5.1 This test method is used primarily to determine the heat evolved in, or contributed to, a fire involving materials or products that emit low levels of heat release. The recommended use for this test method is for materials with a total heat release rate measured of less than 10 MJ over the first 20 min test period, and which do not give peak heat release rates of more than 200 kW/m2 for periods extending more than 10 s. Also included is a determination of the effective heat of combustion, mass loss rate, the time to sustained flaming, and (optionally) smoke production. These properties are determined on small size test specimens that are representative of those in the intended end use.5.2 This test method is applicable to various categories of products and is not limited to representing a single fire scenario.5.3 This test method is not applicable to end-use products that do not have planar, or nearly planar, external surfaces.1.1 This fire-test-response standard provides a procedure for measuring the response of materials that emit low levels of heat release when exposed to controlled levels of radiant heating with or without an external igniter.1.2 This test method differs from Test Method E1354 in that it prescribes a different specific test specimen size, specimen holder, test specimen orientation, a direct connection between the plenum and the top plate of the cone heater assembly to ensure complete collection of all the combustion gases (Fig. 1), and a lower volumetric flow rate for analyses via oxygen consumption calorimetry. It is intended for use on materials and products that contain only small amounts of combustible ingredients or components, such as test specimens that yield a peak heat release of <200 kW/m2 and total heat release of <15 MJ/m2.NOTE 1: PMMA is typically used to check the general operation of a Cone Calorimeter. PMMA should not be used with this standard as the heat release rate is too high.1.3 The rate of heat release is determined by measurement of the oxygen consumption as determined by the oxygen concentration and the flow rate in the exhaust product stream. The effective heat of combustion is determined from a concomitant measurement of test specimen mass loss rate, in combination with the heat release rate. Smoke development (an optional measurement) is measured by obscuration of light by the combustion product stream.1.4 Test specimens shall be exposed to initial test heat fluxes generated by a conical radiant heater. External ignition, when used, shall be by electric spark. The test specimen testing orientation is horizontal, independent of whether the end-use application involves a horizontal or a vertical orientation.1.5 Ignitability is determined as a measurement of time from initial exposure to time of sustained flaming.1.6 This test method has been developed for use for material and product evaluations, mathematical modeling, design purposes, and development and research. Examples of material test specimens include portions of an end-use product or the various components used in the end-use product.1.7 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.8 This standard is used to measure and describe the response of materials, products, or assemblies to heat and flame under controlled conditions, but does not by itself incorporate all factors required for fire hazard or fire risk assessment of the materials, products, or assemblies under actual fire conditions.1.9 Fire testing is inherently hazardous. Adequate safeguards for personnel and property shall be employed in conducting these tests.1.10 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 7.1.11 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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5.1 This test method is used to evaluate oxidation stability of lubricating base oils with additives in the presence of chemistries similar to those found in gasoline engine service. Test results on some ASTM reference oils have been found to correlate with sequence IIID engine test results in hours for a 375 % viscosity increase.5 The test does not constitute a substitute for engine testing, which measures wear, oxidation stability, volatility, and deposit control characteristics of lubricants. Properly interpreted, the test may provide input on the oxidation stability of lubricants under simulated engine chemistry.5.2 This test method is intended to be used as a bench screening test and quality control tool for lubricating base oil manufacturing, especially for re-refined lubricating base oils. This test method is useful for quality control of oxidation stability of re-refined oils from batch to batch.5.3 This test method is useful for screening formulated oils prior to engine tests. Within similar additive chemistry and base oil types, the ranking of oils in this test appears to be predictive of ranking in engine tests. When oils having completely different additive chemistry or base oil type are compared, oxidation stability results may not reflect the actual engine test result.5.4 Other oxidation stability test methods have demonstrated that soluble metal catalyst supplies are very inconsistent and they have significant effects on the test results. Thus, for test comparisons, the same source and same batch of metal naphthenates shall be used.NOTE 2: It is also recommended as a good research practice not to use different batches of the fuel component in test comparisons.1.1 This test method evaluates the oxidation stability of engine oils for gasoline automotive engines. This test, run at 160 °C, utilizes a high pressure reactor pressurized with oxygen along with a metal catalyst package, a fuel catalyst, and water in a partial simulation of the conditions to which an oil may be subjected in a gasoline combustion engine. This test method can be used for engine oils with viscosity in the range from 4 mm2/s (cSt) to 21 mm2/s (cSt) at 100 °C, including re-refined oils.1.2 This test method is not a substitute for the engine testing of an engine oil in established engine tests, such as Sequence IIID.