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1.1 Committee D-30, having conducted several interlaboratory tests of high modulus fibers, believes that many types of equipment and techniques will yield consistent data characterizing the tensile strength and modulus of high modulus fibers. The most important consideration is the complete description of the test methods. 1.2 This guide consists of the following three parts: 1.2.1 Part A- Description of Equipment and Techniques- This section describes the equipment and the techniques used for each series of tests. The section is complete and universal, and should be reviewed by the engineer or scientist responsible for the overall test program. 1.2.2 Part B- Description of Test Specimens- This section describes each type of fiber tested in a particular series, and can be prepared by the test technician. 1.2.3 Part C- Report of Tension Test Results- This section summarizes the results of each test series. The format simplifies the reporting of essential data. Additional information may be required to report the results of tests on specific fiber types. 1.3 This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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Each year, many thousands of water samples are collected and the chemical components are determined from natural groundwater sources. An understanding of the relationships between the similarities and differences of these water analyses are facilitated by displaying each separate analysis as a pictorial diagram. This type of diagram allows for a direct comparison between two or more analyses and their displayed ions. This guide presents a compilation of diagrams that allows for transformation of numerical data into visual, usable forms. It is not a guide to selection or use. That choice is program or project specific. The single sample water-analysis diagrams described in this guide display the following; (1) the ppm or mg/L concentrations of the cations and anions on bars, circles, or baseline diagrams; (2) the epm or meq/L percentages of the cation and anion weights on bars, double bars, circles, radiating vectors, or kitelike shapes and; (3) a combination of (1) and (2) on circles (1, 3, 25, 27, 28, 29). The classification of the composition of natural groundwater is an early use of the single sample water-analysis diagram. Note 3—Palmer, in 1911, developed a tabular system for the classification of natural water. Rogers, in a 1917 study of oil-field waters, presented the Palmer classification on a graphical display that had three vertical bars (6, 7, 29). The origin of the water may be postulated by the amount and the relationship of the cations and anions in a water sample that is plotted on the diagram. Patterns visually indicate water types and origins. Comparison of the visual similarity or dissimilarity of diagrams for different water analyses that are from separate locations allows the analyst to evaluate if the samples may be from the same water source or not. Numerous interpretive methods are possible from the examination of a series of the single sample water-analysis diagrams. Note 4—For example, by arranging the diagrams at the point of origin as represented on a geologic cross section or on an areal map, the hydrochemical changes can be visualized as the water travels through the hydrologic regime, the amount of mixing that has taken place with water from a different origin, and the effects of ambient conditions, such as air, temperature, rock, and man-induced contaminants, on the water. Note 5—It should be noted that for many hydrochemical research problems involving the interpretation of the origin, chemical reactions, and mixing of natural water, the single sample water-analysis diagram is only one segment of several analytical methods needed to understand condition.1.1 This guide covers the category of water-analysis diagrams that use pictorial or pattern methods (for example, bar, radiating vectors, pattern, and circular) as a basis for displaying each of the individual chemical components that were determined from the analysis of a single sample of natural groundwater (see Terminology). 1.2 This guide on single-analysis diagrams is the second of several standards to inform the professionals in the field of hydrology with the traditional graphical methods available to display groundwater chemistry. Note 1—The initial guide described the category of water-analysis diagrams that use two-dimensional trilinear graphs to display, on a single diagram, the common chemical components from two or more complete analyses of natural groundwater. 1.2.1 A third guide will be for diagrams based on data analytical calculations that include those categories of water analysis graphs where multiple analyses are analyzed statistically and the results plotted on a diagram (for example, the box, and so forth). 1.3 Numerous methods have been developed to display, on single-analyses diagrams, the ions dissolved in water. These methods were developed by investigators to assist in the interpretation of the origin of the ions in the water and to simplify the comparison of analyses, one with another. 1.4 This guide presents a compilation of diagrams from a number of authors that allows for transformation of numerical data into visual, usable forms. It is not a guide to selection or use. That choice is program or project specific. Note 2—Use of tradenames in this guide is for identification purposes only and does not constitute endorsement by ASTM. 1.5 This guide offers an organized collection of information or a series of options and does not recommend a specific course of action. This document cannot replace education or experience and should be used in conjunction with professional judgment. Not all aspects of this guide may be applicable in all circumstances. This ASTM standard is not intended to represent or replace the standard of care by which the adequacy of a given professional service must be judged, nor should this document be applied without consideration of a project's many unique aspects. The word “Standard” in the title of this document means only that the document has been approved through the ASTM consensus process.

