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5.1 Uranium hexafluoride used to produce nuclear fuel must meet certain criteria for its isotopic composition as described in Specifications C787 and C996.1.1 This method applies to the determination of isotopic composition in hydrolyzed nuclear grade uranium hexafluoride. It covers isotopic abundance of  235U between 0.1 and 5.0 % mass fraction, abundance of  234U between 0.0055 and 0.05 % mass fraction, and abundance of   236U between 0.0003 and 0.5 % mass fraction. This test method may be applicable to other isotopic abundance providing that corresponding standards are available.1.2 This test method can apply to uranyl nitrate solutions. This can be achieved either by transforming the uranyl nitrate solution to a uranyl fluoride solution prior to the deposition on the filaments or directly by depositing the uranyl nitrate solution on the filaments. In the latter case, a calibration with uranyl nitrate standards must be performed.1.3 This test method can also apply to other nuclear grade matrices (for example, uranium oxides) by providing a chemical transformation to uranyl fluoride or uranyl nitrate solution.1.4 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The test method is capable of measuring uranium isotopic abundances of 234U, 235U, 236U, and 238U as required by Specifications C787 and C996.1.1 This test method covers the isotopic abundance analysis of 234U, 235U, 236U, and 238U in samples of hydrolysed uranium hexafluoride (UF6) by inductively coupled plasma source, multicollector, mass spectrometry (ICP-MC-MS). The method applies to material with  235U abundance in the range of 0.2 to 6 % mass. This test method is also described in ASTM STP 1344.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 By use of standard or reference grade materials for any two of the three components, namely, oxygenated solvent, diluent, or cellulose nitrate, the effect of different batches or different types of the third component can be determined.4.2 This test method is applicable for the determination of the following:4.2.1 The dilution ratio of toluene as the standard diluent to an oxygenated solvent under test, using as the solute standard cellulose nitrate as defined in 5.2.4.2.2 The dilution ratio of a hydrocarbon diluent under test to n-butyl acetate as the standard solvent, using as a solute standard cellulose nitrate as defined in 5.2.4.2.3 The dilution ratio of toluene, as the standard diluent, to n-butyl acetate as the standard solvent, using as the solute cellulose nitrate of varying solubility characteristics.4.3 The information developed through this test may be useful in the formulation of cellulose-based lacquers and adhesives.1.1 This test method covers the determination of the volume ratio of hydrocarbon diluent to active solvent required to cause persistent heterogeneity (precipitation) in a solution of cellulose nitrate.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 The following applies to all specified limits in this standard; for purposes of determining conformance with this standard, an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 6.1.5 For hazard information and guidance, see the supplier's Material Safety Data Sheet.

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ASTM D3867-16(2021)e1 Standard Test Methods for Nitrite-Nitrate in Water Active 发布日期 :  1970-01-01 实施日期 : 

5.1 Both test methods use identical reagents and sample processing. The only difference between the two methods is that one test method is automated and the other is manual. The ranges and interferences are identical.5.2 The automated test method is preferred when large numbers of samples are to be analyzed. The manual test method is used for fewer samples or when automated instrumentation is not available.5.3 These test methods replace Test Methods D1254 (Nitrite) and D992 (Nitrate). The nitrite test method (Test Method D1254) used a reagent that is considered to be a potential carcinogen. The nitrate test method (Test Method D992) has been shown to have relatively large errors when used in wastewaters and also has greater manipulative difficulties than the test method described herein.5.4 Test Method D7781 uses a nitrate reductase enzyme for the reduction of nitrate to nitrite. Cadmium is considered a toxic metal. Also, the heterogeneous cadmium reductant creates greater difficulty than the reduction described in this test method.1.1 These test methods cover the determination of nitrite nitrogen, nitrate nitrogen, and combined nitrite-nitrate nitrogen in water and wastewater in the range from 0.05 to 1.0 mg/L nitrogen. Two test methods2 are given as follows:  SectionsTest Method A—Automated Cadmium Reduction  9 to 18Test Method B—Manual Cadmium Reduction 19 to 281.2 These test methods are applicable to surface, saline, waste, and ground waters. It is the user's responsibility to ensure the validity of these test methods for waters of untested matrices.1.3 The values stated in either SI or inch-pound units are to be regarded as the standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see 8.2.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D301-95(2004) Standard Test Methods for Soluble Cellulose Nitrate (Withdrawn 2011) Withdrawn, No replacement 发布日期 :  1970-01-01 实施日期 : 

Ash accounts for the nonsoluble, nonfilm forming portion of the polymer. It may affect solution clarity and film properties.1.1 These test methods cover the material known as soluble cellulose nitrate (also known as soluble nitrocellulose), which is shipped wet in conformance with regulations of the Interstate Commerce Commission.1.2 The test methods appear in the following sections: SectionsAsh Drying Samples Nitrogen Stability Toluene Dilution Viscosity 1.3 The values stated in SI units are to be regarded as the standard. Values given in parentheses are for information only.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see 12.2, 13.3, 16.1, and 16.2.

