5.1 This test method provides a simple means of characterizing the important rheological properties and viscosity of thermoplastic polymers using very small amounts of material (approximately 25 to 50 mm in diameter by 1 to 3 mm in thickness ... approximately 3 to 5 g). Data are generally used for quality control, research and development, and establishment of optimum processing conditions.5.2 Dynamic mechanical testing provides a sensitive method for determining molten polymer properties by measuring the elastic and loss moduli as a function of frequency, strain, temperature, or time. Plots of viscosity, storage, and loss moduli, and tan delta as a function of the aforementioned process parameters provide graphical representation indicative of molecular weight, molecular weight distribution, effects of chain branching, and melt-processability for specified conditions.5.2.1 Observed data are specific to experimental conditions. Reporting in full (as described in this test method) the conditions under which the data was obtained is essential to assist users with interpreting the data an reconciling apparent or perceived discrepancies.5.3 Values obtained in this test method can be used to assess the following:5.3.1 Complex viscosity of the polymer melt as a function of dynamic oscillation,5.3.2 Processing viscosity, minimum as well as changes in viscosity as a function of experimental parameters,5.3.3 Effects of processing treatment,5.3.4 Relative polymer behavioral properties, including viscosity and damping, and5.3.5 Effects of formulation additives that might affect processability or performance.5.4 Before proceeding with this test method, refer to the specification for the material being tested. Any test specimen preparation, conditioning, dimensions, or testing parameters, or combination thereof, covered in the relevant ASTM materials specification shall take precedence over those mentioned in the test method. If there are no relevant ASTM material specifications, then the default conditions apply.1.1 This test method outlines the use of dynamic mechanical instrumentation in determining and reporting the rheological properties of thermoplastic resins and other types of molten polymers. The method is useful for determining the complex viscosity and other significant viscoelastic characteristics of such materials as a function of frequency, strain amplitude, temperature, and time. It is known that fillers and other additives influence rheological properties.1.2 It incorporates a laboratory test method for determining the relevant rheological properties of a polymer melt subjected to various oscillatory deformations on an instrument of the type commonly referred to as a mechanical or dynamic spectrometer.1.3 This test method is intended to provide a means of determining the rheological properties of molten polymers, such as thermoplastics and thermoplastic elastomers over a range of temperatures by nonresonant, forced-vibration techniques. Plots of modulus, viscosity, and tan delta as a function of dynamic oscillation (frequency), strain amplitude, temperature, and time are indicative of the viscoelastic properties of a molten polymer.1.4 This test method is valid for a wide range of frequencies, typically from 0.01 Hz to 100 Hz.1.5 This test method is intended for homogenous and heterogeneous molten polymeric systems and composite formulations containing chemical additives, including fillers, reinforcements, stabilizers, plasticizers, flame retardants, impact modifiers, processing aids, and other important chemical additives often incorporated into a polymeric system for specific functional properties, and which could affect the processability and functional performance. These polymeric material systems have molten viscosities typically less than 106 Pa·s (107 poise).1.6 Test data obtained by this test method are relevant and appropriate for use in engineering design.1.7 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.NOTE 1: This test method is equivalent to ISO 6721, Part 10.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification provides the standard requirements for polyethylene plastic molding and extrusion materials. The tests involved in this specification are intended to provide information for identifying materials in accordance with the groups, classes, and grades covered. Polyethylene plastic materials are classified into two groups in accordance with the molecular structure which may be branched or linear. Test specimens shall be compression molded, conditioned in a standard or controlled laboratory atmosphere, and tested to determine the materials' physical and electrical properties. The specimens shall comply with the following requirements: flow rate; density; tensile stress at yield; nominal strain at break; secant flexural modulus; environmental stress-crack resistance; slow crack growth resistance; thermal stress crack resistance; permittivity; dissipation factor; volume resistivity; water immersion stability; flammability; and weatherability.1.1 This specification provides for the identification of polyethylene plastics molding and extrusion materials in such a manner that the supplier and the user can agree on the acceptability of different commercial lots or shipments. The tests involved in this specification are intended to provide information for identifying materials in accordance with the groups, classes, and grades covered. It is not the function of this specification to provide specific engineering data for design purposes.1.2 Other requirements necessary to identify particular characteristics important to specialized applications shall be agreed upon between the user and the supplier, by using the suffixes given in Section 1.3.1.3 Ethylene plastic materials, being thermoplastic, are reprocessable and recyclable (see Note 1). This specification allows for the use of those ethylene plastic materials, provided that any specific requirements as governed by the producer and the end user are met.NOTE 1: See Guide D7209 for information and definitions related to recycled plastics.1.4 The values stated in SI units are regarded as standard.1.5 The following precautionary caveat pertains to the test method portion only, Section 12, of this specification. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 For information regarding plastic pipe materials see Specification D3350. For information regarding wire and cable materials, see Specification D1248.NOTE 2: There is no known ISO equivalent to this standard.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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X1.2 SignificanceX1.2.1 Concentrations of trace metals are measured as extracts in simulated body fluids. The metal’s concentration in extracts is based on the surface area of the plastic extracted from which the total amount of metal deliverable to the patient may be estimated.AbstractThis specification covers the properties for polyethylene plastics for use in medical device applications involving human tissue contact devices, short term indwellings, and fluid transfer devices. Biocompatibility tests must be conducted on the final products as the biocompatibility of these materials as a class has not been established. Plyethylene plastics should consist of basic polymers with ethylene as essentially the sole monomer. The compound may contain optional adjuvant substances required in polymer production or fabrication. The final compound should yield a consistent absorption spectrum characteristic of the established formulation. The polyethylene plastics should be tested using the specified physical test procedures for density, melt flow, tensile properties, compressive properties, stiffness, flexural fatigue, and other flexural properties.1.1 This specification covers polyethylene plastics (as defined in Terminology D883) intended for use in medical device applications involving human tissue contact devices, short-term indwellings of 30 days or less, and fluid transfer devices. The biocompatibility of these materials as a class has not been established. Biocompatibility tests must be conducted on the final product.1.2 This specification is not applicable to ultra-high molecular weight polyethylenes (UHMWPE) plastics, such as those used in joint implants, and so forth.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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5.1 The results of this test provide a relative measure of the total soluble fraction of polypropylene homopolymers and copolymers. The soluble fraction approximately correlates to the amorphous fraction in the polypropylene. Xylene is widely used for determining the soluble fraction in polypropylene as it is more specific to the atactic fraction than other solvents. The concentration of a soluble fraction obtained with a specific solvent has been found to relate closely to the performance characteristics of a product in certain applications, for example film and fiber. Data obtained by one solvent and at one precipitation time cannot be compared with data obtained by another solvent or precipitation time, respectively.1.1 This test method is to be used for determining the 25 °C xylene-soluble fraction of polypropylene homopolymers and copolymers.1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.NOTE 1: This test method is technically equivalent to ISO 16152.1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Dirt, paper and mixtures of polymeric materials complicate the interpretation of data from procedures used to identify the contaminants in recycled plastics.1.1 This practice describes a procedure for separating recycled plastics based on their color and a procedure for washing dirty, ground plastic, which results in separation of light materials (density <1.00 g/cm3). This practice is not intended to represent generic washing procedures used in the plastics recycling industry. The described procedures are solely for preparation of plastic samples for use in other analytical tests. The procedure includes a room temperature wash step to facilitate separation of paper (for example, labels) followed by washing at an elevated temperature.NOTE 1: Although not presented as a quantitative method, the procedure presented in this practice may be used to provide quantitative results. The user assumes the responsibility to verify the reproducibility of quantitative results.1.2 The values stated in SI units are to be regarded as the standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.NOTE 2: There is no known ISO equivalent to this standard.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification covers non-floating products made from plastics (including packaging and coatings) that are designed to be biodegradable under the marine environmental conditions of aerobic marine waters or anaerobic marine sediments, or both. (Possible environments are shallow and deep salt water and brackish water.) This specification is intended to establish the requirements for labeling materials and products, including packaging, as "biodegradable in marine waters and sediments." The products should exhibit satisfactory performances in terms of disintegration during marine degradation, inherent biodegradation, and environmental toxicity. However, this specification does not describe the contents or their performance with regard to biodegradability.1.1 This specification covers products made from plastics (including packaging and coatings) that are designed to be biodegradable under the marine environmental conditions of aerobic marine waters or anaerobic marine sediments, or both. (Possible environments are shallow and deep salt water and brackish water.)1.2 This specification is intended to establish the requirements for labeling materials and products, including packaging, as "biodegradable in marine waters and sediments."1.3 The properties in this specification are those required to determine if products (including packaging) will biodegrade satisfactorily, including biodegrading at a rate comparable to known compostable materials. Further, the properties in the specification are required to assure that the degradation of these materials will not diminish the value or utility of the marine resources and habitat.1.4 This specification does not describe contents or their performance with regard to biodegradability.1.5 The following safety hazards caveat pertains to the test methods portion of this standard: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate health and safety practices and to determine the applicability of regulatory limitations prior to use.Note 1—There is no known ISO equivalent to this standard.