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3.1 Exception—Pressure units are provided in psig, and dimensions are provided in inches in Annex A1, because these are the industry accepted standard and the apparatus is built according to the figures shown.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see Sections 7 and 8.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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5.1 This test method describes a rapid method to determine the maximum quantity of oxygen that may be consumed by impurities in water. As outlined in Test Methods D1252, chemical oxygen demand is typically used to monitor and control oxygen-consuming pollutants, both organic and inorganic, in domestic and industrial wastewaters. This photoelectrochemical oxygen demand test method is specific for measuring organics and inorganics in freshwater sources for drinking water treatment plants and treated drinking water matrices. This photoelectrochemical oxygen demand test method is not intended for domestic and industrial wastewaters to replace Test Methods D1252.5.2 This test method does not require the use of the hazardous reagents, such as mercuric sulfate, potassium dichromate and silver sulfate, that are associated with chemical oxygen demand. It can also provide a result more rapidly than chemical oxygen demand as samples do not require reflux.1.1 This test method covers a protocol for the determination of the photoelectrochemical oxygen demand of freshwater sources for drinking water treatment plants and treated drinking water in the range of 0.7 mg/L to 20 mg/L. Higher levels may be determined by sample dilution.1.2 Photoelectrochemical oxygen demand is determined using the current generated from the photoelectrochemical oxidation of the sample using titanium dioxide (TiO2) irradiated with ultraviolet (UV) light from a light-emitting diode (LED).1.3 This test method does not require the use of the hazardous reagents, such as mercuric sulfate, potassium dichromate and silver sulfate, that are often associated with the determination of chemical oxygen demand (that is, Test Methods D1252). It can also provide a result rapidly, as samples do not require reflux.1.4 Determination of photoelectrochemical oxygen demand in freshwater sources for drinking water treatment plants and treated drinking water matrices has important implications for assessing treatment efficacy. Photoelectrochemical oxygen demand can be used as a bulk surrogate measure of natural organic matter, a key target for drinking water treatment. In aerobic biological treatment processes, determination of photoelectrochemical oxygen demand can provide an estimation of the oxygen required by microorganisms to degrade organic matter. This test method is complementary to existing natural organic matter (NOM) monitoring techniques and will help scientists and engineers further the understanding of NOM in water with a rapid oxygen demand test.1.5 This test method was used successfully with reagent grade water spiked with pure compounds, freshwater sources for drinking water treatment plants and treated drinking water. It is the user’s responsibility to ensure the validity of this test method for waters of untested matrices.1.6 This test method is applicable to oxidizable matter, <50 µm that can be introduced into the sensor.NOTE 1: This test method can be performed (1) immediately in the field or laboratory on an unpreserved sample, and (2) in the laboratory on a properly preserved sample following the stated hold times.1.7 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 9.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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5.1 The conventional determination of oxygen content in liquid or solid samples is a relatively difficult chemical procedure. It is slow and usually of limited sensitivity. The 14-MeV neutron activation and direct counting technique provides a rapid, highly sensitive, nondestructive procedure for oxygen determination in a wide range of matrices. This test method is independent of the chemical form of the oxygen.5.2 This test method can be used for quality and process control in the metals, coal, and petroleum industries, and for research purposes in a broad spectrum of applications.1.1 This test method covers the measurement of oxygen concentration in almost any matrix by using a 14-MeV neutron activation and direct-counting technique. Essentially, the same system may be used to determine oxygen concentrations ranging from under 10 μg/g to over 500 mg/g, depending on the sample size and available 14-MeV neutron fluence rates.NOTE 1: The range of analysis may be extended by using higher neutron fluence rates, larger samples, and higher counting efficiency detectors.1.2 This test method may be used on either solid or liquid samples, provided that they can be made to conform in size, shape, and macroscopic density during irradiation and counting to a standard sample of known oxygen content. Several variants of this method have been described in the technical literature. A monograph is available which provides a comprehensive description of the principles of activation analysis using a neutron generator (1).21.