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ASTM D1839-14(2019) Standard Test Method for Amyl Nitrate in Diesel Fuels (Withdrawn 2019) Withdrawn, No replacement 发布日期 :  1970-01-01 实施日期 : 

4.1 In diesel fuel, the presence of alkyl nitrates such as amyl nitrate, hexyl nitrate, or octyl nitrate causes a higher residue value than observed in untreated fuel, which can lead to erroneous conclusions as to the coke forming propensity of the fuel. The presence of such alkyl nitrate in the fuel can be determined using this test method. This test method can be used to determine the amount of amyl nitrate that has been added to diesel fuels to improve cetane number. This test method is applicable as a basis for judging compliance with specifications covering amyl nitrate.1.1 This test method covers the determination of 0.1 % to 0.5 % by volume amyl nitrate in diesel fuels.NOTE 1: This test method has been used for the determination of hexyl nitrate in diesel fuels, but has not been cooperatively tested for such samples. For the determination of hexyl nitrate, use standards containing nitrate esters of primary hexanol. Use a density of 0.97 in calculating results.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The method is designed to show whether or not the tested materials meet the specifications as given in Specifications C787 and C788.1.1 This method covers the determination of bromine (Br) and chlorine (Cl) in uranium hexafluoride (UF6) and uranyl nitrate solution. The method as written covers the determination of bromine in UF6 over the concentration range of 0.2 to 8 µg/g, uranium basis. The chlorine in UF6 can be determined over the range of 4 to 160 µg/g, uranium basis. Higher concentrations may be covered by appropriate dilutions. The detection limit for Br is 0.2 µg/g uranium basis and for Cl is 4 µg/g uranium basis.1.2 The values stated in SI units are to be regarded as the standard.1.3 This standard may involve hazardous materials, operations and equipment. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method is an accelerated test for detecting the presence of residual (internal) stresses that might result in failure of individual parts in storage or in service due to stress corrosion cracking.5.2 This test method is not intended for use on assemblies or parts under applied stress. If used for that purpose, the results shall be for information only and not a cause for rejection of the assembly, its component parts, or the original mill product.1.1 This test method describes the technique for conducting the mercurous nitrate test for residual stresses in wrought copper alloy mill products.NOTE 1: For any particular copper alloy, reference should be made to the material specification.NOTE 2: Test Method B858 may be considered as a possible alternative test method which does not involve the use of mercury.NOTE 3: This test method is considered historically reliable for determining the potential state of residual stress in copper alloys, but not promoted for use due to the hazards relating to mercury use and environmentally appropriate disposal.1.2 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determines the applicability of regulatory limitations prior to use. For specific precautionary and hazard statements see Sections 1, 6, and 7. (Warning—Mercury has been designated by many regulatory agencies as a hazardous substance that can cause serious medical issues. Mercury, or its vapor, has been demonstrated to be hazardous to health and corrosive to materials. Use caution when handling mercury and mercury-containing products, or both. See the applicable product Safety Data Sheet (SDS) for additional information. The potential exists that selling mercury or mercury-containing products, or both, is prohibited by local or national law. Users must determine legality of sales in their location.)1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method is for the determination of the anions: chloride, nitrate, and sulfate in atmospheric wet deposition.5.2 Fig. X1.1 in the appendix represents cumulative frequency percentile concentration plots of chloride, nitrate, and sulfate obtained from analyses of over 5000 wet deposition samples. These data may be used as an aid in the selection of appropriate calibration solutions (2).1.1 This test method is applicable to the determination of chloride, nitrate, and sulfate in atmospheric wet deposition samples (rain, snow, sleet, and hail) by suppressed ion chromatography. For additional applications, see to Test Method D4327.1.2 The concentration ranges for this test method are as listed below. The range tested was confirmed using the interlaboratory collaborative test (see Table 1 for statistical summary of the collaborative test).  