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4.1 Compression Molding—In compression molding, the difference between the dimensions of a mold and of the molded article produced therein from a given material vary according to the design and operation of the mold. It is probable that shrinkage will approach a minimum where design and operation are such that a maximum of material is forced solidly into the mold cavity or some part of it, or where the molded article is hardened to a maximum while still under pressure, particularly by cooling. In contrast, shrinkages are higher where the charge must flow in the mold cavity but does not receive and transmit enough pressure to be forced firmly into all its recesses, or where the molded article is not fully hardened when discharged. The plasticity of the material used affects shrinkage insofar as it affects the retention and compression of the charge.4.2 Injection Molding—In injection molding, as in compression molding, the differences between the dimensions of the mold and of the molded article produced therein from a given material vary according to the design and operation of the mold. The differences vary with the type and size of molding machine, the thickness of molded sections, the degree and direction of flow or movement of material in the mold, the size of the nozzle, sprue, runner, and gate, the cycle on which the machine is operated, the temperature of the mold, and the length of time that follow-up pressure is maintained. As in the case of compression molding, shrinkages will approach a minimum where design and operation are such that a maximum of material is forced solidly into the mold cavity and where the molded article is hardened to a maximum while still under pressure as a result of the use of a runner, sprue, and nozzle of proper size, along with proper dwell. As in compression molding, shrinkages are higher where the charge must flow in the mold cavity but does not receive and transmit enough pressure to be forced firmly into all of the recesses of the mold. The plasticity of the material used affects shrinkage indirectly, in that the more readily plasticized material will require a lower molding temperature.4.3 Transfer Molding—In transfer molding, as in compression or injection molding, the difference between the dimensions of the mold and of the molded article produced therein from a given material vary according to the design and operation of the mold. It is affected by the size and temperature of the pot or cylinder and the pressure on it, as well as on mold temperature and molding cycle. Direction of flow is not as important a factor.4.4 Materials Standards—Always refer to material standards for special treatment prior to molding, molding conditions and special handling of the test specimens after molding. In the event the material standard is unavailable, contact the manufacturer for these recommendations.4.5 Utility—Measurement of batch-to-batch consistency in initial shrinkage from mold to molded dimensions is useful for evaluating the quality of thermosetting plastics.1.1 This test method is intended to measure shrinkage from mold cavity to molded dimensions of thermosetting plastics when molded by compression, injection, or transfer under specified conditions.1.2 This test method provides for the measurement of shrinkage of thermosetting plastics from their molds both initially (within 16 to 72 h of molding) and after aging (post–shrinkage at elevated temperatures).1.3 This method will give comparable data based on standard specimens and can not predict absolute values in actual molded parts with varying flow paths, wall thicknesses, pressure gradiants and process conditions. Differences in mold shrinkage generally is observed between the specimen geometries described in this test method.1.4 Knowledge of the initial shrinkage of plastics is important for the construction of molds and knowledge of post molding shrinkage is important for determining the suitability of the molding material for manufacturing thermosetting plastic components with accurate dimensions.1.5 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.NOTE 1: This test method and ISO 2577-1984 are equivalent when bars of 120 mm length, 15 mm width, and 10 mm thickness are used for compression molding; or flat, square plaques approximately 120 by 120 by 4 mm are used for injection molding.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Flexural properties as determined by this test method are especially useful for quality control and specification purposes. They include:5.1.1 Flexural Stress (σf)—When a homogeneous elastic material is tested in flexure as a simple beam supported at two points and loaded at the midpoint, the maximum stress in the outer surface of the test specimen occurs at the midpoint. Flexural stress is calculated for any point on the load-deflection curve using equation (Eq 3) in Section 12 (see Notes 5 and 6).NOTE 5: Eq 3 applies strictly to materials for which stress is linearly proportional to strain up to the point of rupture and for which the strains are small. Since this is not always the case, a slight error will be introduced if Eq 3 is used to