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4.1 Benzene is classed as a toxic and carcinogenic material. A knowledge of the concentration of this compound may be an aid in evaluating the possible health hazards to persons handling and using hydrocarbon solvents, but this test method is not intended to evaluate such hazards.1.1 This test method covers the determination by gas chromatography of benzene at levels from 0.01 to 1 volume % in hydrocarbon solvents.NOTE 1: For benzene levels lower than 0.01 volume %, use Test Method D6229.1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.3 For purposes of determining conformance of an observed or a calculated value using this test method to relevant specifications, test result(s) shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29.1.4 For hazard information and guidance, see the supplier's Material Safety Data Sheet. For specific hazard statements, see Section 7.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Knowledge of the specified individual component composition (speciation) of gasoline fuels and blending stocks is useful for refinery quality control and product specification. Process control and product specification compliance for many individual hydrocarbons may be determined through the use of this test method.1.1 This test method covers the determination of individual hydrocarbon components of spark-ignition engine fuels and their mixtures containing oxygenate blends (MTBE, ETBE, ethanol, and so forth) with boiling ranges up to 225 °C. Other light liquid hydrocarbon mixtures typically encountered in petroleum refining operations, such as blending stocks (naphthas, reformates, alkylates, and so forth) may also be analyzed; however, statistical data was obtained only with blended spark-ignition engine fuels.1.2 Based on the cooperative study results, individual component concentrations and precision are determined in the range of 0.01 % mass to approximately 30 % mass. The procedure may be applicable to higher and lower concentrations for the individual components; however, the user must verify the accuracy if the procedure is used for components with concentrations outside the specified ranges.1.3 The test method also determines methanol, ethanol, t-butanol, methyl t-butyl ether (MTBE), ethyl t-butyl ether (ETBE), t-amyl methyl ether (TAME) in spark ignition engine fuels in the concentration range of 1 % mass to 30 % mass. However, the cooperative study data provided sufficient statistical data for MTBE only.1.4 Although a majority of the individual hydrocarbons present are determined, some co-elution of compounds is encountered. If this test method is utilized to estimate bulk hydrocarbon group-type composition (PONA) the user of such data should be cautioned that some error will be encountered due to co-elution and a lack of identification of all components present. Samples containing significant amounts of olefinic or naphthenic (for example, virgin naphthas), or both, constituents above n-octane may reflect significant errors in PONA type groupings. Based on the gasoline samples in the interlaboratory cooperative study, this procedure is applicable to samples containing less than 25 % mass of olefins. However, some interfering coelution with the olefins above C7 is possible, particularly if blending components or their higher boiling cuts such as those derived from fluid catalytic cracking (FCC) are analyzed, and the total olefin content may not be accurate. Caution should also be exercised when analyzing olefin-free samples using this test method as some of the paraffins may be reported as olefins since analysis is based purely on retention times of the eluting components.1.4.1 Total olefins in the samples may be obtained or confirmed, or both, if necessary, by Test Method D1319 (percent volume) or other test methods, such as those based on multidimensional PONA type of instruments (Test Method D6839).1.5 If water is or is suspected of being present, its concentration may be determined, if desired, by the use of Test Method D1744, or equivalent. Other compounds containing oxygen, sulfur, nitrogen, and so forth, may also be present, and may co-elute with the hydrocarbons. If determination of these specific compounds is required, it is recommended that test methods for these specific materials be used, such as Test Methods D4815 and D5599 for oxygenates, and D5623 for sulfur compounds, or equivalent.1.6 Annex A1 of this test method compares results of the test procedure with other test methods for selected components, including olefins, and several group types for several interlaboratory cooperative study samples. Although benzene, toluene, and several oxygenates are determined, when doubtful as to the analytical results of these components, confirmatory analyses can be obtained by using specific test methods.1.7 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification covers manufacturing and joining requirements for peelable or skinned polyethylene (PE) pipe, which is PE pipe meeting the requirements of Specification D2513, with a peelable outer layer of polypropylene (PP). The peelable PP layer does not contribute to outside diameter and wall thickness used for pressure rating or tensile loading calculations.1.1 This standard specification covers