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5.1 This test method provides a simple means of characterizing the important rheological properties and viscosity of thermoplastic polymers using very small amounts of material (approximately 25 to 50 mm in diameter by 1 to 3 mm in thickness ... approximately 3 to 5 g). Data are generally used for quality control, research and development, and establishment of optimum processing conditions.5.2 Dynamic mechanical testing provides a sensitive method for determining molten polymer properties by measuring the elastic and loss moduli as a function of frequency, strain, temperature, or time. Plots of viscosity, storage, and loss moduli, and tan delta as a function of the aforementioned process parameters provide graphical representation indicative of molecular weight, molecular weight distribution, effects of chain branching, and melt-processability for specified conditions.5.2.1 Observed data are specific to experimental conditions. Reporting in full (as described in this test method) the conditions under which the data was obtained is essential to assist users with interpreting the data an reconciling apparent or perceived discrepancies.5.3 Values obtained in this test method can be used to assess the following:5.3.1 Complex viscosity of the polymer melt as a function of dynamic oscillation,5.3.2 Processing viscosity, minimum as well as changes in viscosity as a function of experimental parameters,5.3.3 Effects of processing treatment,5.3.4 Relative polymer behavioral properties, including viscosity and damping, and5.3.5 Effects of formulation additives that might affect processability or performance.5.4 Before proceeding with this test method, refer to the specification for the material being tested. Any test specimen preparation, conditioning, dimensions, or testing parameters, or combination thereof, covered in the relevant ASTM materials specification shall take precedence over those mentioned in the test method. If there are no relevant ASTM material specifications, then the default conditions apply.1.1 This test method outlines the use of dynamic mechanical instrumentation in determining and reporting the rheological properties of thermoplastic resins and other types of molten polymers. The method is useful for determining the complex viscosity and other significant viscoelastic characteristics of such materials as a function of frequency, strain amplitude, temperature, and time. It is known that fillers and other additives influence rheological properties.1.2 It incorporates a laboratory test method for determining the relevant rheological properties of a polymer melt subjected to various oscillatory deformations on an instrument of the type commonly referred to as a mechanical or dynamic spectrometer.1.3 This test method is intended to provide a means of determining the rheological properties of molten polymers, such as thermoplastics and thermoplastic elastomers over a range of temperatures by nonresonant, forced-vibration techniques. Plots of modulus, viscosity, and tan delta as a function of dynamic oscillation (frequency), strain amplitude, temperature, and time are indicative of the viscoelastic properties of a molten polymer.1.4 This test method is valid for a wide range of frequencies, typically from 0.01 Hz to 100 Hz.1.5 This test method is intended for homogenous and heterogeneous molten polymeric systems and composite formulations containing chemical additives, including fillers, reinforcements, stabilizers, plasticizers, flame retardants, impact modifiers, processing aids, and other important chemical additives often incorporated into a polymeric system for specific functional properties, and which could affect the processability and functional performance. These polymeric material systems have molten viscosities typically less than 106 Pa·s (107 poise).1.6 Test data obtained by this test method are relevant and appropriate for use in engineering design.1.7 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.NOTE 1: This test method is equivalent to ISO 6721, Part 10.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Dielectric measurement and testing provide a method for determining the permittivity and loss factors as a function of temperature, frequency, time, or a combination of these variables. Plots of the dielectric properties against these variables yield important information and characteristics about the specimen under test.This procedure can be used to do the following:5.2.1 Locate transition temperatures of polymers and other organic materials, that is, changes in molecular motion (or atomic motion in the case of ions) of the material. In temperature regions where significant changes occur, permittivity increases with increasing temperature (at a given frequency) or with decreasing frequency (at constant temperature). A maximum is observed for the loss factor in cases where dipole motions dominate over ionic movement.35.2.2 Track the reaction in polymerization and curing reactions. This may be done under either isothermal or nonisothermal conditions. Increasing molecular weight or degree of crosslinking normally leads to decreases in conductivity.45.2.3 Determine diffusion coefficients of polar gases or