calculate stress for materials that are not true Hookean materials. The equation is valid for obtaining comparison data and for specification purposes, but only up to a maximum fiber strain of 5 % in the outer surface of the test specimen for specimens tested by the procedures described herein.NOTE 6: When testing highly orthotropic laminates, the maximum stress may not always occur in the outer surface of the test specimen.4 Laminated beam theory must be applied to determine the maximum tensile stress at failure. If Eq 3 is used to calculate stress, it will yield an apparent strength based on homogeneous beam theory. This apparent strength is highly dependent on the ply-stacking sequence of highly orthotropic laminates.5.1.2 Flexural Stress for Beams Tested at Large Support Spans (σf)—If support span-to-depth ratios greater than 16 to 1 are used such that deflections in excess of 10 % of the support span occur, the stress in the outer surface of the specimen for a simple beam is reasonably approximated using equation (Eq 4) in 12.3 (see Note 7).NOTE 7: When large support span-to-depth ratios are used, significant end forces are developed at the support noses which will affect the moment in a simple supported beam. Eq 4 includes additional terms that are an approximate correction factor for the influence of these end forces in large support span-to-depth ratio beams where relatively large deflections exist.5.1.3 Flexural Strength (σfM)—Maximum flexural stress sustained by the test specimen (see Note 6) during a bending test. It is calculated according to Eq 3 or Eq 4. Some materials that do not break at strains of up to 5 % give a load deflection curve that shows a point at which the load does not increase with an increase in strain, that is, a yield point (Fig. 1, Curve b), Y. The flexural strength is calculated for these materials by letting P (in Eq 3 or Eq 4) equal this point, Y.FIG. 1 Typical Curves of Flexural Stress (σf) Versus Flexural Strain (εf)NOTE 1: Curve a: Specimen that breaks before yielding.Curve b: Specimen that yields and then breaks before the 5 % strain limit.Curve c: Specimen that neither yields nor breaks before the 5 % strain limit.5.1.4 Flexural Offset Yield Strength—Offset yield strength is the stress at which the stress-strain curve deviates by a given strain (offset) from the tangent to the initial straight line portion of the stress-strain curve. The value of the offset must be given whenever this property is calculated.NOTE 8: Flexural Offset Yield Strength may differ from flexural strength defined in 5.1.3. Both methods of calculation are described in the annex to Test Method D638.5.1.5 Flexural Stress at Break (σfB)—Flexural stress at break of the test specimen during a bending test. It is calculated according to Eq 3 or Eq 4. Some materials give a load deflection curve that shows a break point, B, without a yield point (Fig. 1, Curve a) in which case σfB = σfM. Other materials give a yield deflection curve with both a yield and a break point, B (Fig. 1, Curve b). The flexural stress at break is calculated for these materials by letting P (in Eq 3 or Eq 4) equal this point, B.5.1.6 Stress at a Given Strain—The stress in the outer surface of a test specimen at a given strain is calculated in accordance with Eq 3 or Eq 4 by letting P equal the load read from the load-deflection curve at the deflection corresponding to the desired strain (for highly orthotropic laminates, see Note 6).5.1.7 Flexural Strain, ɛf—Nominal fractional change in the length of an element of the outer surface of the test specimen at midspan, where the maximum strain occurs. Flexural strain is calculated for any deflection using Eq 5 in 12.4.5.1.8 Modulus of Elasticity: 5.1.8.1 Tangent Modulus of Elasticity—The tangent modulus of elasticity, often called the “modulus of elasticity,” is the ratio, within the elastic limit, of stress to corresponding strain. It is calculated by drawing a tangent to the steepest initial straight-line portion of the load-deflection curve and using Eq 6 in 12.5.1 (for highly anisotropic composites, see Note 9).NOTE 9: Shear deflections can seriously reduce the apparent modulus of highly anisotropic composites when they are tested at low span-to-depth ratios.4 For this reason, a span-to-depth ratio of 60 to 1 is recommended for flexural modulus determinations on these composites. Flexural strength should be determined on a separate set of replicate specimens at a lower span-to-depth ratio that induces tensile failure in the outer fibers of the beam along its lower face. Since the flexural modulus of highly anisotropic laminates is a critical function of ply-stacking sequence, it will not necessarily correlate with tensile modulus, which is not stacking-sequence dependent.5.1.8.2 Secant Modulus—The secant modulus is the ratio of stress to corresponding strain at any selected point on the stress-strain curve, that is, the slope of the straight line that joins the origin and a selected point on the actual stress-strain curve. It shall be expressed in megapascals (pounds per square inch). The selected point is chosen at a pre-specified stress or strain in accordance with the appropriate material