MethodDetectionL (mg/L) (1) Range ofMethod(mg/L) RangeTested(mg/L)Chloride 0.03 0.09–2.0 0.15–1.36Nitrate 0.03 0.09–5.0 0.15–4.92Sulfate 0.03 0.09–8.0 0.15–6.521.3 The method detection limit (MDL) is based on single operator precision (1)2 and may be higher or lower for other operators and laboratories. The precision and bias data presented are insufficient to justify use at this low level; however, it has been reported that this test method is reliable at lower levels than those that were tested. The MDLs listed above were determined following the guidance in 40 CFR Part 136 Appendix B. Other approaches to the determination of MDLs may yield different MDLs.1.4 Method Detection Limits will vary depending on the type and length of column(s) used, the composition and strength of eluent used, the bore size of the instrumentation (that is, microbore or standard bore), eluent flow rate and other variables between instruments. The method detection limits listed above are those used in determining the Precision and Bias of this method as given in Table 1.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 9.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 These test methods are designed to show whether a given material meets the purchaser's specifications.4.1.1 An assay is performed to determine whether the material has the specified plutonium content.4.1.2 Determination of the isotopic content of the plutonium in the plutonium-nitrate solution is made to establish whether the effective fissile content is in compliance with the purchaser's specifications.4.1.3 Impurity content is determined by a variety of methods to ensure that the maximum concentration limit of specified impurities is not exceeded. Determination of impurities is also required for calculation of the equivalent boron content (EBC).4.2 Fitness for Purpose of Safeguards and Nuclear Safety Applications—Methods intended for use in safeguards and nuclear safety applications shall meet the requirements specified by Guide C1068 for use in such applications.1.1 These test methods cover procedures for the chemical, mass spectrometric, spectrochemical, nuclear, and radiochemical analysis of nuclear-grade plutonium nitrate solutions to determine compliance with specifications.1.2 The analytical procedures appear in the following order:  Sections Plutonium by Controlled-Potential Coulometry 2Plutonium by Amperometric Titration with Iron(II) 2Plutonium by Diode Array Spectrophotometry  Free Acid by Titration in an Oxalate Solution 8 to 15Free Acid by Iodate Precipitation-Potentiometric Titration  Test Method 16 to 22Uranium by Arsenazo I Spectrophotometric Test Method 23 to 33Thorium by Thorin Spectrophotometric Test Method 34 to 42Iron by 1,10-Phenanthroline Spectrophotometric Test Method 43 to 50Impurities by ICP-AES  Chloride by Thiocyanate Spectrophotometric Test Method 51 to 58Fluoride by Distillation-Spectrophotometric Test Method 59 to 66Sulfate by Barium Sulfate Turbidimetric Test Method 67 to 74Isotopic Composition by Mass Spectrometry 75 to 76Plutonium-238 Isotopic Abundance by Alpha Spectrometry  Americium-241 by Extraction and Gamma Counting 77 to 85Americium-241 by Gamma Counting 86 to 94Gamma-Emitting Fission Products, Uranium, and Thorium by Gamma-Ray Spectroscopy 94 to 102Rare Earths by Copper Spark Spectrochemical Test Method 103 to 105Tungsten, Niobium (Columbium), and Tantalum by Spectro- chemical Test Method 106 to 114Sample Preparation for Spectrographic Analysis for General Impurities 115 to 1181.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific safeguard and safety hazard statements, see Section 6.