manufacturing and joining requirements for peelable (skinned) polyethylene (PE) pipe, which is PE pipe meeting the requirements of Specification D2513, with a peelable outer layer of polypropylene (PP). These requirements are in addition to those in Specification D2513 for the PE pipe.1.2 The peelable PP layer does not contribute to outside diameter and wall thickness used for pressure rating or tensile loading calculations.1.3 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in figures and tables) shall not be considered as requirements of the standard.1.4 Units—The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Knowledge of the individual component composition (speciation) of gasoline fuels and blending stocks is useful for refinery quality control and product specification. Process control and product specification compliance for many individual hydrocarbons can be determined through the use of this test method.5.2 This test method is adopted from earlier development and enhancement.4,5,6,7 The chromatographic operating conditions and column tuning process, included in this test method, were developed to provide and enhance the separation and subsequent determination of many individual components not obtained with previous single-column analyses. The column temperature program profile is selected to afford the maximum resolution of possible co-eluting components, especially where these are of two different compound types (for example, a paraffin and a naphthene).5.3 Although a majority of the individual hydrocarbons present in petroleum distillates are determined, some co-elution of compounds is encountered. If this test method is utilized to determine bulk hydrocarbon group-type composition (PONA), the user of such data should be cautioned that some error will be encountered due to co-elution and a lack of identification of all components present. Samples containing significant amounts of olefinic or naphthenic, or both, constituents above octane may reflect significant errors in PONA-type groupings.5.4 If water is or is suspected of being present, its concentration is determined by the use of Test Method D1744. Other compounds containing oxygen, sulfur, nitrogen, and so forth may also be present, and may co-elute with the hydrocarbons. When known co-elution exists, these are noted in the test method data tables. If determination of these specific compounds is required, it is recommended that test methods for these specific materials be used, such as Test Method D4815 and D5599 for oxygenates, Test Method D5580 for aromatics, and Test Method D5623 for sulfur compounds.1.1 This test method covers the determination of individual hydrocarbon components of spark-ignition engine fuels and their mixtures containing oxygenate blends (MTBE, ETBE, ethanol, and so forth) with boiling ranges up to 225 °C. Other light liquid hydrocarbon mixtures typically encountered in petroleum refining operations, such as blending stocks (naphthas, reformates, alkylates, and so forth) may also be analyzed; however, statistical data was obtained only with blended spark-ignition engine fuels.1.2 Based on the cooperative study results, individual component concentrations and precision are determined in the range from 0.01 % to approximately 30 % by mass. The test method may be applicable to higher and lower concentrations for the individual components; however, the user must verify the accuracy if the test method is used for components with concentrations outside the specified ranges.1.3 This test method also determines methanol, ethanol, t-butanol, methyl t-butyl ether (MTBE), ethyl t-butyl ether (ETBE), and t-amyl methyl ether (TAME) in spark ignition engine fuels in the concentration range from 1 % to 30 % by mass. However, the cooperative study data provided insufficient statistical data for obtaining a precision statement for these compounds.1.4 Although a majority of the individual hydrocarbons present are determined, some co-elution of compounds is encountered. If this test method is utilized to estimate bulk hydrocarbon group-type composition (PONA), the user of such data should be cautioned that some error will be encountered due to co-elution and a lack of identification of all components present. Samples containing significant amounts of naphthenic (for example, virgin naphthas) constituents above n-octane may reflect significant errors in PONA-type groupings. Based on the gasoline samples in the interlaboratory cooperative study, this test method is applicable to samples containing less than 25 % by mass of olefins. However, some interfering co-elution with the olefins above C7 is possible, particularly if blending components or their higher boiling cuts such as those derived from fluid catalytic cracking (FCC) are analyzed, and the total olefin content may not be accurate. Annex A1 of this test method compares results of the test method with other test methods for selected components, including olefins, and several group types for several interlaboratory cooperative study samples. Although benzene, toulene, and several oxygenates are determined, when doubtful as to the analytical results of these components, confirmatory analyses can be obtained by using the specific test methods listed in the reference section.1.4.1 Total olefins in the samples