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.Specific precautions are given in Section 8.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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This specification covers the design, construction, testing, and operating requirements for hand operated, quick-change cartridge trim, in-line body and angle-body, globe-style valves for use in gas (except oxygen gas) and hydraulic systems. These valves may be used for on-off, and/or throttling applications. Valves under this specification shall be Type I or Type II; Style I or Style II; and shall have the specified size, pressure rating, and end connections. Valves furnished under this specification shall be soft-seated, globe-style valves using a cartridge in which all working parts including the seat are removable as an assembly. The pressure containing envelope shall be made of corrosion-resistant steel, nickel-copper, nickel-aluminum-bronze, or bronze. Internal parts in contact with the line media shall be made of corrosion-resistant steel, nickel-copper, copper-nickel, bronze, nickel-aluminum bronze, or naval brass. Valve construction requirements for the following are detailed: (1) soft-seating insert, (2) pressure envelope, (3) threads, (4) accessibility, (5) nonmetallic element interchangeability, (6) maintainability, (7) reversibility, (8) adjustments, (9) bidirectional operation and bubbletight shut off, (10) guiding, (11) valve operating force, (12) pressurizing rate, (13) operation, and (14) envelope dimensions. Valves shall meet the performance requirements of flow capacity, seat tightness, and external leakage. Each valve shall pass the following tests: visual examination, hydrostatic shell test, seat tightness test, and external leakage test. The envelope dimensions for angle body and inline body construction are illustrated.1.1 This specification covers the design, construction, testing, and operating requirements for hand-operated, quick-change cartridge trim, in-line body and angle-body, globe-style valves for use in gas (except oxygen gas) and hydraulic systems. These valves may be used for on-off, or throttling applications, or both.1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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4.1 Most organic liquids and solids will ignite in a pressurized oxidizing gas atmosphere if heated to a sufficiently high temperature and pressure. This procedure provides a numerical value for the temperature at the onset of ignition under carefully controlled conditions. Means for extrapolation from this idealized situation to the description, appraisal, or regulation of fire and explosion hazards in specific field situations, are not established. Ranking of the ignition temperatures of several materials in the standard apparatus is generally in conformity with field experience.4.2 The temperature at which material will ignite spontaneously (AIT) will vary greatly with the geometry of the test system and the rate of heating. To achieve good interlaboratory agreement of ignition temperatures, it is necessary to use equipment of approximately the dimensions described in the test method. It is also necessary to follow the described procedure as closely as possible.4.3 The decomposition and oxidation of some fully fluorinated materials releases so little energy that there is no clear-cut indication of ignition. Nor will there be a clear indication of ignition if a sample volatilizes, distilling to another part of the reaction vessel, before reaching ignition temperature.1.1 This test method covers the determination of the temperature at which liquids and solids will spontaneously ignite. These materials must ignite without application of spark or flame in a high-pressure oxygen-enriched environment.1.2 This test method is intended for use at pressures of 2.1 MPa to 20.7 MPa [300 psi to 3000 psi]. The pressure used in the description of the method is 10.3 MPa [1500 psi], and is intended for applicability to high pressure conditions. The test method, as described, is for liquids or solids with ignition temperature in the range from 60 °C to 500 °C [140 °F to 932 °F].NOTE 1: Test Method G72/G72M normally utilizes samples of approximately 0.20 ± 0.03-g mass, a starting pressure of 10.3 MPa [1500 psi] and a temperature ramp rate of 5 °C/min. However, Autogenous Ignition Temperatures (AIT) can also be obtained under other test conditions. Testing experience has shown that AIT testing of volatile liquids can be influenced by the sample pre-conditioning and the sample mass. This will be addressed in the standard as Special