5.1 With the common occurrence in water of organic compounds, some of which are toxic, it is often necessary to identify the specific compounds present and to determine the concentration.1.1 This guide covers the identification and quantitation of organic compounds by gas chromatography/mass spectrometry (GC-MS) (electron impact) that are present or extracted from water and are capable of passing through a gas chromatograph without alteration. This guide can be used to provide tentative identifications of volatile and semi-volatile organics, but is restricted to (a) compounds for which reference spectra can be obtained and (b) compounds that can be separated by gas chromatography (GC). These restrictions are imposed on the guide, but are not a limitation of the technique. The guide is written for analysis using automated data acquisition and handling.1.2 Guidelines have been included for quantitation using ASTM Test Methods D3871, D3973, and other GC-MS volatile/semivolatile procedures used for environmental analysis2. The actual detection limits for each component must be determined in each laboratory. Actual detection amounts will vary with the complexity of the matrix, the kind and condition of the GC-MS system, the sample preparation technique chosen, and the application of cleanup techniques to the sample extract, if any. Lower levels of detection can be achieved using modern sensitive instruments or with selected ion monitoring (SIM). To determine the interlaboratory detection estimate (IDE) and the interlaboratory quantitation estimate (IQE), follow Practices D6091 and D6512.1.3 The guide is applicable to the identification of many organic constituents of natural and treated waters. It includes all modes of sample introduction, including injection of organic extracts, direct aqueous injection, and purge and trap techniques.1.4 The guide is applicable to capillary column gas chromatography.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test method is applicable to the determination of trace amounts of aldehydes and ketones in aqueous solutions and a wide variety of organic solvents.1.1 This test method covers the determination of total carbonyl in the range from 0.5 μg to 50 μg calculated as CO.1.2 This test method is intended to be general and does not include steps for sample preparation.1.3 Acetals that hydrolyze under the conditions of the test are also determined.1.4 Carbonyl derivatives such as acetals and imines that are easily hydrolyzed may be determined by an alternative procedure.1.5 The developed color is not stable and must be measured within a specified period.NOTE 1: Other test methods for the determination of traces of carbonyl compounds are given in Test Methods D1089, D1612, D2119, and D2191.1.6 Review the current appropriate Safety Data Sheets (SDS) for detailed information concerning toxicity, first aid procedures, and safety precautions.1.7 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.8 In determining the conformance of the test results using this method to applicable specifications, results shall be rounded off in accordance with the rounding-off method of Practice E29.1.9 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazards statements are given in Section 7 and Section 8.1.10 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This practice provides a general procedure for the solid phase micro extraction of volatile and semi-volatile organic compounds from an aqueous matrix or its headspace. Solid sorbent extraction is used as the initial step in the extraction of organic constituents for the purpose of quantifying or screening for extractable organic compounds.5.2 Typical detection limits that can be achieved using SPME techniques with gas chromatography with flame ionization detector (FID), electron capture detector (ECD), or with a mass spectrometer (MS) range from mg/L to μg/L. The detection limit, linear concentration range, and sensitivity of the test method for a specific organic compound will depend upon the aqueous matrix, the fiber phase, the sample temperature, sample volume, sample mixing, and the determinative technique employed.5.3 SPME has the advantages of speed, no desorption solvent, simple extraction device, and the use of small amounts of sample.5.3.1 Extraction devices vary from a manual SPME fiber holder to automated commercial device specifically designed for SPME.5.3.2 Listed below are examples of organic compounds that can be determined by this practice. This list includes both high and low boiling compounds.Volatile Organic Compounds (1-3)3Pesticides, General (4, 5)Organochlorine Pesticides (6)Organophosphorous Pesticides (7, 8)Polyaromatic Hydrocarbons (9, 10)Polychlorinated Biphenyls (10)Phenols (11)Nitrophenols (12)Amines (13)5.3.3 SPME may be used to screen water samples prior to purge and trap extraction to determine if dilution is necessary, thereby eliminating the possibility of trap overload.1.1 This practice covers procedures for the extraction of volatile and semi-volatile organic compounds from water and its headspace using solid phase micro extraction (SPME).1.2 The compounds of interest must have a greater affinity for the SPME-absorbent polymer or adsorbent or combinations of these than the water or headspace phase in which they reside.1.3 Not all of the analytes that can be determined by SPME are addressed in this practice. The applicability of the absorbent polymer, adsorbent, or combination thereof, to extract the compound(s) of interest must be demonstrated before use.1.4 This practice provides sample extracts suitable for quantitative or qualitative analysis by gas chromatography (GC) or gas chromatography-mass spectrometry (GC-MS).1.5 Where used, it is the responsibility of the user to validate the application of SPME to the analysis of interest.1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 12.