liquids into polymer films on dielectric sensors. The observed change in permittivity typically is linear with diffusant concentration, as long as the total concentration is relatively low.5This procedure can be used, for example, to evaluate by comparison to known reference materials:5.3.1 The mix ratio of two different organic materials. This may be determined either through use of permittivity or loss factor values. In early studies, permittivity has been found to be linear with concentration.65.3.2 The degree of phase separation in multicomponent systems.5.3.3 The filler type, amount, pretreatment, and dispersion.This test method can be used for observing annealing and the submelting point crystallization process.This test method can be used for quality control, specification acceptance, and process control.1.1 This test method describes the gathering and reporting of dynamic dielectric data. It incorporates laboratory test method for determining dynamic dielectric properties of specimens subjected to an oscillatory electric field using a variety of dielectric sensor/cell configurations on a variety of instruments called dielectric, microdielectric, DETA (DiElectric Thermal Analysis), or DEA (DiElectric Analysis) analyzers.1.2 This test method determines permittivity, loss factor, ionic conductivity (or resistivity), dipole relaxation times, and transition temperatures, and is intended for materials that have a relative permittivity in the range of 1 to 105; loss factors in the range of 0 to 108; and, conductivities in the range 10 16to 1010S/cm.1.3 The test method is primarily useful when conducted over a range of temperatures for nonreactive systems (160C to degradation) and over time (and temperature) for reactive systems and is valid for frequencies ranging from 1 mHz to 100 kHz.1.4 Apparent discrepancies may arise in results obtained under differing experimental conditions. Without changing the observed data, completely reporting the conditions (as described in this test method) under which the data were obtained, in full, will enable apparent differences observed in another study to be reconciled.1.5 SI units are the standard.This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 10.

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5.1 Many petroleum products, and some non-petroleum materials, are used as lubricants, and the correct operation of the equipment depends upon the appropriate viscosity of the liquid being used. In addition, the viscosity of many petroleum fuels is important for the estimation of optimum storage, handling, and operational conditions. Thus, the accurate determination of viscosity is essential to many product specifications.1.1 This test method specifies a procedure for the determination of the kinematic viscosity, ν, of liquid petroleum products, both transparent and opaque, by measuring the time for a volume of liquid to flow under gravity through a calibrated glass capillary viscometer. The dynamic viscosity, η, can be obtained by multiplying the kinematic viscosity, ν, by the density, ρ, of the liquid.NOTE 1: For the measurement of the kinematic viscosity and viscosity of bitumens, see also Test Methods D2170 and D2171.NOTE 2: ISO 3104 corresponds to Test Method D445 – 03.1.2 The result obtained from this test method is dependent upon the behavior of the sample and is intended for application to liquids for which primarily the shear stress and shear rates are proportional (Newtonian flow behavior). If, however, the viscosity varies significantly with the rate of shear, different results may be obtained from viscometers of different capillary diameters. The procedure and precision values for residual fuel oils, which under some conditions exhibit non-Newtonian behavior, have been included.1.3 The range of kinematic viscosities covered by this test method is from 0.2 mm2/s to 300 000 mm2/s (see Table A1.1) at all temperatures (see 6.3 and 6.4). The precision has only been determined for those materials, kinematic viscosity ranges and temperatures as shown in the footnotes to the precision section.1.4 The values stated in SI units are to be regarded as standard. The SI unit used in this test method for kinematic viscosity is mm2/s, and the SI unit used in this test method for dynamic viscosity is mPa·s. For user reference, 1 mm2/s = 10-6 m2/s = 1 cSt and 1 mPa·s = 1 cP = 0.001 Pa·s.1.5 WARNING—Mercury has been designated by many regulatory agencies as a hazardous substance that can cause serious medical issues. Mercury, or its vapor, has been demonstrated to be hazardous to health and corrosive to materials. Use Caution when handling mercury and mercury-containing products. See the applicable product Safety Data Sheet (SDS) for additional information. The potential exists that selling mercury or mercury-containing products, or both, is prohibited by local or national law. Users must determine legality of sales in their location.