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification applies to nuclear-grade aqueous uranyl nitrate solution or crystals not exceeding 5% 235U intended for subsequent manufacture into either UF6 or direct conversion to uranium oxide. This specification is intended to provide the nuclear industry with a general standard for aqueous uranyl nitrate solution or crystals. The purpose of this specification is: to define the impurity and uranium isotope limits for commercial standard uranyl nitrate, and to define additional limits for reprocessed uranyl nitrate (or any mixture of reprocessed and commercial standard uranyl nitrate).1.1 This specification applies to nuclear-grade aqueous uranyl nitrate solution or crystals not exceeding 5 % 235U intended for subsequent manufacture into either UF6 (for feed to an enrichment plant) or direct conversion to uranium oxide (for use in reactors).1.2 This specification is intended to provide the nuclear industry with a general standard for aqueous uranyl nitrate solution or crystals. It recognizes the diversity of manufacturing methods and the processes to which it is subsequently to be subjected. It is therefore anticipated that it may be necessary to include supplementary specification limits by agreement between purchaser and manufacturer. Different limits are appropriate depending on whether or not the uranyl nitrate is to be converted to UF6 for subsequent processing.1.3 The purpose of this specification is: (a) to define the impurity and uranium isotope limits for commercial standard uranyl nitrate, and (b) to define additional limits for reprocessed uranyl nitrate (or any mixture of reprocessed and commercial standard uranyl nitrate). For such uranyl nitrates, special provisions may need to be made to ensure that no extra hazard arises to the employees, the process equipment, or the environment.1.4 The scope of this specification does not comprehensively cover all provisions for preventing criticality accidents, for health and safety, or for shipping. Observance of this standard does not relieve the user of the obligation to conform to all international, federal, state and local regulations for processing, shipping, or any other way of using the uranyl nitrate. An example of a U.S. Government Document is the Code of Federal Regulations, Title 10, Part 50 (latest edition).1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Specific gamma-ray emitting radionuclides in UF6 are identified and quantified using a high-resolution gamma-ray energy analysis system, which includes a high-resolution germanium detector. This test method shall be used to meet the health and safety specifications of C787, C788, and C996 regarding applicable fission products in reprocessed uranium solutions. This test method may also be used to provide information to parties such as conversion facilities on the level of uranium decay products in such materials. Pa-231 is a specific uranium decay product that may be present in uranium ore concentrate and is amenable to analysis by gamma spectrometry.1.1 This test method covers the measurement of gamma energy emitted from fission products in uranium hexafluoride (UF6) and uranyl nitrate solution. This test method may also be used to measure the concentration of some uranium decay products. It is intended to provide a method for demonstrating compliance with UF6 specifications C787 and C996, uranyl nitrate specification C788, and uranium ore concentrate specification C967.1.2 The lower limit of detection is 5000 MeV Bq/kg (MeV/kg per second) of uranium and is the square root of the sum of the squares of the individual reporting limits of the nuclides to be measured. The limit of detection was determined on a pure, aged natural uranium (ANU) solution. The value is dependent upon detector efficiency and background.1.3 The fission product nuclides to be measured are 106Ru/106Rh, 103Ru, 137Cs, 144Ce, 144Pr, 141Ce, 95Zr, 95Nb, and 125Sb. Among the uranium decay product nuclides that may be measured is 231Pa. Other gamma energy-emitting fission and uranium decay nuclides present in the spectrum at detectable levels should be identified and quantified as required by the data quality objectives.1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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1.1 This test method covers the sample preparation and analysis by X-ray fluorescence (XRF) of sulfur in uranium oxides and uranyl nitrate solutions.1.2 This test method is valid for those solutions containing 100 to 500 g sulfur/mL. Higher concentrations may be measured by appropriate dilutions.This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See Section 9 and Note 1 for specific hazards statements.