specification or by customer contract. It is calculated in accordance with Eq 6 by letting m equal the slope of the secant to the load-deflection curve. The chosen stress or strain point used for the determination of the secant shall be reported.5.1.8.3 Chord Modulus (Ef)—The chord modulus is calculated from two discrete points on the load deflection curve. The selected points are to be chosen at two pre-specified stress or strain points in accordance with the appropriate material specification or by customer contract. The chosen stress or strain points used for the determination of the chord modulus shall be reported. Calculate the chord modulus, Ef using Eq 7 in 12.5.2.5.2 Experience has shown that flexural properties vary with specimen depth, temperature, atmospheric conditions, and strain rate as specified in Procedures A and B.5.3 Before proceeding with these test methods, refer to the ASTM specification of the material being tested. Any test specimen preparation, conditioning, dimensions, or testing parameters, or combination thereof, covered in the ASTM material specification shall take precedence over those mentioned in these test methods. Table 1 in Classification System D4000 lists the ASTM material specifications that currently exist for plastics.1.1 These test methods are used to determine the flexural properties of unreinforced and reinforced plastics, including high modulus composites and electrical insulating materials utilizing a three-point loading system to apply a load to a simply supported beam (specimen). The method is generally applicable to both rigid and semi-rigid materials, but flexural strength cannot be determined for those materials that do not break or yield in the outer surface of the test specimen within the 5.0 % strain limit.1.2 Test specimens of rectangular cross section are injection molded or, cut from molded or extruded sheets or plates, or cut from molded or extruded shapes. Specimens must be solid and uniformly rectangular. The specimen rests on two supports and is loaded by means of a loading nose midway between the supports.1.3 Measure deflection in one of two ways; using crosshead position or a deflectometer. Please note that studies have shown that deflection data obtained with a deflectometer will differ from data obtained using crosshead position. The method of deflection measurement shall be reported.NOTE 1: Requirements for quality control in production environments are usually met by measuring deflection using crosshead position. However, more accurate measurement may be obtained by using an deflection indicator such as a deflectometer.NOTE 2: Materials that do not rupture by the maximum strain allowed under this test method may be more suited to a 4-point bend test. The basic difference between the two test methods is in the location of the maximum bending moment and maximum axial fiber stresses. The maximum axial fiber stresses occur on a line under the loading nose in 3-point bending and over the area between the loading noses in 4-point bending. A four-point loading system method can be found in Test Method D6272.1.4 The values stated in SI units are to be regarded as the standard. The values provided in parentheses are for information only.1.5 The text of this standard references notes and footnotes that provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.NOTE 3: This standard and ISO 178 address the same subject matter, but differ in technical content.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test is particularly suited to control and development work. Data obtained by this test method shall not be used to predict the behavior of plastic materials at elevated temperatures except in applications in which the factors of time, temperature, method of loading, and fiber stress are similar to those specified in this test method. The data are not intended for use in design or predicting endurance at elevated temperatures.5.2 For many materials, it is possible there will be a specification that requires the use of this test method, but with some procedural modifications that take precedence when adhering to the specification. Therefore, it is advisable to refer to that material specification before using this test method. Refer to Table 1 in Classification D4000, which lists the ASTM material standards that currently exist.1.1 This test method covers the determination of the temperature at which an arbitrary deformation occurs when specimens are subjected to an arbitrary set of testing conditions.1.2 This test method applies to molded and sheet materials available in thicknesses of 3 mm (1/8 in.) or greater and which are rigid or semirigid at normal temperature.NOTE 1: Sheet stock less than 3 mm (0.125 in.) but more than 1 mm (0.040 in.) in thickness may be tested by use of a composite sample having a minimum thickness of 3 mm. The laminae must be of uniform stress distribution. One type of composite specimen has been prepared by cementing the ends of the laminae together and then smoothing the edges with sandpaper. The direction of loading shall be perpendicular to the edges of the individual laminae.1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.1.4 This standard and ASTM D648 address the same subject matter and are essentially the same test. However, due to known differences in results caused by the differences in heat transfer media, the results from this standard and ASTM D648 must not be compared or considered equivalent.