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 It is well understood how to measure the forces applied to a specimen under static conditions. Practices E4 details the required process for verifying the static force measurement capabilities of testing machines. During dynamic operation however, additional errors may manifest themselves in a testing machine. Further verification is necessary to confirm the dynamic force measurement capabilities of testing machines.NOTE 1: The static machine verification accomplished by Practices E4 simply establishes the reference. Indicated forces measured from the force cell are compared with the dynamometer conditioned forces statically for confirmation and then dynamically for dynamic verification of the fatigue testing system's force output.NOTE 2: The dynamic accuracy of the force cell's output will not always meet the accuracy requirement of this standard without correction. Dynamic correction to the force cell output can be applied provided that verification is performed after the correction has been applied.NOTE 3: Overall test accuracy is a combination of measurement accuracy and control accuracy. This practice provides methods to evaluate either or both. As control accuracy is dependent on many more variables than measurement accuracy it is imperative that the test operator utilize appropriate measurement tools to confirm that the testing machine’s control behavior is consistent between verification activities and actual testing activities.4.2 Dynamic errors are primarily span dependent, not level dependent. That is, the error for a particular force endlevel during dynamic operation is dependent on the immediately preceding force endlevel. Larger spans imply larger absolute errors for the same force endlevel.4.3 Due to the many test machine factors that influence dynamic force accuracy, verification is recommended for every new combination of potential error producing factors. Primary factors are specimen design, machine configuration, test frequency, and loading span. Clearly, performing a full verification for each configuration is often impractical. To address this problem, dynamic verification is taken in two parts.4.3.1 First, one or more full verifications are performed at least annually. The main body of this practice describes that procedure. This provides the most accurate estimate of dynamic errors, as it will account for electronic as well as acceleration-induced sources of error.4.3.2 The second part, described in Annex A1, is a simplified verification procedure. It provides a simplified method of estimating acceleration-induced errors only. This procedure is to be used for common configuration changes (that is, specimen/grip/crosshead height changes).4.4 Dynamic verification of the fatigue system is recommended over the entire range of force and frequency over which the planned fatigue test series is to be performed. Endlevels are limited to the machine's verified static force as defined by the current static force verification when tested in accordance with Practices E4.NOTE 4: There is uncertainty as to whether or not the vibration in a frame will be different when operating in compression as opposed to tension. As a consequence, this practice recommends performing verifications at maximum tension and maximum compression endlevels. The total span does not need to be between those two levels, but can be performed as two tests.NOTE 5: Primary electronic characteristics affecting dynamic measurement accuracy are noise and bandwidth. Excessive noise is generally the dominant effect at the minimum test frequency. Insufficient bandwidth-induced errors are generally most significant at the maximum test frequency.1.1 This practice covers procedures for the dynamic verification of cyclic force amplitude control or measurement accuracy during constant amplitude testing in an axial fatigue testing system. It is based on the premise that force verification can be done with the use of a strain gaged elastic element. Use of this practice gives assurance that the accuracies of forces applied by the machine or dynamic force readings from the test machine, at the time of the test, after any user applied correction factors, fall within the limits recommended in Section 9. It does not address static accuracy which must first be addressed using Practices E4 or equivalent.1.2 Verification is specific to a particular test machine configuration and specimen. This standard is recommended to be used for each configuration of testing machine and specimen. Where dynamic correction factors are to be applied to test machine force readings in order to meet the accuracy recommended in Section 9, the verification is also specific to the correction process used. Finally, if the correction process is triggered or performed by a person, or both, then the verification is specific to that individual as well.1.3 It is recognized that performance of a full verification for each configuration of testing machine and specimen configuration could be prohibitively time consuming and/or expensive. Annex A1 provides methods for estimating the dynamic accuracy impact of test machine and specimen configuration changes that may occur between full verifications. Where test machine dynamic accuracy is influenced by a person, estimating the dynamic accuracy impact of all individuals involved in the correction process is recommended. This practice does not specify how that assessment will be done due to the strong dependence on owner/operators of the test machine.1.4 This practice is