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test method covers the evaluation of the apparent density physical characteristic of powders. The degree of correlation between the results of this test and the quality of powders in use will vary with each particular application and has not been fully determined.4.2 The apparent density measured via this test method is often referred to as the “Scott Density.”1.1 This test method covers determination of the apparent density of metal powders and related compounds using the Scott Volumeter, also known as the Paint Pigment Volumeter.1.2 Units—With the exception of the values for density and the mass used to determine density, for which the use of the gram per cubic centimetre (g/cm3) and gram (g) units is the longstanding industry practice, the values stated in SI units are to be regarded as the standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 These test methods provide procedures for determining the envelope-specific surface area of powders, from which is calculated an “average” particle diameter, assuming the particles are monosize, smooth surface, nonporous, spherical particles. For this reason, values obtained by these test methods will be reported as an average particle size or Fisher Number. The degree of correlation between the results of these test methods and the quality of powders in use will vary with each particular application and has not been fully determined.4.2 These test methods are generally applicable to all metal powders and related compounds, including carbides, nitrides, and oxides, for particles having diameters between 0.2 and 75 μm (MIC SAS) or between 0.5 and 50 μm (FSSS). They should not be used for powders composed of particles whose shape is too far from equiaxed - that is, flakes or fibers. In these cases, it is permissible to use the test methods described only by agreement between the parties concerned. These test methods shall not be used for mixtures of different powders, nor for powders containing binders or lubricants. When the powder contains agglomerates, the measured surface area may be affected by the degree of agglomeration. Methods of de-agglomeration such as that specified in Practice B859 may be used if agreed upon between the parties concerned.4.3 When an “average” particle size of powders is determined either the MIC SAS or the FSSS, it should be clearly kept in mind that this average size is derived from the determination of the specific surface area of the powder using a relationship that is true only for powders of uniform size and spherical shape. Thus, the results of these methods are only estimates of average particle size.1.1 These test methods use air permeability to determine an envelope-specific surface area and its associated average equivalent spherical diameter (from 0.2 to 75μm) of metal powders and related compounds. The powders may be analyzed in their “as-supplied” (shipped, received, or processed) condition or after they have been de-agglomerated or milled by a laboratory procedure (“lab milled”) such as that specified in Practice B859. The values obtained are not intended to be absolute but are generally useful on a relative basis for control purposes.1.2 Units—With the exception of the values for density and the mass used to determine density, for which the use of the gram per cubic centimetre (g/cm3) and gram (g) units is the longstanding industry practice; and the units for pressure, cm H2O - also long-standing practice; the values in SI units are to be regarded as standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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PVC compounds are used in a wide variety of products and hence they are formulated to provide a wide range of physical properties. The physical properties required in a compound depend upon the product in which it is used. These properties are largely determined by the type, quantity, and quality of the compounding ingredients. The analytical test method described below makes use of infrared spectrophotometry for the qualitative or quantitative determination, or both, of many of these ingredients in PVC compounds. This test method may be used for a variety of applications including process control, raw material acceptance, product evaluation, and determination of changes in composition resulting from environmental testing.This test method is directly applicable only to those components listed in the appendix and to those components which are known to be similar in chemical composition and in solubility characteristics to the chemicals listed in the appendix.1.1 This test method provides for the identification of certain resins, plasticizers, stabilizers, and fillers in poly(vinyl chloride) (PVC) compounds by an infrared spectrophotometric technique. In many cases, individual components may be measured quantitatively. Complementary procedures, such as chromatographic and other separations, will be necessary to separate specific components and extend the applications of this test method. Other instrumental test methods, such as optical emission or X-ray spectroscopic methods, may yield complementary information which may allow more complete or, in some cases, easier measurement of the components. The resin components covered in this test method are listed in the appendix.1.2 PVC formulations are too varied to be covered adequately by a single test method. Using the following test method, many compounds may be separated into resins, plasticizers, stabilizers, and fillers. A number of components can be quantitatively measured. Many more can be identified and their concentrations estimated. By the use of prepared standards, one may determine the usefulness and accuracy of the test method for specific PVC formulations. This test method is applicable for the resin components listed in the appendix and for other components having similar chemical compositions and solubility characteristics. This test method can lead to error in cases where the nature of the components is not known.1.3 The values stated in SI units are to be regarded as the standard. The values in brackets are given for information only.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.Note 1—There is no known ISO equivalent to this standard.