may be obtained or confirmed, or both, if necessary, by Test Method D1319 (percent by volume) or other test methods, such as those based on multidimentional PONA-type of instruments.1.5 If water is or is suspected of being present, its concentration may be determined, if desired, by the use of Test Method D1744 or equivalent. Other compounds containing oxygen, sulfur, nitrogen, and so forth, may also be present, and may co-elute with the hydrocarbons. If determination of these specific compounds is required, it is recommended that test methods for these specific materials be used, such as Test Methods D4815 and D5599 for oxygenates, and Test Method D5623 for sulfur compounds, or equivalent.1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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3.1 For custody transfer and other purposes, it is frequently necessary to convert a component analysis of light hydrocarbon mixture from one basis (either gas volume, liquid volume, or mass) to another.3.2 The component distribution data of light hydrocarbon mixtures can be used to calculate physical properties such as relative density, vapor-pressure, and calorific value. Consistent and accurate conversion data are extremely important when calculating vapor, liquid, or mass equivalence.1.1 This practice describes the procedure for the interconversion of the analysis of C5 and lighter hydrocarbon mixtures to gas-volume (mole), liquid-volume, or mass basis.1.2 The computation procedures described assume that gas-volume percentages have already been corrected for nonideality of the components as a part of the analytical process by which they have been obtained. These are numerically the same as mole percentages.1.3 The procedure assumes the absence of nonadditivity corrections for mixtures of the pure liquid compounds. This is approximately true only for mixtures of hydrocarbons of the same number of carbon atoms, and in the absence of diolefins and acetylenic compounds.1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Residue in LPG is a contaminant that can lead to operational problems in some end use applications. Engines, micro-turbines, fuel cells and other equipment may be sensitive to residue levels as low as 10 mg/kg.5.2 Contamination of LPG can occur during production, transport, delivery, storage and use. A qualitative indication of the contaminants can help track down the source of the contamination from manufacture, through the distribution system, and to the end user.5.3 This test method is designed to provide a lower detection limit, wider dynamic range, and better accuracy than gravimetric methods like Test Method D2158.5.4 This test method can be performed with little or no discharge of LPG vapors, compared to Test Method D2158 which requires evaporation of 100 mL of sample per test.5.5 Sampling for residue in LPG using sorbent tubes can be performed in the field, and the sorbent tubes sent to a laboratory for analysis. This saves significant costs in shipping (weight of tube is approximately 10 grams), and is much safer and easier than transporting LPG cylinders.5.6 This test method determines total residues from C6 to C40, compared to a thermal gravimetric residue method such as Test Method D2158 which heat the residue to 38°C, resulting in a lower recovery due to loss of lighter residue components.5.7 If there is a need to decrease the detection limit of residue or individual compounds of interest below 10 µg/g, the procedures in this test method can be modified to achieve 50 times enhanced detection limit, or 0.2 µg/g.1.1 This test method covers the determination of residue in LPG by automated thermal desorption/gas chromatography (ATD/GC) using flame ionization detection (FID).1.2 The quantitation of residue covers a component boiling point range from 69°C to 522°C, equivalent to the boiling points of C6 through C40 n-paraffins.1.2.1 The boiling range covers possible LPG contaminants such as gasoline, diesel fuel, phthalates and compressor oil. Qualitative information on the nature of the residue can be obtained from this test method.1.2.2 Materials insoluble in LPG and components which do not elute from the gas chromatograph or which have no response in a flame ionization detector are not determined.1.2.3 The reporting limit (or limit of quantitation) for total residue is 6.7 µg/g.1.2.4 The dynamic range of residue quantitation is 6.7 to 3300 µg/g.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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5.1 The presence of trace amounts of hydrogen, oxygen, carbon monoxide, and carbon dioxide can have deleterious effects in certain processes using hydrocarbon products as feed stock. This test method is suitable for setting specifications, for use as an internal quality control tool, and for use in development and research work.1.1 This test method covers the determination of hydrogen, nitrogen, oxygen, methane, carbon monoxide, and carbon dioxide in the parts per billion mole (nmol/mol) to parts per million mole (µmol/mol) range in C2 and C3 hydrocarbons.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For some specific hazard statements, see Annex A1.1.3.1 The user is advised to obtain LPG safety training for the safe operation of this test method procedure and related activities.