be regarded as nonconformance with this standard.”1.7.1 The slug unit of mass is typically not used in commercial practice; that is, density, balances, and so on. Therefore, the standard unit for mass in this standard is either kilogram (kg) or gram (g) or both. Also, the equivalent inch-pound unit (slug) is not given/presented in parentheses.1.7.2 It is common practice in the engineering/construction profession to concurrently use pounds to represent both a unit of mass (lbm) and of force (lbf). This practice implicitly combines two separate systems of units; the absolute and the gravitational systems. It is scientifically undesirable to combine the use of two separate sets of inch-pound units within a single standard. As stated, this standard includes the gravitational system of inch-pound units and does not use/present the slug unit for mass. However, the use of balances or scales recording pounds of mass (lbm) or recording density in lbm/ft3 shall not be regarded as nonconformance with this standard.1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.9 These practices offer a set of instructions for performing one or more specific operations. This document cannot replace education or experience and should be used in conjunction with professional judgement. Not all aspects of this practice may be applicable in all circumstances. This ASTM standard is not intended to represent or replace the standard of care by which the adequacy of a given professional service must be judged, nor should this document be applied without consideration of a project's many unique aspects. The word “standard” in the title of this document means only that the document has been approved through the ASTM consensus process.1.10 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The test method calibrates or demonstrates conformity of the torque signal of a rheometer at ambient temperature.5.2 A calibration factor thus determined may be used to obtain correct torque values.5.3 This test method may be used in research, development, specification acceptance, and quality control or assurance.1.1 This test method describes the calibration or performance conformance for the torque signal generated by commercial or custom-built rheometers. The specific range of the test depends upon the torque range of the rheometer.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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