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AbstractThe purpose of this classification system is to provide a method of adequately identifying poly(methyl methacrylate) (PMMA) molding and extrusion compounds. These compounds are polymers based on methyl methacrylate, and at least 70 % of the polymer shall be polymerized from methyl methacrylate. Poly(methyl methacrylate) molding and extrusion compounds are classified into groups in accordance with their composition. These groups are subdivided into classes and grades: class 1, 2, 3, and 4; grade 1 - materials used where special ultraviolet transmission, filtering, or stabilization characteristics are not required, grade 2 - materials used for those specialized applications in which the greatest amount of transmission of UV light is required, and grade 3 - materials (transparent UV stabilized or transparent UV absorbing) used when either special resistance to slight color change over long exposure times or high-intensity UV radiation is required, or when the material is required to filter out ultraviolet light. The plastics composition shall be uniform and shall conform to the requirements specified.1.1 The purpose of this classification system is to provide a method of adequately identifying PMMA materials using a system consistent with that of Classification System D4000. It further provides a means for specifying these materials by the use of a simple line callout designation.1.2 This classification system covers poly(methyl methacrylate) molding and extrusion compounds. These compounds are polymers based on methyl methacrylate, and at least 70 % of the polymer shall be polymerized from methyl methacrylate.1.3 The properties in this classification system are those required to identify the compositions covered. Other requirements necessary to identify particular characteristics important to specific applications shall be described by using the suffixes as given in Section 5.1.4 Acrylic molding and extrusion compounds are used frequently in applications where extreme clarity and the ability to retain that clarity and color under severe weathering and other environmental exposures are of primary significance. While the test specimen properties of this document extend to the evaluation of nonvirgin materials, the user must take precautions to ensure that parts made from these materials meet the desired end-use requirements. Accordingly, this specification allows for the use of those acrylic plastic materials that can be recycled, reconstituted, and reground provided the following:1.4.1 The requirements as stated in this specification are met, and1.4.2 The requirements of the particular end-use application are met.1.5 This classification system and subsequent line callout (specification) are not intended for the selection of materials, but only as a means to call out plastic materials to be used for the manufacture of parts. The selection of these materials is to be made by personnel with expertise in the plastics field in which the environment, inherent properties of the materials, performance of the parts, part design, manufacturing process, and economics are considered.NOTE 1: This classification system is similar to ISO 8257-1:1987 in title only. The technical content is significantly different.1.6 The values stated in SI units are to be regarded as standard.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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5.1 The conditions at which compounds are molded are known to influence the properties of the specimens. The degree of cure, elimination of knit-lines between particles, density of the part, and degradation of the polymer are among those factors which will be affected by the molding conditions. Thus it is important to conform to a standard set of conditions in order to have a valid comparison of properties between different compounds and different batches of the same compound.5.2 Molded specimens showing evidence of low-density areas due to trapped gases shall be discarded. A breathe step can be incorporated to eliminate this situation. If used, it is critical that the breathe step be as brief as possible to avoid precuring of the compound before full pressure is applied leading to poorly “knitted” areas and lower strength in the molded specimen.1.1 This practice covers the general principles to be followed when compression molding test specimens of thermosetting molding compounds, such as phenolics, aminoplastics, melamine phenolics, epoxies, and unsaturated polyesters.1.2 Molding conditions are given for amino, phenolic, and allyl molding compounds. The exact molding conditions will vary from material to material, and, if not incorporated in the material specification, shall be agreed upon between the purchaser and the supplier or determined by previous experience with the particular type of material being used1.3 The values stated in SI units are to be regarded as standard. The values in parentheses are given for information only.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.NOTE 1: This standard and ISO 295 address the same subject matter, but differ in technical content.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification covers the testing and requirements for two types of compression-molding, thermosetting urea-formaldehyde molding compounds. Type 1 are general purpose molding compounds with alpha-cellulose fillers, while, Type 2 are general purpose molding compounds with cellulose fillers other than alpha-cellulose. The molding compounds shall be of uniform composition, and the apparent density, bulk factor, plasticity, particle size, and color shall be compounded as to conform to the requirements prescribed herein. Also, sampled test specimens shall be examined and conform correspondingly to the following physical requirements: specific gravity; flexural strength; impact resistance; water absorption; dielectric strength; and arc resistance.1.1 This specification covers compression molding thermosetting, urea-formaldehyde molding compounds as further defined in 3.1.1.2 The values stated in SI units are to be regarded as the standard.NOTE 1: The properties included in this specification are those required to identify the types of molding compounds covered. There may be other requirements necessary to identify particular characteristics. Transfer or injection molding will usually result in different physical and electrical characteristics than compression molding.1.3 The following safety hazards caveat pertains only to the test method portion, Section 7, of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.NOTE 2: ISO 2112-1977(E) is similar but not equivalent to this specification. Product classification and characterization are not the same.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method provides a guide as to the amount of volatile matter that will be emitted from a channel glazing compound when tested by this test method.1.1 This test method describes the determination of the volatility of oil- and resin-based, knife-grade, channel glazing compounds.1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.3 The subcommittee with jurisdiction is not aware of any similar ISO standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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