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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3.1 Tall oil fractionated products derived from tall oil are important commercial materials, primarily composed of fatty acids and rosin acids, but also containing some neutral material (see Terminology D804). For many applications, it is necessary to know the level of the individual fatty acids and rosin acids present in these products. Gas chromatography has proven to be a useful tool for such determinations (see Test Methods D509), and capillary chromatography, described in these test methods, is considered to be the most effective gas chromatographic technique currently available. In particular situations, other techniques may be more suitable than gas chromatography. For example, the presence of fatty acid esters in the sample would result in transesterification during the derivatization step that may affect the results.3.2 Due to hydrogen bonding, unmodified tall oil fatty acids and rosin acids cannot be volatilized at atmospheric pressure without undergoing decomposition. So, it is necessary to convert the free acids to the more volatile and more stable methyl esters, prior to chromatographic separation.3.3 These test methods describe four ways to prepare methyl esters. The classic method is through the use of diazomethane, but diazomethane is a hazardous and toxic material, and so is no longer the preferred agent. The use of diazomethane is detailed in Appendix X1.3.3.1 TMAH causes isomerization of a sample’s di- and polyunsaturated fatty acids, when it is used in even a slight excess. This leads to inaccurate results for the individual fatty acid components. TMAH should be used for materials containing only rosin acids, or when the identification or quantitation of individual fatty acid components is not important.3.3.2 TMPAH is the recommended methylating agent when the identification or quantitation of individual di- and polyunsaturated fatty acids is required. TMPAH produces results that are very similar to those of diazomethane, but without the hazards that are associated with diazomethane. A considerable excess of TMPAH may cause isomerization of conjugated compounds similar to that encountered with TMAH.3.3.3 DMF-DMA gives results comparable to TMPAH and is easy and safe to use. However, the reagent is moisture sensitive, requiring samples to be free of any significant levels of water.3.4 Two test methods for calculating the amounts of the individual fatty acid and rosin acid methyl esters are included in these test methods. When the actual weight percentage of a given compound is required, the “internal standard” method must be used. This method involves adding a known amount of an internal standard to a known amount of test material, and comparing the area of the peak associated with the internal standard with the area of the peak of the individual fatty acid or rosin acid methyl esters. The “area percent” method will give the relative amount of each component, by comparing the area of the appropriate peak to the total area of all peaks. Non-eluting compounds will lead to erroneous (absolute) results with this method.PREPARATION OF METHYL ESTERSNOTE 1: Any of these three methods can be used, with the choice being dependent on the factors mentioned in 3.3.1.1 These test methods cover the determination of the amounts of the individual fatty acids and rosin acids in fractionated tall oil products, using capillary gas chromatographic separation of the volatile methyl esters of these acids.1.2 Four methods for forming the methyl esters, and two methods for determining the amounts of the individual fatty acids and rosin acids are described.1.2.1 The classic method for the formation of methyl esters is through the use of diazomethane, but diazomethane is a hazardous and toxic material, and so is no longer the preferred reagent. The use of diazomethane is detailed in the Appendix. Methyl esters may be formed through the use of tetramethylammonium hydroxide (TMAH), trimethylphenylammonium hydroxide (TMPAH), or N,N-dimethylformamide dimethyl acetal (DMF-DMA).1.2.2 The two methods for determining the amount of the individual fatty acids and rosin acids are the “internal standard” method, which yields absolute values, and the “area percent” method, which yields relative values.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Knowledge of the individual component composition (speciation) of gasoline fuels and blending stocks is useful for refinery quality control and product specification. Process control and product specification compliance for many individual hydrocarbons may be determined through the use of this test method.1.1 This test method covers the determination of individual hydrocarbon components of spark-ignition engine fuels with boiling ranges up to 225 °C. Other light liquid hydrocarbon mixtures typically encountered in petroleum refining operations, such as, blending stocks (naphthas, reformates, alkylates, and so forth) may also be analyzed; however, statistical data was obtained only with blended spark-ignition engine fuels. The tables in Annex A1 enumerate the components reported. Component concentrations are determined in the range from 0.10 % to 15 % by mass. The procedure may be applicable to