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5.1 Many competent measurement laboratories comply with accepted quality system requirements such as ISO 9001, QS 9000, or ISO 17025. When using standard test methods, the measurement results should agree with those from other similar laboratories within the combined uncertainty limits of the laboratories’ measurement systems. It is for this reason that quality system requirements demand that a statement of the uncertainty of the test results accompany every test result.5.2 Preparation of uncertainty estimates is a requirement for laboratory certification under ISO 17025. This practice describes the procedures by which such uncertainty estimates may be calculated.1.1 This practice describes a protocol to be utilized by measurement laboratories for estimating and reporting the uncertainty of a measurement result when the result is derived from a measurand that has been obtained by spectrophotometry.1.2 This practice is specifically limited to the reporting of uncertainty of color measurement results that are reported as color-differences in ΔE format, even though the measurement itself may be reported in other units such as percent reflectance or transmittance.1.3 The procedures defined here are not intended to be applicable to national standardizing laboratories or transfer laboratories.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Many thousands of water samples are collected each year and the chemical components are determined from natural groundwater sources. A single analysis can be interpreted easily regarding composition and geochemical type; however, it is difficult to comprehend all of the factors of similarities, interrelationships, and differences when large numbers of analyses are being compared. One of the methods of interpreting the implication of these chemical components in the water is by displaying a number of related water analyses graphically on a visually summarizing water analysis diagram. The water analysis diagrams described in this guide display the percentages of the individual cation and anion weights of the total cation and anion weights on graphs shaped as triangles, squares, diamonds, and rectangles. Note 3—The concentration of dissolved solids determined for each analysis is not evident by the plotted location. Scaled symbols, usually circles, can represent the amount of dissolved solids for each analysis plotted on the diagrams. Classification of the composition of natural groundwater is a major use of water analysis diagrams. Note 4—Palmer (20) developed a tabular system for the classification of natural water. Hill (1) classified water by composition using two trilinear and one diamond-shaped diagrams of his own design combined. Back (21) improved the classification techniques for determining the hydrochemical facies of the groundwater by a modification of the Piper diagram. The origin of the water or degree of mixing may be postulated by examination of the placement and relationship of the cations and anions from different water samples that are plotted on the diagrams. Numerous interpretive methods are possible from the examination of water analysis diagrams. For example, it is reasonable to hypothesize the path that the groundwater has traveled while in the hydrologic regime, the amount of mixing that has occurred with water from a different origin, and the effects of ambient conditions, such as air, temperature, rock, and man-induced contaminants, on the water. Note 5—It should be noted that for many hydrochemical research problems involving the interpretation of the origin, chemical reactions, and mixing of natural water, the water analysis diagram is only one segment of several analytical methods necessary to understand the condition.1.1 This guide covers the category of water analysis diagrams that use two-dimensional trilinear graphs as a technique for displaying the common chemical components from two or more complete analyses of natural groundwater (see Section 3) on a single diagram. This category includes not only trilinear-shaped diagrams but also the diamond- or parallelogram-, rectangular-, or square-shaped graphs that have trilinear subdivisions. 1.2 This guide is the first of several documents to inform professionals in the field of hydrology with the traditional graphical methods available to display groundwater chemistry. Note 1—Subsequent guides are planned that will describe the other categories of diagrams that have been developed to display groundwater chemical analyses. (1) A guide for diagrams based on data analytical calculations will include those categories of water analysis graphs in which one analysis is plotted on each diagram (for example, the pattern, bar, radial, and circle diagrams). (2) A guide for statistical diagrams will include those categories of water analysis graphs in which multiple analyses are analyzed statistically and the results plotted on the diagram (for example, the box, etc.). 1.3 Numerous methods have been developed to display the ions dissolved in water on trilinear diagrams. These diagrams are valuable as a means of interpreting the physical and chemical mechanisms controlling the composition of water. 1.4 The most commonly used trilinear methods were developed by Hill (1-3), Langelier and Ludwig (4), Piper (5, 6), and Durov (7-13). These techniques are proven systems for interpreting the origin of the ions in natural groundwater and for facilitating the comparison of results from a large number of analyses. Note 2—The use of trade names in this guide is for identification purposes only and does not constitute endorsement by ASTM. 1.5 This guide offers an organized collection of information or a series of options and does not recommend a specific course of action. This document cannot replace education or experience and should be used in conjunction with professional judgment. Not all aspects of this guide may be applicable in all circumstances. This ASTM standard is not intended to represent or replace the standard of care by which the adequacy of a given professional service must be judged, nor should this document be applied without consideration of a project's many unique aspects. The word “Standard” in the title of this document means only that the document has been approved through the ASTM consensus process.

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5.1 This practice gives techniques to use in the preparation of lubricants or lubricant components for acute or chronic aquatic toxicity tests. Most lubricants and lubricant components are difficult to evaluate in toxicity tests because they are mixtures of chemical compounds with varying and usually poor solubility in water. Lubricants or lubricant component mixtures should not be added directly to aquatic systems for toxicity testing because the details of the addition procedure will have a large effect on the results of the toxicity test. Use of the techniques described in this practice will produce well-characterized test systems that will lead to tests with meaningful and reproducible results.5.2 The toxicity of mixtures of poorly soluble components cannot be expressed in the usual terms of lethal concentration (or the similar terms of effect concentration or inhibition concentration) because the mixtures may not be completely soluble at treat levels that lead to toxic effects. The test material preparation techniques given in this practice lead to test results expressed in terms of loading rate, which is a practical and meaningful concept for expressing the toxicity of this type of material.5.3 One of the recommended methods of material preparation for lubricants or their components is the mechanical dispersion technique. This particular technique generates turbulence, and thus, it should not be used for poorly swimming organisms.1.1 This practice covers procedures to be used in the preparation of lubricants or their components for toxicity testing in aquatic systems and in the interpretation of the results of such tests.1.2 This practice is suitable for use on fully-formulated lubricants or their components that are not completely soluble at the intended test treat rates. It is also suitable for use with additives, if the additive is tested after being blended into a carrier fluid at the approximate concentration as in the intended fully formulated lubricant. The carrier fluid shall meet the above solubility criterion, be known to be minimally toxic in the toxicity test in which the material will be tested, and be known to have a chemical composition similar to the rest of the intended fully formulated lubricant.1.3 Samples prepared in accordance with this practice may be used in acute or chronic aquatic toxicity tests conducted in fresh water or salt water with fish, large invertebrates, or algae. This practice does not address preparation of samples for plant toxicity testing other than algae.1.4 Standard acute and chronic aquatic toxicity procedures are more appropriate for lubricants with compositions that are completely soluble at the intended test treat rates (1, 2, 3, 4, 5).21.5 This practice is intended for use with lubricants or lubricant components of any volatility.1.6 This practice does not address any questions regarding the effects of any lubricant or lubricant component on human health.1.7 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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