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4.1 These test methods can be used to identify and estimate the amount of some of the constituents of lubricating greases. These test methods are applicable to many, but not all, greases.4.2 Composition should not be considered as having any direct bearing on service performance unless such correlation is established.NOTE 2: Details on other test methods for grease analysis can be found in other reference material.4,5,61.1 These test methods for analysis cover greases of the conventional type, which consist essentially of petroleum oil and soap. The constituents that can be determined are soap, unsaponifiable matter (petroleum oil, and so forth), water, free alkalinity, free fatty acid, fat, glycerin, and insolubles.NOTE 1: Any of the test methods described herein are best used by an experienced grease analyst who may also be able to make appropriate adaptations of the techniques as occasion requires.1.2 A supplementary test method is provided in Appendix X1. This test method is intended primarily for application to greases containing thickeners that are essentially insoluble in n-hexane, and to greases that cannot be analyzed by conventional methods because of the presence of such constituents as nonpetroleum fluids or nonsoap-type thickeners, or both. In some cases, these constituents can react with strong acid or alkaline solutions.1.3 These test methods appear in the following order:  SectionsAsh Determination  7 – 11Insolubles, Soap, Fat, Petroleum Oil, and Unsaponifiable Matter 12 – 20Free Alkali and Free Acid 21 – 23Water 24Glycerin (Quantitative) 25 – 291.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Oxidation induction time, as determined under the conditions of this test method, can be used as an indication of oxidation stability.3 This test method can be used for research and development, quality control and specification purposes. However, no correlation has been determined between the results of this test method and service performance.1.1 This test method covers the determination of oxidation induction time of lubricating greases subjected to oxygen at 3.5 MPa (500 psig) and temperatures between 155 °C and 210 °C.1.2 Warning—The original data published in Research Report RR:D02-1314, was not analyzed in accordance the current D2PP. It also used instruments which are no longer manufactured and in a check of currently used instruments, none of the original instruments were still in use. The new precision of this test method is still to be established.1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The loss of volatile materials from greases and oils can adversely affect the original performance characteristics of a lubricant and, therefore, could be a significant factor in evaluating a lubricant for a specific use. Such volatiles can also be considered contaminants in the environment in which the lubricant is to be used. Correlation between results from this test method and service performance has not been established.5.2 The test method can be used at any specified temperature between 93 °C and 316 °C (200 °F and 600 °F) that may be agreed upon by the user of the method. (Warning—This test method should not be used at temperatures which exceed the flash point of the base oil of the grease.)NOTE 1: The specified flow of air, 2.58 g/min ± 0.02 g/min, (2 L/min at standard temperature and pressure), assumes dry air. It is not known that the original work involved dry air but it has since been shown that this can be a factor in reproducibility and should be addressed. Air with a dew point of less than 10 °C at standard temperature and pressure will be satisfactory.1.1 This test method covers the determination of evaporation loss of lubricating greases at temperatures between 93 °C and 316 °C (200 °F and 600 °F). This test method is intended to augment Test Method D972, which is limited to 149 °C (300 °F).1.2 The values stated in SI units are to be regarded as the standard. The values in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific safety information, see 5.2.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method, used for specification purposes, differentiates between lubricating greases having low, medium, and high level of extreme-pressure properties. The results do not necessarily correlate with results from service.45.2 It is noted that lubricating greases that have as their fluid component a silicone, halogenated silicone, or a mixture comprising silicone fluid and petroleum oil, are not applicable to this method of test.1.1 This test method covers the determination of the load-carrying properties of lubricating greases. Three determinations are made:1.1.1 Load-Wear Index (formerly called Mean-Hertz Load),1.1.2 Weld Point, by means of the Four-Ball Extreme-Pressure (EP) Tester, and1.1.3 Last nonseizure load (LNSL).1.2 The values stated in SI units are to be regarded as the standard. The values in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价： 590元 / 折扣价： 502 元 加购物车

