5.1 The test method is designed to show whether or not a material meets the specifications as given in Specifications C753 or C776.5.2 The powder’s stoichiometry is useful for predicting the oxide's sintering behavior in the pellet production process.1.1 This test method covers the determination of uranium and the oxygen to uranium atomic ratio in nuclear grade uranium dioxide powder and pellets.1.2 This test method does not include provisions for preventing criticality accidents or requirements for health and safety. Observance of this test method does not relieve the user of the obligation to be aware of and conform to all international, national, or federal, state and local regulations pertaining to possessing, shipping, processing, or using source or special nuclear material.1.3 This test method also is applicable to UO3 and U3O8 powder.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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5.1 This test method is used to determine the time to sustained flaming and heat release of materials and composites exposed to a prescribed initial test heat flux in the cone calorimeter apparatus.5.2 Quantitative heat release measurements provide information that can be used for upholstery and mattress product designs and product development.5.3 Heat release measurements provide useful information for product development by yielding a quantitative measure of specific changes in fire performance caused by component and composite modifications. Heat release data from this test method will not be predictive of product behavior if the product does not spread flame over its surface under the fire exposure conditions of interest.5.4 Test Limitations—The test data are invalid if either of the following conditions occur: (1) explosive spalling; or (2) the specimen swells sufficiently prior to ignition to touch the spark plug, or the specimen swells up to the plane of the heater base during combustion.1.1 This fire-test-response test method can be used to determine the ignitability and heat release from the composites of contract, institutional, or high-risk occupancy upholstered furniture or mattresses using a bench scale oxygen consumption calorimeter.1.2 This test method provides for measurement of the time to sustained flaming, heat release rate, peak and total heat release, and effective heat of combustion at a constant initial test heat flux of 35 kW/m2. This test method is also suitable to obtain heat release data at different heat fluxes. The specimen is oriented horizontally, and a spark ignition source is used.1.3 The times to sustained flaming, heat release, and effective heat of combustion are determined using the apparatus and procedures described in Test Method E1354.1.4 The tests are performed on bench-scale specimens combining the furniture or mattress outer layer components. Frame elements are not included.1.5 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.6 This standard is used to measure and describe the response of materials, products, or assemblies to heat and flame under controlled conditions, but does not by itself incorporate all factors required for fire hazard or fire risk assessment of the materials, products, or assemblies under actual fire conditions.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific precautionary statements, see Section 6.1.8 Fire testing is inherently hazardous. Adequate safeguards for personnel and property shall be employed in conducting these tests.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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5.1 MOX is used as a nuclear-reactor fuel. This test method is designed to determine whether the O/M ratio meets the requirements of the fuel specification. Examples for establishing a fuel specification are given in Specification C833.5.2 This method is suitable for all sintered MOX pellets containing up to 12 weight % PuO2 when the UO2 and PuO2 meet the requirements of Specifications C753 and C757.1.1 This practice is an alternative method to Test Method C698 for the determination of the oxygen-to-metal atom ratio (O/M) in sintered mixed oxide fuel (MOX) pellets. The method presented in Test Method C698 is a one-step thermogravimetric method for determining O/M ratio in sintered MOX powders and pellets. As stated in Test Method C698, thermogravimetric methods using a two-step heating cycle are also satisfactory (1, 2).2 The method presented in this test method is a two-step heating cycle method. This test method is applicable to sintered MOX pellets containing up to 10 weight percent PuO2.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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5.1 O2GTR at a given temperature and %RH is an important determinant of the packaging protection afforded by barrier materials. It is not, however the sole determinant, and additional tests, based on experience, must be used to correlate packaging performance with O2GTR. It is suitable as a referee method of testing, provided that purchaser and seller have agreed on sampling procedures, standardization procedures, test conditions and acceptance criteria.1.1 This test method covers a procedure for determination of the rate of transmission of oxygen gas, at steady-state, at a given temperature and %RH level, through film, sheeting, laminates, co-extrusions, or plastic-coated papers or fabrics. This test method extends the common practice dealing with zero humidity or, at best, an assumed humidity. Humidity plays an important role in the oxygen gas transmission rate (O2GTR) of many materials. This test method provides for the determination of oxygen gas transmission rate (O2GTR), the permeance of the film to oxygen gas (PO2), the permeation coefficient of the film to its thickness (P”O2), and oxygen permeability coefficient (PʹO2) in the case of homogeneous materials at given temperature and %RH level(s).1.2 The values stated in SI units are to be regarded as the standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 9.