higher and lower concentrations for the individual components; however, the user must verify the accuracy if the procedures are used for components with concentrations outside the specified ranges.1.2 This test method is applicable also to spark-ignition engine fuel blends containing oxygenated components. However, in this case, the oxygenate content must be determined by Test Methods D5599 or D4815.1.3 Benzene co-elutes with 1-methylcyclopentene. Benzene content must be determined by Test Method D3606 or D5580.1.4 Toluene co-elutes with 2,3,3-trimethylpentane. Toluene content must be determined by Test Method D3606 or D5580.1.5 Although a majority of the individual hydrocarbons present are determined, some co-elution of compounds is encountered. If this procedure is utilized to estimate bulk hydrocarbon group-type composition (PONA) the user of such data should be cautioned that error may be encountered due to co-elution and a lack of identification of all components present. Samples containing significant amounts of naphthenic (for example, virgin naphthas) constituents above n-octane may reflect significant errors in PONA type groupings. Based on the interlaboratory cooperative study, this procedure is applicable to samples having concentrations of olefins less than 20 % by mass. However, significant interfering coelution with the olefins above C7 is possible, particularly if blending components or their higher boiling cuts such as those derived from fluid catalytic cracking (FCC) are analyzed, and the total olefin content may not be accurate. Many of the olefins in spark ignition fuels are at a concentration below 0.10 %; they are not reported by this test method and may bias the total olefin results low.1.5.1 Total olefins in the samples may be obtained or confirmed, or both, by Test Method D1319 (volume %) or other test methods, such as those based on multidimensional PONA type of instruments.1.6 If water is or is suspected of being present, its concentration may be determined, if desired, by the use of Test Method D1744. Other compounds containing sulfur, nitrogen, and so forth, may also be present, and may co-elute with the hydrocarbons. If determination of these specific compounds is required, it is recommended that test methods for these specific materials be used, such as Test Method D5623 for sulfur compounds.1.7 The values stated in SI units are to be regarded as the standard. The values given in parentheses are provided for information only.1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification covers the qualification requirements and test methods for field-assembled anodeless riser kits for use with outside diameter controlled polyethylene gas distribution pipes and tubing in sizes of up to 2 IPS. The anodeless riser kits shall be manufactured in accordance with the specified materials, physical properties, and design, which include the riser casings, moisture seals, threads, bend radius, coatings, welding procedures, and riser adapter to riser casing connections. The riser adapter to riser casing connections shall tested by tensile pull testing.1.1 This specification covers requirements and test methods for field-assembled anodeless riser kits for use with outside diameter controlled polyethylene and PA11 gas distribution pipe and tubing in sizes through 2 IPS as specified in Specification D2513 polyethylene and Specification F2945 for PA11.1.2 The test methods described are not intended to be routine quality control tests.1.3 This specification covers the types of field-assembled anodeless riser kits described in 3.3.2.1.4 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and not considered standard.1.5 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures), shall not be considered as requirements of the standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Butadiene dimer and styrene may be present as impurities in commercial butadiene. This test method is suitable for use in internal quality control and in establishing product specifications.1.1 This test method covers the determination of butadiene dimer (4-vinylcyclohexene-1) and styrene in butadiene concentrates, both recycle and specification grade.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific precautionary statements see Sections 6 and 8.1.3.1 The user is advised to obtain LPG safety training for the safe operation of this test method procedure and related activities.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The significance of this test method in any overall measurements program to assess the erosion behavior of materials will depend on many factors concerning the conditions of service applications. The users of this test method should determine the degree of correlation of the results obtained with those from field performance or results using other test systems and methods. This test method may be used to rank the erosion resistance of materials under the specified conditions of testing.1.1 This test method covers the determination of material loss by gas-entrained solid particle impingement erosion with jetnozzle type erosion equipment. This test method may be used in the laboratory to measure the solid particle erosion of different materials and has been used as a screening test for ranking solid particle erosion rates of materials in simulated service environments (1, 2).2 Actual erosion service involves particle sizes, velocities, attack angles, environments, and so forth, that will vary over a wide range (3-5). Hence, any single laboratory test may not be sufficient to evaluate expected service performance. This test method describes one well characterized procedure for solid particle impingement erosion measurement for which interlaboratory test results are available.1.2 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard (exceptions below).1.2.1 Exceptions: Table 1 uses HRB hardness. Footnote 7 and 11.2 use abrasive grit designations.