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4.1 Uranyl nitrate solution is used as a feed material for conversion to the hexafluoride as well as for direct conversion to the oxide. In order to be suitable for this purpose, the material must meet certain criteria for uranium content, isotopic composition, acidity, radioactivity, and impurity content. These methods are designed to show whether a given material meets the specifications for these items described in Specification C788.4.1.1 An assay is performed to determine whether the material has the specified uranium content.4.1.2 Determination of the isotopic content of the uranium is made to establish whether the effective fissile content is in accordance with the purchaser’s specifications.4.1.3 Acidity, organic content, and alpha, beta, and gamma activity are measured to establish that they do not exceed their maximum limits.4.1.4 Impurity content is determined to ensure that the maximum concentration limit of certain impurity elements is not exceeded. Impurity concentrations are also required for calculation of the equivalent boron content (EBC), and the total equivalent boron content (TEBC).1.1 These test methods cover procedures for the chemical, mass spectrometric, spectrochemical, nuclear, and radiochemical analysis of nuclear-grade uranyl nitrate solution to determine compliance with specifications.1.2 The analytical procedures appear in the following order:  SectionsDetermination of Uranium 8Specific Gravity by Pycnometry  16 – 21Free Acid by Oxalate Complexation  22 – 28Determination of Thorium 29Determination of Chromium 30Determination of Molybdenum 31Halogens Separation by Steam Distillation  32 – 36Fluoride by Specific Ion Electrode  37 – 43Halogen Distillate Analysis: Chloride, Bromide, and Iodide by  Amperometric Microtitrimetry 44Determination of Chloride and Bromide 45Determination of Sulfur by X-Ray Fluorescence 46Sulfate Sulfur by (Photometric) Turbidimetry 47Phosphorus by the Molybdenum Blue (Photometric) Method  55 – 62Silicon by the Molybdenum Blue (Photometric) Method 63 – 70Carbon by Persulfate Oxidation-Acid Titrimetry 71Conversion to U3O8 72 – 75Boron by Emission Spectrography AImpurity Elements by Spark Source Mass Spectrography 77Isotopic Composition by Thermal Ionization Mass Spectrometry 78Uranium-232 by Alpha Spectrometry 79 – 85Total Alpha Activity by Direct Alpha Counting 86 – 92Fission Product Activity by Beta Counting 93 – 99Entrained Organic Matter by Infrared Spectrophotometry 100Fission Product Activity by Gamma Counting 101Determination of Arsenic 102Determination of Impurities for the EBC Calculation 103Determination of Technetium 99 104Determination of Plutonium and Neptunium 1051.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 6.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method replaces Methods D1254 (Nitrite) and D992 (Nitrate). The nitrite test method (Method D1254) used a reagent that is considered to be a potential carcinogen. The nitrate test method (Method D992) has been shown to have relatively large errors when used in wastewaters and also has greater manipulative difficulties than the test method described herein.5.2 This test method can be used in place of Test Methods D3867 (Nitrite-Nitrate). Test Methods D3867 uses cadmium for the reduction of nitrate to nitrite. Cadmium is considered a toxic metal. Also, the heterogeneous cadmium reductant creates greater difficulty than the reduction described in this test method.1.1 This test method is applicable to the determination of nitrate plus nitrite (as nitrogen) in drinking water, surface, saline, wastewater, and ground waters. The applicable range of this test method is from 0.05 to 5 mg/L of nitrogen. The range may be extended upward by dilution of an appropriate aliquot. The 40 CFR Part 136 Method Detection Limit (MDL) is 0.02 mg/L.1.2 It is the user's responsibility to ensure the validity of this test method for waters of untested matrices. The quality control criteria in Section 17 for method blanks, laboratory control samples, matrix spikes and matrix duplicates must be met.1.3 The values stated in SI units are regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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