5.1 Cyanide and hydrogen cyanide are highly toxic. Regulations have been established to require the monitoring of cyanide in industrial and domestic wastewaters and surface waters.45.2 This test method is applicable for natural water, saline waters, and wastewater effluent.5.3 This test method may be used for process control in wastewater treatment facilities.5.4 The spot test outlined in Test Methods D2036, Annex A1, can be used to detect cyanide and thiocyanate in water or wastewater, and to approximate its concentration.1.1 This test method is used for determining total cyanide in drinking and surface waters, as well as domestic and industrial wastes. Cyanide ion (CN–), hydrogen cyanide in water (HCN(aq)), and the cyano-complexes of zinc, copper, cadmium, mercury, nickel, silver, and iron may be determined by this test method. Cyanide ions from Au(I), Co(III), Pd(II), and Ru(II) complexes are only partially determined.1.2 The method detection limit (MDL) is 1.0 μg/L cyanide and the minimum level (ML) is 3 μg/L. The applicable range of the method is 3 to 500 μg/L cyanide using a 200-μL sample loop. Extend the range to analyze higher concentrations by sample dilution or changing the sample loop volume.1.3 This test method can be used by analysts experienced with equipment using segmented flow analysis (SFA) and flow injection analysis (FIA) or working under the close supervision of such qualified persons.1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in 8.5 and Section 9.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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定价： 646元 加购物车

定价： 646元 加购物车

定价： 712元 加购物车

定价： 646元 加购物车

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5.1 This test method is used for determination of the carbon content of water from a variety of natural, domestic, and industrial sources. In its most common form, this test method is used to measure organic carbon as a means of monitoring organic pollutants in high purity and drinking water. These measurements are also used in monitoring waste treatment processes.5.2 The relationship of TOC to other water quality parameters such as chemical oxygen demand (COD) and total oxygen demand (TOD) is described in the literature (6).1.1 This test method covers the determination of total carbon (TC), inorganic carbon (IC), and total organic carbon (TOC) in water in the range from 0.5 to 30 mg/L of carbon. Higher levels may be determined by sample dilution. The test method utilizes ultraviolet-persulfate oxidation of organic carbon, coupled with a CO2 selective membrane to recover the CO2 into deionized water. The change in conductivity of the deionized water is measured and related to carbon concentration in the oxidized sample. Inorganic carbon is determined in a similar manner without the requirement for oxidation. In both cases, the sample is acidified to facilitate CO2 recovery through the membrane. The relationship between the conductivity measurement and carbon concentration is described by a set of chemometric equations for the chemical equilibrium of CO2, HCO3−, H+, and the relationship between the ionic concentrations and the conductivity. The chemometric model includes the temperature dependence of the equilibrium constants and the specific conductances.1.2 This test method has the advantage of a very high sensitivity detector that allows very low detection levels on relatively small volumes of sample. Also, use of two measurement channels allows determination of CO2 in the sample independently of organic carbon. Isolation of the conductivity detector from the sample by the CO2 selective membrane results in a very stable calibration, with minimal interferences.1.3 This test method was used successfully with reagent water spiked with sodium bicarbonate and various organic materials. It is the user's responsibility to ensure the validity of this test method for waters of untested matrices.1.4 This test method is applicable only to carbonaceous matter in the sample that can be introduced into the reaction zone. The injector opening size generally limits the maximum size of particles that can be introduced.1.5 In addition to laboratory analyses, this test method may be applied to on line monitoring.1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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定价： 646元 加购物车

定价： 646元 加购物车

定价： 590元 加购物车