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.NOTE 2: The text of this standard references notes and footnotes that provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.NOTE 3: This standard and ISO 75-1 and ISO 75-2 address the same subject matter, but differ in technical content, and results shall not be compared between the two test methods.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This classification was developed to permit the addition of descriptive symbols and values for further new formulations with improved properties without complete reorganization of the standard and to facilitate the incorporation of future new test methods to keep pace with changing industry requirements.1.1 This classification provides guidance to engineers and users in the selection of practical vinyl chloride plastics for medical applications and further provides a method for specifying these materials by use of a simple line call-out designation. This classification excludes vinyl chloride plastics used in long-term implants.1.2 Use is made of a classification scheme based on the premise that the composition of vinyl chloride plastics, copolymers, fillers, plasticizers, stabilizers, and other additives in these systems can be arranged into characteristic material designations.1.3 In all cases where the provisions of this classification system would conflict with those of the detailed specification for a particular device, the latter shall take precedence.NOTE 1: For cases in which the vinyl chloride plastic may be used for purposes where the requirements are too specific to be completely described by this classification system, it is advisable for the purchaser to consult the supplier to secure adjustment of the properties to suit the actual conditions to which the device is to be subjected.1.4 The biocompatibility of vinyl chloride plastics as a class of materials has not been established. Since many compositions and formulations fall under this class, it is essential that the fabricators/device manufacturers assure the safety and efficacy of the specific composition or formulation, in its intended application, using state-of-the-art test methods.1.5 This classification is to assist the interface between the material supplier and the device manufacturer (fabricator) who purchases a formulated vinyl chloride plastic for a component. For those device manufacturers (fabricators) who do their own formulating, compounding, extrusion, molding, and so forth, this classification does not apply.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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1.1 This test method describes the procedures required to carry out a pure-culture study for evaluating the biodegradation of degradable plastics in submerged culture under aerobic conditions. Degradation will be evaluated by weight loss, tensile strength loss, percent-elongation loss and changes in molecular-weight distribution. 1.2 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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4.1 This practice is intended to simulate the effects produced by exposure to solar radiation through glass. This practice uses exposure in a xenon-arc device equipped with window glass filters and operated in accordance with Practices G151 and G155.NOTE 2: Practice D4674 describes exposures in a device that uses a combination of fluorescent “cool white” and ultraviolet (UV) lamps to simulate the effects of exposures to indoor fluorescent light and window glass filtered daylight.4.2 Warning—Variation in results may be expected when operating conditions are varied within the accepted limits of this practice. Therefore, all references to the use of this practice must be accompanied by a report prepared in accordance with Section 9 that describes the specific operating conditions used. Refer to Practice G151 for detailed information on the caveats applicable to use of results obtained in accordance with this practice.NOTE 3: Additional information on sources of variability and on strategies for addressing variability in the design, execution and data analysis of laboratory accelerated exposure tests is found in Guide G141.4.3 Test results will depend upon the care that is taken to operate the equipment in accordance with Practice G155. Significant factors include regulation of line voltage, temperature and humidity control, and condition and age of the lamps and filters.4.4 Reproducibility of test results between laboratories has been shown to be good when the stability of materials is evaluated in terms of performance ranking compared to other materials or to a control.4,5 Therefore, exposure of a similar material of known performance (a control) at the same time as the test materials is strongly recommended. The number of specimens of the control material should be the same as that used for test materials. It is recommended