Case 1 in subsection 8.2.2. Testing experience has also shown that AIT testing of solid or non-volatile liquid materials at low pressures (that is, < 2.1 MPa) can be significantly influenced by the sample mass and the temperature ramp rate. This will be addressed in the standard as Special Case 2, in subsection 8.2.3. Since the AIT of a material is dependent on the sample mass/configuration and test conditions, any departure from the standard conditions normally used for Test Method G72/G72M testing should be clearly indicated in the test report.1.3 This test method is for high-pressure pure oxygen. The test method may be used in atmospheres from 0.5 % to 100 % oxygen.1.4 An apparatus suitable for these requirements is described. This test method could be applied to higher pressures and materials of higher ignition temperature. If more severe requirements or other oxidizers than those described are desired, care must be taken in selecting an alternative safe apparatus capable of withstanding the conditions.1.5 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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This specification covers the requirements, test methods, and markings for crosslinked polyethylene (PEX) tubing with a polymeric oxygen barrier layer, made in one standard dimension ratio (SDR 9), and distribution system components intended for hydronic heating and cooling applications up to and including a maximum working temperature of 200°F (93°C). Components are comprised of tubing, fittings, valves, and manifolds that are intended for use in residential and commercial hydronic heating and cooling systems. Tubing made to this specification incorporates a single outer or middle wall oxygen barrier layer designed to inhibit the transmission or permeation of oxygen through the tubing wall. The requirements and test methods cover materials, workmanship, tubing dimensions and tolerances, burst pressure, sustained pressure, excessive temperature and pressure, thermo-cycling, bent tube, oxidative resistance, layer adhesion, UV resistance, oxygen permeation, and fitting pullout strength tests.1.1 This specification covers requirements, test methods, and marking requirements for crosslinked polyethylene (PEX) tubing with a polymeric oxygen barrier layer, made in one standard dimension ratio (SDR 9), and distribution system components intended for hydronic heating and cooling applications up to and including a maximum working temperature of 200 °F (93 °C).1.1.1 Components are comprised of tubing, fittings, valves, and manifolds. Tubing made to this specification incorporates a single outer or middle wall oxygen barrier layer intended for inhibiting the transmission or permeation of oxygen through the tubing wall. Requirements and test methods are included for materials, workmanship, tubing dimensions and tolerances, burst pressure, sustained pressure, excessive temperature and pressure, thermo-cycling, bent tube, oxidative resistance, layer adhesion, UV resistance, oxygen permeation, and fitting pull-out strength tests. The components covered by this specification are intended for use in residential and commercial hydronic heating and cooling systems. Requirements for potable water applications are outside the scope of this specification.1.2 The text of this specification references notes, footnotes, and appendixes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the specification.1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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5.1 This guide describes stabilization criteria for recording field measurements of temperature, DO, SC, and pH.5.2 This guide describes the procedures used to calibrate and check meters to be used in the field to records these measurements and the procedures to be use in the field to obtain these data.5.3 This guide describes quality assurance procedures to be followed when obtaining cross-sectional means of temperature, DO, SC, and pH of water flowing in open channels.5.4 Field measurement must accurately represent the water flowing in the open channel being measured. Methods need to be used that will result in an accurate representation of the mean of the parameter of interest. Procedures must be used that will take into consideration the variation in the parameter across the sections and with depth.5.5 Temperature and DO must be measured directly in the water in the open channel. SC and pH are often measured in situ, but also may be measured in a subsample of a composite sample collected using discharge-weighted methods.1.1 This guide describes procedures to collect cross-sectional means of temperature, dissolved oxygen (DO), specific electrical conductance (SC), and pH of water flowing in open channels.1.2 This guide provides guidelines for preparation and calibration of the equipment to collect cross-sectional means of temperature, DO, SC, and pH of water flowing in open channels.1.3 This guide describes what equipment should be used to collect cross-sectional means of temperature, DO, SC, and pH of water flowing in open channels.1.4 This guide covers the cross-sectional means of temperature, DO, SC, and pH of fresh water flowing in open channels.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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