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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18.1 For purpose of determining compliance with the specified limits for requirements of the properties listed in Table 5, an observed value or calculated value shall be rounded as indicated in accordance with the rounding method of Practice E29.1.1 This specification establishes the requirements for Type GAS seamless Copper UNS No. C12200 tube for use in above ground natural gas and liquified petroleum (LP) gas fuel distribution systems, commonly assembled with flared fittings or brazed joints.NOTE 1: Tube temper, size, and joining method are determined by installation code requirements.1.2 Units—The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.3 The following safety hazard caveat pertains only to the test method(s) portion, Section 17, of this specification. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 In hydrocarbon type analyses of gasolines, highly volatile fuels can need to be stabilized by depentanization (Test Method D2001) prior to analysis. A knowledge of the composition of light hydrocarbons in the overhead from the depentanization process is useful in converting analyses of the depentanized fraction to a total sample basis.1.1 This test method covers the determination of the two (C2) through five (C5-) carbon paraffins and mono-olefins in gasolines. The concentrations by volume or mass (weight) of the following components are generally reported:1.1.1 Ethylene plus ethane1.1.2 Propane1.1.3 Propylene1.1.4 Isobutane1.1.5 n-Butane1.1.6 Butene-1 plus isobutylene1.1.7 trans-Butene-21.1.8 cis-Butene-21.1.9 Isopentane1.1.10 3-Methylbutene-11.1.11 n-Pentane1.1.12 Pentene-11.1.13 2-Methylbutene-11.1.14 trans-Pentene-21.1.15 cis-Pentene-21.1.16 2-Methylbutene-21.2 This test method does not cover the determination of cyclic olefins, diolefins, or acetylenes. These are usually minor components in finished gasolines.1.3 Samples to be analyzed should not contain significant amounts of material boiling lower than ethylene.1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4.1 Exception—Alternative units, in common usage, are also provided to improve the clarity and aid the user of this test method.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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3.1 Although it is possible to observe and measure each of the several characteristics of the ELCD under different and unique conditions, in particular its different modes of selectivity, it is the intent of this practice that a complete set of detector specifications should be obtained at the same operating conditions, including geometry, gas and solvent flow rates, and temperatures. It should be noted that to specify a detector's capability completely, its performance should be measured at several sets of conditions within the useful range of the detector. The terms and tests described in this practice are sufficiently general so that they may be used at whatever conditions may be chosen for other reasons.3.2 Linearity and speed of response of the recorder used should be such that it does not distort or otherwise interfere with the performance of the detector. Effective recorder response should be sufficiently fast so that it can be neglected in sensitivity of measurements. If additional amplifiers are used between the detector and the final readout device, their characteristics should also first be established.1.1 This practice covers testing the performance of an electrolytic conductivity detector (ELCD) used as the detection component of a gas chromatographic system.1.2 This practice is directly applicable to electrolytic conductivity detectors that perform a chemical reaction on a given sample over a nickel catalyst surface under oxidizing or reducing conditions and employ a scrubber, if needed, to remove interferences, deionized solvent to dissolve the reaction products, and a conductivity cell to measure the electrolytic conductivity of ionized reaction products.1.3 This practice covers the performance of the detector itself, independently of the chromatographic column, in terms that the analyst can use to predict overall system performance when the detector is coupled to the column and other chromatographic system components.1.4 For general gas chromatographic procedures, Practice E260 should be followed except where specific changes are recommended herein for the use of an electrolytic conductivity detector. For definitions of gas chromatography and its various terms see Practice E355.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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