that at least three replicates of each material be exposed to allow for statistical evaluation of results.1.1 This practice covers specific procedures and test conditions that are applicable for exposure of plastics in window glass-filtered xenon-arc devices in accordance with Practices G151 and G155 for evaluating the stability of plastics intended for use in indoor applications.1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.NOTE 1: There is no known ISO equivalent to this practice.1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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1.1 This practice covers the exposure of plastics to a specific test environment. The test environment is a laboratory-scale reactor that simulates a self-heating composting system and that uses aeration to control maximum temperature. Plastic exposure occurs in the presence of a media undergoing aerobic composting. The standard media simulates a municipal solid waste from which inert materials have been removed. This practice allows for the use of other media to represent particular waste streams. This practice provides exposed specimens for further testing and for comparison with controls. This test environment does not necessarily reproduce conditions that could occur in a particular full-scale composting process. 1.2 Changes in the material properties of the plastic and controls should be determined using appropriate ASTM test procedures. Changes could encompass physical and chemical changes such as disintegration and degradation. 1.3 This practice may be used for different purposes. Therefore, the interested parties must select the following: exposure conditions from those allowed by this practice; criteria for a valid exposure, that is, minimum or maximum change requirements for the compost and controls; and the magnitudes of material properties changes required for the plastic specimens. 1.4 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in Section 8. Note 1-There is no similar or equivalent ISO standard.

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1.1 This practice is intended to define the exposure conditions of plastics at various temperatures when exposed solely to hot air for extended periods of time. Only the procedures for heat exposure are specified, not the test method or specimen. The effect of heat on any particular property may be determined by selection of the appropriate test method and specimen; however, it is recommended that Practice D 3826 be used to determine the embrittlement endpoint, which is defined as that point in the history of a material when 75 % of the specimens tested have a tensile elongation at break of 5 % or less at an initial strain rate of 0.1 mm/mm min.1.2 This practice should be used as a guide for comparing the thermal-aging characteristics of materials as measured by the change in some property of interest (that is, embrittlement by means of loss of elongation). It is very similar to Practice D3045 but is intended for use in evaluating plastics designed to be oxidized easily after use. The exposure times used for this practice will be significantly shorter than those used for Practice D3045.1.3 The type of oven used can affect the results obtained from this practice. The user can use one of two methods for oven exposure. The results based on one method should not be mixed with those based on the other.1.3.1 Procedure A: Gravity-Convection Oven--Recommended for film specimens having a nominal thickness not greater than 0.25 mm (0.010 in.).1.3.2 Procedure B: Forced-Ventilation Oven--Recommended for specimens having a nominal thickness greater than 0.25 mm (0.010 in.).1.4 This practice recommends procedures for comparing the thermal aging characteristics of materials at a single temperature. Recommended procedures for determining the thermal aging characteristics of a material at a series of temperatures for the purpose of estimating time to a defined property change at some lower temperature are also described. This practice does not predict thermal aging characteristics where interactions between stress, environment, temperature, and time control failure.1.5 The values stated in SI units are to be regarded as the standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.Note 1--There is no ISO standard that is equivalent to this standard.

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4.1 The folding endurance is frequently used to estimate the ability of the paper and plastics film to withstand repeated bending, folding, and creasing.4.2 Folding endurance has also been found useful in measuring the deterioration of paper and plastics film upon aging.1.1 This test method describes the use of the M.I.T.-type folding apparatus for determining folding endurance of paper and plastics film. The M.I.T. tester can be adjusted for samples of any thickness; however, if the outer layers thicker than about 0.25 mm (0.01 in.) rupture during the first few folds, the test loses its significance. The procedure for the Schopper-type apparatus is given in Test Method D643.1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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