intended to be used periodically. Consistent results between verifications is expected. Failure to obtain consistent results between verifications using the same machine configuration implies uncertain accuracy for dynamic tests performed during that time period.1.5 This practice addresses the accuracy of the testing machine's force control or indicated forces, or both, as compared to a dynamometer's indicated dynamic forces. Force control verification is only applicable for test systems that have some form of indicated force peak/valley monitoring or amplitude control. For the purposes of this verification, the dynamometer's indicated dynamic forces will be considered the true forces. Phase lag between dynamometer and force transducer indicated forces is not within the scope of this practice.1.6 The results of either the Annex A1 calculation or the full experimental verification must be reported per Section 10 of this standard.1.7 This practice provides no assurance that the shape of the actual waveform conforms to the intended waveform within any specified tolerance.1.8 This standard is principally focused at room temperature operation. It is believed there are additional issues that must be addressed when testing at high temperatures. At the present time, this standard practice must be viewed as only a partial solution for high temperature testing.1.9 The values stated in inch-pound units are to be regarded as standard. No other units of measurement are included in this standard.1.10 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.11 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test method is designed to quantify the static and dynamic characteristics of different designs of single level spinal constructs. Wear may also be assessed for implants that allow motion using testing medium (see 6.1) for simulating the physiologic environment at 37 °C. Wear is assessed using a weight loss method in addition to dimensional analyses. Weight loss is determined after subjecting the implants to dynamic profiles specified in this test method. This information will allow the manufacturer or end user of the product to understand how the specific device in question performs under the test conditions prescribed in this test method.4.2 This test method is intended to be applicable for single level extra-discal spinal constructs. Three different types of fixtures are specified for testing single level extra-discal spinal constructs See Fig. 2, Fig. 4, and Fig. 5. See also Table 1.4.3 Implants may be designed using a variety of materials (for example, ceramics, metals, polymers, or combinations thereof), and it is the goal of this test method to enable a comparison of the static, dynamic, and wear properties generated by these devices, regardless of material and type of device.AbstractThis test method deals with static, dynamic, and wear testing of extra-discal motion preserving implants. These implants are intended to augment spinal stability without significant tissue removal while allowing motion of the functional spinal unit(s). Wear is assessed using a weight loss method and a dimensional analysis for determining wear of components used in extra-discal spinal motion preserving procedures, using testing medium as defined in this test method. This test method is not intended to address facet arthroplasty devices and any potential failure mode as it relates to the fixation of the device to its bony interfaces; and does not prescribe methods for assessing the mechanical characteristics of the device in translation. The static test includes the static flexion test, static extension test, static torsion test, static lateral bending test, and fatigue tests. Wear test includes flexion/extension wear assessment, rotational wear assessment, and bending wear assessment. The apparatus which shall be used includes implant components and spinal testing apparatus. The calculation and interpretation of wear results are also elaborated.1.1 This test method describes methods to assess the static and dynamic properties of single level spinal constructs.1.2 An option for assessing wear using a weight loss method and a dimensional analysis is given. This method, described herein, is used for the analysis of devices intended for motion preservation, using testing medium as defined in this standard (6.1).1.3 This test method is not intended to address any potential failure mode as it relates to the fixation of the device to its bony interfaces.1.4 It is the intent of this test method to enable single level extra-discal spinal constructs with regard to kinematic, functional, and wear characteristics when tested under the specified conditions.1.5 This test method is not intended to address facet arthroplasty devices.1.6 In order that the data be reproducible and comparable within and between laboratories, it is essential that uniform procedures be established. This test method is intended to facilitate uniform testing methods and data reporting.1.7 The motion profiles specified by this test method do not necessarily accurately reproduce those occurring in vivo. Rather this method provides useful boundary/endpoint conditions for evaluating implant designs in a functional manner.1.8 This test method is not intended