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5.1 Leakage of glycol-base antifreeze into the crankcase is serious because the coolant tends to interfere with the lubricant and its ability to lubricate; it also promotes sludging. Ethylene glycol present in the coolant can increase varnish deposit formation in the crankcase as a result of glycol oxidation and the interaction between glycol and lubricant. Furthermore, because glycol is a higher boiling material than water, it will tend to stay longer in the crankcase oil than water. Lubricant displacement, sludging, and deposit formation all lead to engine malfunction and possible seizure.5.2 These tests are designed to detect glycol-base coolant contamination even at low levels because early detection enables corrective measures to be taken to prevent leaking coolant from accumulating and seriously damaging the engine.5.3 These test methods are also significant because the reagents can be packaged as a field kit, and the procedure can be followed at the site where there is a concern.1.1 These test methods cover the qualitative determination of glycol-base antifreeze in used lubricating oils (mineral base) by two procedures, one using reagents in tablet form and the other using laboratory shelf reagents. Principally the test methods detect ethylene glycol but will also detect other 1,2-glycols that may be present.1.1.1 When a positive result is obtained and a sample of the unused oil is available, the unused oil is also tested and used as a reference.NOTE 1: Since the inception of this test method (1971), there have been many changes in base stock technology and additive technology. Therefore, when available, the new, unused oil, or a sample of the same used oil, known to not contain antifreeze, is tested as a reference.1.2 The tablet procedure (Procedure A) is sensitive to about 100 mg/kg and the shelf reagent procedure (Procedure B) to about 300 mg/kg of ethylene glycol.1.3 Glycol-based coolant leaks into crankcases may not be detected or may result in a low bias using these test methods if the glycol has degraded or been thermally or otherwise oxidized. The conditions in crankcases may be such that contaminant glycols are oxidized or degraded to a degree to which the color indicator reaction does not occur or is biased enough so as to not trigger the color change. Other test methods for the detection of coolants or coolant additives in lubricating oils should be used if the results from these test methods alone are inconclusive or questionable.1.4 Carbohydrates such as sugars and sugar-containing substances are sometimes used for sabotage purposes. If the presence of these substances is suspected, Procedure A contains a modification to remove these interferences.1.5 Both procedures are adaptable to field kit use, and brief descriptions for converting to field kit form are given in Annex A1.1.5.1 Commercial field testing kits are available.2,31.6 The results obtained by this method are qualitative expressions. However, for the preparation of reagents and in the procedures, acceptable SI units are to be regarded as the standard.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The tendency of oils to foam at high temperature can be a serious problem in systems such as high-speed gearing, high volume pumping, and splash lubrication. Foaming can cause inadequate lubrication, cavitation, and loss of lubricant due to overflow, and these events can lead to mechanical failure.5.2 Correlation between the amount of foam created or the time for foam to collapse, or both, and actual lubrication failure has not been established. Such relations should be empirically determined for foam sensitive applications.1.1 This test method covers the procedure for determining the foaming characteristics of lubricating oils (specifically transmission fluid and motor oil) at 150 °C.1.2 Foaming characteristics of lubricating oils at temperatures up to 93.5 °C are determined by Test Method D892 or IP 146.1.3 The values stated in SI units are to be regarded as standard.1.3.1 Exception—The values given in parentheses are provided for information only.1.4 WARNING—Mercury has been designated by many regulatory agencies as a hazardous substance that can cause serious medical issues. Mercury, or its vapor, has been demonstrated to be hazardous to health and corrosive to materials. Use caution when handling mercury and mercury-containing products. See the applicable product Safety Data Sheet (SDS) for additional information. The potential exists that selling mercury or mercury-containing products, or both, is prohibited by local or national law. Users must determine legality of sales in their location.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Fully refined petroleum oils normally contain no naphtha-insoluble material. Semirefined or black oils frequently contain some naphtha-insoluble material (sometimes referred to as asphaltenes). This test measures the amount of naphtha-insoluble material in the oil. This quantity is reported as the precipitation number.1.1 This test method covers the determination of the precipitation number of steam cylinder stocks and black oils, and can be used for other lubricating oils.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Lubricating greases can contain the lithium soap of hydroxy stearic acid or the sodium soap of various fatty acids as thickeners. The determination of total lithium or total sodium is a measure of the amount of thickener in the grease.1.1 This test method covers determination of the lithium and sodium content of lubricating greases by means of a flame photometer.1.2 A multi-element analysis method for greases, which includes the measurement of lithium and sodium concentrations using inductively couple plasma-atomic emission spectroscopy (ICP-AES), is available in Test Method D 7303.1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.The preferred units are mass %.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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定价： 590元 / 折扣价： 502 元 加购物车

定价： 590元 / 折扣价： 502 元 加购物车

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5.1 The linear flame propagation rate of a sample is a property that is relevant to the overall assessment of the flammability or relative ignitability of fire resistance lubricants and hydraulic fluids. It is intended to be used as a bench-scale test for distinguishing between the relative resistance to ignition of such materials. It is not intended to be used for the evaluation of the relative flammability of flammable, extremely flammable, or volatile fuels, solvents, or chemicals.1.1 This test method covers the determination of the linear flame propagation rates of lubricating oils and hydraulic fluids supported on the surfaces of and impregnated into ceramic fiber media. Data thus generated are to be used for the comparison of relative flammability.1.2 This test method should be used to measure and describe the properties of materials, products, or assemblies in response to heat and flame under controlled laboratory conditions and should not be used to describe or appraise the fire hazard or fire risk of materials, products, or assemblies under actual fire conditions. However, results of this test method may be used as elements of fire risk which takes into account all of the factors that are pertinent to an assessment of the fire hazard of a particular end use.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test method measures the net change in pressure resulting from consumption of oxygen by oxidation and gain in pressure due to formation of volatile oxidation by-products. This test method may be used for quality control to indicate batch-to-batch uniformity. It predicts neither the stability of greases under dynamic service conditions, nor the stability of greases stored in containers for long periods, nor the stability of films of greases on bearings and motor-parts. It should not be used to estimate the relative oxidation resistance of different grease types.1.1 This test method determines resistance of lubricating greases to oxidation when stored statically in an oxygen atmosphere in a sealed system at an elevated temperature under conditions of test.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.2.1 Exception—Pressure measurement appears in kPa with psi provided for information only.1.2.2 Exception—In Fig. A1.1, A1.1, and Appendix X1, all dimensions are in millimeters, with inches provided in parentheses for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements see Sections 6 and 7.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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