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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4.1 These test methods for the chemical analysis of metals and alloys are primarily intended to test such materials for compliance with compositional specifications. It is assumed that all who use these test methods will be trained analysts, capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory.1.1 These test methods cover the determination of carbon, sulfur, nitrogen, and oxygen, in steel, iron, nickel, and cobalt alloys having chemical compositions within the following limits:Element Mass Fraction Range, %Aluminum 0.001 to 18.00Antimony 0.002 to 0.03Arsenic 0.0005 to 0.10Beryllium 0.001 to 0.05Bismuth 0.001 to 0.50Boron 0.0005 to 1.00Cadmium 0.001 to 0.005Calcium 0.001 to 0.05Carbon 0.001 to 4.50Cerium 0.005 to 0.05Chromium 0.005 to 35.00Cobalt 0.01 to 75.0Niobium 0.002 to 6.00Copper 0.005 to 10.00Hydrogen 0.0001 to 0.0030Iron 0.01 to 100.0Lead 0.001 to 0.50Magnesium 0.001 to 0.05Manganese 0.01 to 20.0Molybdenum 0.002 to 30.00Nickel 0.005 to 84.00Nitrogen 0.0005 to 0.50Oxygen 0.0005 to 0.03Phosphorus 0.001 to 0.90Selenium 0.001 to 0.50Silicon 0.001 to 6.00Sulfur 0.002 to 0.35Tantalum 0.001 to 10.00Tellurium 0.001 to 0.35Tin 0.002 to 0.35Titanium 0.002 to 5.00Tungsten 0.005 to 21.00Vanadium 0.005 to 5.50Zinc 0.005 to 0.20Zirconium 0.005 to 2.5001.2 The test methods appear in the following order: SectionsCarbon, Total, by the Combustion and Infrared Absorption or Thermal Conductivity Detection Test Method 10 – 20 Nitrogen by the Inert Gas Fusion and Thermal Conductivity Detection Test Method 32 – 42 Oxygen by the Inert Gas Fusion and Infrared Absorption or Thermal Conductivity Detection Test Method 43 – 54 Sulfur by the Combustion-Infrared Absorption Detection Test Method 55 – 65 Sulfur by the Combustion–Infrared Absorption Test Method (Potassium Sulfate Calibration) – Discontinued 2018 21 – 311.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazards statements are given in Section 6.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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5.1 This test method provides a means to determine various fire-test-response characteristics, including the time to sustained flaming and the heat release rate, of composites exposed to a prescribed initial test heat flux in the cone calorimeter apparatus, after they have been vandalized in a prescribed manner, to expose the filling material.5.2 It is clearly impossible to predict the manner in which a mattress or furniture will be vandalized. The objective of this test method is to develop data indicating the effect of violating the integrity of the fabric (or the fabric plus interliner composite) protection and exposing the padding to the source of heat (see Appendix X3).5.3 Quantitative heat release measurements provide information which is useful for product design and product development, for mattresses or furniture destined for correctional occupancies.5.4 Heat release measurements provide useful information for product development by giving a quantitative measure of specific changes in fire performance caused by component and composite modifications. Heat release data from this method will not be predictive of product behavior if the product will not spread flame over its surface under the fire exposure conditions of interest.5.5 The use of test specimens simulating vandalism allows the investigation of the variation in response between the system as designed by the manufacturer and the way the system is occasionally present in actual use, with the filling material exposed to the incident energy.5.6 This test method allows alternative strategies to be employed for producing a product (mattress or upholstered furniture) with the required fire-test-response characteristics for the scenario under consideration.5.7 Limitations: 5.7.1 The test data are invalid if any of the events in 5.7.1.1 or 5.7.1.2 occur.5.7.1.1 Explosive spalling.5.7.1.2 The specimen swells sufficiently prior to ignition to touch the spark plug or swells up to the plane of the heater base during combustion.5.7.2 This test method is not applicable to ignition by cigarettes, or by any other smoldering source.5.7.3 The ignition source in this test method is a radiant energy source of relatively high intensity (35 kW/m2 initial test heat flux). It has been shown that this source models well, for furniture composites, a full scale source equivalent to five sheets of newspaper (2). It has also been shown that upholstered furniture and mattresses, particularly in public occupancies, are, on occasion, involved in fires after exposure to flaming ignition sources, However, it is not known what fraction of actual flaming mattress or furniture fires occur with ignitions more or less intense than the one modeled here.5.7.4 It is not known whether the results of this test method will be equally valid when it is carried out under conditions different from the specified ones. In particular, it is unclear whether the use of a different ignition source, or the same ignition source but at a different initial test heat flux, will change relative results.5.7.5 The value of heat release rate corresponding to the critical limit between propagating mattress fires and non-propagating mattress fires is not known.5.7.6 It is not known what fraction of the vandalism that occurs is represented by the prescribed model used in this standard. However, the method described here is adequate to address one of the major objectives of the standard, namely investigate the effect of the exposed filling material on the fire-test-response characteristics of the composite.1.1 This fire-test-response test method is designed for use to determine various fire-test-response characteristics, including ignitability and heat release rate, from composites of mattresses or furniture, or correctional facilities, which have been vandalized in a prescribed manner to expose the filling material, by using a bench scale oxygen consumption calorimeter.1.2 This test method provides for measurements of the time to sustained flaming, heat release rate, peak and total heat release, and effective heat of combustion at a constant radiant initial test heat flux of 35 kW/m2. See 5.7 for limitations.1.3 The apparatus used in this test method is also capable of determining heat release data at different initial test heat fluxes.1.4 The specimen is oriented horizontally and a spark ignition source is used.1.5 All fire-test-response characteristics are determined using the apparatus and the procedures described in Test Method E1354.1.6 The tests are done on bench-scale specimens combining the mattress or furniture outer layer components. Frame elements are not included.1.7 The vandalism is simulated by causing a prescribed cut on the outer layer of the composite, deep enough to expose the filling material to the incident radiation.1.8 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.9 This standard is used to measure and describe the response of materials, products, or assemblies to heat and flame under controlled conditions, but does not by itself incorporate all factors required for fire hazard or fire risk assessment of the materials, products, or assemblies under actual fire conditions.1.10 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific safety precautions, see Section 7.1.11 Fire testing is inherently hazardous. Adequate safeguards for personnel and property shall be employed in conducting these tests.1.12 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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