to be a performance standard. It is the responsibility of the user of this test method to characterize the safety and effectiveness of the device under evaluation.1.9 Multiple test methods are included in this standard. However, it must be noted that the user is not obligated to test using all of the described methods. Instead, the user should only select test methods that are appropriate for a particular device design. In most instances, only a subset of the herein described test methods will be required.1.10 The values stated in SI units are to be regarded as the standard with the exception of angular measurements, which may be reported in either degrees or radians. No other units of measurement are included in this standard.1.11 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.12 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The tackiness test is designed for quantifying how sticky or non-sticky a material is at a certain temperature. The test should be run at various temperatures expected in the field for tack coat materials. If the results show the residue is tacky at pavement temperatures, the material may not be suitable for applications like less-tracking tack coats and bond coats.5.2 Determining the temperature that the residue becomes tacky by increasing the temperature in successive testing can give formulators an indicator of performance.NOTE 2: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.1.1 This test method covers the determination of pull-off force and pull-off work of asphalt binders and emulsified asphalt residue by means of pull-off testing. The tackiness test is conducted using the dynamic shear rheometer (DSR) at one or more temperatures.NOTE 1: This standard may be used for unconditioned material or material conditioned in accordance with Test Method D2872. The majority of development work on this test method was performed on unconditioned material. The emulsified asphalt residue should never be conditioned.1.2 A precision and bias statement for this standard has not been developed at this time. Therefore, this standard should not be used for acceptance or rejection of a material for purchasing purposes.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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1.1 This test method covers dynamic tear testing and is applicable to graphitic cast irons and establishes the transition temperature from examination of fracture appearance. Details of apparatus, specimens, and procedures are included.1.2 The values stated in SI units are to be regarded as the standard. The inch-pound units given in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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5.1 This test method is useful because the choice of a solvent system for removing water-formed deposits depends upon the ability of the dynamic solvent system to dissolve both unattached and attached deposits.1.1 This test method covers the determination of the relative efficacy of dynamic solvent systems for dissolving water-formed deposits that have been removed from the underlying material or deposits attached to the underlying material.1.2 The nature of this test method is such that statements of precision and bias as determined by round robin tests could mislead users of this test method (see Sections 11 and 12). Therefore, no precision and bias statements are made.1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method provides a simple means of characterizing the cure behavior of thermosetting resins using very small amounts of material (fewer than 3 to 5 g). The data obtained may be used for quality control, research and development, and establishment of optimum processing conditions.5.2 Dynamic mechanical testing provides a sensitive method for determining cure characteristics by measuring the elastic and loss moduli as a function of temperature or time, or both. Plots of cure behavior and tan delta of a material versus time provide graphical representation indicative of cure behavior under a specified time-temperature profile.5.3 This test method can be used to assess the following:5.3.1 Cure behavior, including rate of cure, gel, and cure time.5.3.2 Processing behavior, as well as changes as a function of time/temperature.NOTE 3: The presence of the substrate prevents an absolute measure, but allows relative measures of flow behavior during cure.5.3.3 The effects of processing treatment.5.3.4 Relative resin behavioral properties, including cure behavior and damping.5.3.5 The effects of substrate types on cure.NOTE 4: Due to the rigidity of a supporting braid, the gel time obtained from dynamic mechanical traces will be longer than actual gel time of the unsupported resin measured at the same frequency. This difference will be greater for composites having greater support-to-polymer rigidity ratios.35.3.6 Effects of formulation additives that might affect processability or performance.5.4 For many materials, there may be a specification that requires the use of this test method, but with some procedural modifications that take precedence when adhering to the specification. Therefore, it is advisable to refer to that material specification before using this test method. Table 1 of Classification System D4000 lists the ASTM materials standards that currently exist.1.1 This test method covers the use of dynamic-mechanical-oscillation instrumentation for gathering and reporting the thermal advancement of cure behavior of thermosetting resin. It may be used for determining the cure properties of both unsupported resins and resins supported on substrates subjected to various oscillatory deformations.1.2 This test method is intended to provide a means for determining the cure behavior of supported and unsupported thermosetting resins over a range of temperatures by free vibration as well as resonant and nonresonant forced-vibration techniques, in accordance with Practice D4065. Plots of modulus, tan delta, and damping index as a function of time/temperature are indicative of the thermal advancement or cure characteristics of a resin.1.3 This test method is valid for a wide range of frequencies, typically from 0.01 to 100 Hz. However, it is strongly recommended that low-frequency test conditions, generally below 1.5 Hz, be utilized as they generally will result in more definitive cure-behavior information.1.4 This test method is intended for resin/substrate composites that have an uncured effective elastic modulus in shear greater than 0.5 MPa.1.5 Apparent discrepancies may arise in results obtained under differing experimental conditions. These apparent differences from results observed in another study can usually be reconciled, without changing the observed data, by reporting in full (as described in this test method) the conditions under which the data were obtained.1.6 Due to possible instrumentation compliance, especially in the compressive mode, the data generated may indicate relative and not necessarily absolute property values.1.7 Test data obtained by this test method are relevant and appropriate for use in engineering design.1.8 The values stated in SI units are to be regarded as the standard.1.9 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Note 5.NOTE 1: There is no known ISO equivalent to this standard.1.10 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The ability to correlate results of analyzers to sieve sets enables the use of non-sieve methods to be employed that give comparable results to each other.5.2 The use of analyzers for proppant measurement has the benefit of providing particle shape characteristics which are important in the performance of these materials. Shape analysis is currently done by operator’s determination based on a visual observation of a small number of particles per API 19C. Available information from imaging analysis of many particles can be used to assess the proppant shape characteristics as opposed to just a small number.1.1 This practice describes procedural steps to create a correlation that can be used to compare results of proppant size distributions between dynamic imaging analyzers (analyzers) and prescribed sieve sets.1.2 The proppant size and distribution specifications that are included in this practice are listed in API Standard 19C (API 19C) and shown in Table 1, however as industry evolves additional specifications may come into use and this practice can be used with those as well.1.3 This practice may not be applicable to all proppant types and designations. The acceptability of the correlations determined are judged by the operator.1.4 The values stated in SI units are to be regarded as the standard, except sieve designations are typically identified using the ‘alternative’ system in accordance with Practice E11, such as 3 in. and No. 200 instead of the ‘standard’ system of 75 mm and 75 µm, respectively.1.5 Observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026, unless superseded by this standard.1.5.1 The procedures used to specify how data are collected/recorded and calculated in Practice D6026 are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of these test methods to consider significant digits used in analysis methods for engineering data.1.6 This practice offers a set of instructions for performing one or more specific operations. This document cannot replace education or experience and should be used in conjunction with professional judgment. Not all aspects of this practice may be applicable in all circumstances. This ASTM standard is not intended to represent or replace the standard of care by which the adequacy of a given professional service must be judged, nor should this document be applied without consideration of a project’s many unique aspects. The word “Standard” in the title means only that the document has been approved through the ASTM consensus process.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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1.1 This specification covers two types of asphalt intended for use in built-up roof construction, construction of some modified bitumen systems, construction of bituminous vapor retarder systems, and for adhering insulation boards used in various types of roof systems. The specification is intended for general classification purposes only and does not imply restrictions on the slope at which an asphalt must be used.1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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