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5.1 The bioavailability of chemical elements is poorly related to the chemical composition of soils and plant growth media containing a mineral or any type of adsorbed phase. The chemical potential (pi for element, i,) is an intensity parameter (I), and the sorbed amount in equilibrium with the soil solution is a measure of the quantity (Q). These parameters for each element (essential or toxic) should be measured in the presence of other elements at or near the desired intensity. This test method is the only method that generates these results simultaneously for several elements. The computer software allows these values to be related to the total sorbed quantities of the different elements. For many substrates, it has been found that the theory for the method holds to the degree that vegetation has been established on many non-soil substrates and soil-water-food chain problems have been evaluated by this test method. This test method has been used on many sites in Pennsylvania and other locations to monitor the effect of sewage sludge applications on land as a source of essential elements for plants with no harmful effects on the food chain. It has also been used to evaluate synthetic soils produced from fly-ash alone or as a component of coal refuse for the establishment of vegetation on mine spoils, coal refuse piles, and abandoned mine lands.Note 1—The quality of the result produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection and the like. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.1.1 This test method covers the determination of quantity (Q) and intensity (I) results for several elements in soils, spoils, fly-ash, and other soil substitutes to ascertain their suitability for the growth of vegetation and possible adverse effects of metals on the food chain.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 All measured and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.1.4 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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4.1 For many structural ceramic components in service, their use is often limited by lifetimes that are controlled by a process of SCG. This test method provides the empirical parameters for appraising the relative SCG susceptibility of ceramic materials under specified environments. Furthermore, this test method may establish the influences of processing variables and composition on SCG as well as on strength behavior of newly developed or existing materials, thus allowing tailoring and optimizing material processing for further modification. In summary, this test method may be used for material development, quality control, characterization, and limited design data generation purposes. The conventional analysis of constant stress rate testing is based on a number of critical assumptions, the most important of which are listed in the next paragraphs.4.2 The flexural stress computation for the rectangular beam test specimens or the equibiaxial disk flexure test specimens is based on simple beam theory, with the assumptions that the material is isotropic and homogeneous, the moduli of elasticity in tension and compression are identical, and the material is linearly elastic. The average grain size should be no greater than one-fiftieth of the beam thickness.4.3 The test specimen sizes and fixtures for rectangular beam test specimens should be in accordance with Test Method C1161, which provides a balance between practical configurations and resulting errors, as discussed in Refs (4, 5). Only four-point test configuration is allowed in this test method for rectangular beam specimens. Three-point test configurations are not permitted. The test specimen sizes and fixtures for disk test specimens tested in ring-on-ring flexure should be chosen in accordance with Test Method C1499. The test specimens for direct tension strength testing should be chosen in accordance with Test Method C1273.4.4 The SCG parameters (n and D) are determined by fitting the measured experimental data to a mathematical relationship between strength and applied stress rate, log σf = 1/(n+1) log σ˙ + log D. The basic underlying assumption on the derivation of this relationship is that SCG is governed by an empirical power-law crack velocity, v = A[KI/KIC]n (see Appendix X1).NOTE 3: There are various other forms of crack velocity laws which are usually more complex or less convenient mathematically, or both, but may be physically more realistic (6). It is generally accepted that actual data cannot reliably distinguish between the various formulations. Therefore, the mathematical analysis in this test method does not cover such alternative crack velocity formulations.4.5 The mathematical relationship between strength and stress rate was derived based on the assumption that the slow crack growth parameter is at least n ≥ 5 (1, 7, 8). Therefore, if a material exhibits a very high susceptibility to SCG, that is, n < 5, special care should be taken when interpreting the results.4.6 The mathematical analysis of test results in accordance with the method in 4.4 assumes that the material displays no rising R-curve behavior. It should be noted that the existence of such behavior cannot be determined from this test method.4.7 Slow crack growth behavior of ceramic materials exposed to stress-corrosive gases or liquid environments can vary as a function of mechanical, material, and electrochemical variables. Therefore, it is essential that test results accurately reflect the effects of specific variables under study. Only then can data be compared from one investigation to another on a valid basis or serve as a valid basis for characterizing materials and assessing structural behavior.4.8 The strength of advanced ceramics is probabilistic in nature. Therefore, SCG that is determined from the strengths of a ceramic material is also a probabilistic phenomenon. Hence, a proper range and number of applied stress rates in conjunction with an appropriate number of specimens at each applied stress rate are required for statistical reproducibility and design (2). Guidelines are provided in this test method.NOTE 4: For a given ceramic material/environment system, the SCG parameter n is constant regardless of specimen size although its reproducibility is dependent on the variables mentioned in 4.8. By contrast, the SCG parameter D depends significantly on strength and thus on specimen size (see Eq X1.6 in Appendix X1).4.9 The strength of a ceramic material for a given specimen and test fixture configuration is dependent on its inherent resistance to fracture, the presence of flaws, and environmental effects. Analysis of a fracture surface, fractography, though beyond the scope of this test method, is highly recommended for all purposes, especially to verify the mechanism(s) associated with failure (refer to Practice C1322).4.10 The conventional analysis of constant stress rate testing is based on a critical assumption that stress is uniform throughout the test piece. This is most easily achieved in direct tension test specimens. Only test specimens that fracture in the inner gauge section in four-point testing should be used. Three-point flexure shall not be used. Breakages between the outer and inner fixture contact points should be discounted. The same requirement applies to biaxial disk strength testing. Only fractures which occur in the inner loading circle should be used. Furthermore, it is assumed that the fracture origins are near to the tensile surface and do not grow very large relative to the thickness of rectangular beam flexure or disk strength test specimens.4.11 The conventional analysis of constant stress rate testing is also based on a critical assumption that the same type flaw controls strength in all specimens at all loading rates. If the flaw distribution is multimodal, then the conventional analysis in this standard may produce erroneous slow crack growth parameter estimates.1.1 This test method covers the determination of slow crack growth (SCG) parameters of advanced ceramics by using constant stress rate rectangular beam flexural testing, ring-on-ring biaxial disk flexural testing, or direct tensile strength, in which strength is determined as a function of applied stress rate in a given environment at ambient temperature. The strength degradation exhibited with decreasing applied stress rate in a specified environment is the basis of this test method which enables the evaluation of slow crack growth parameters of a material.NOTE 1: This test method is frequently referred to as “dynamic fatigue” testing (1-3)2 in which the term “fatigue” is used interchangeably with the term “slow crack growth.” To avoid possible confusion with the “fatigue” phenomenon of a material which occurs exclusively under cyclic loading, as defined in Terminology E1823, this test method uses the term “constant stress rate testing” rather than “dynamic fatigue” testing.NOTE 2: In glass and ceramics technology, static tests of considerable duration are called “static fatigue” tests, a type of test designated as stress rupture (See Terminology E1823).1.2 Values expressed in this test method are in accordance with the International System of Units (SI) and IEEE/ASTM SI 10.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 An accelerated test for determining the resistance of interior coated building products to mold growth is useful in estimating the relative performance for use in interior environments under conditions favorable to fungal growth.5.2 Static or environmental chambers provide controlled laboratory micro-environment conditions. These chambers are not intended to duplicate room conditions, and care must be taken when interpreting the results. Static chambers are not a substitute for dynamic chambers or field studies.1.1 This test method covers an environmental chamber and the conditions of operation to evaluate in a 4-week period the relative resistance to mold growth and microbial surface defacement on coated building products designed for interior application using an indirect inoculation method. The apparatus is designed so it can be easily built or obtained by any interested party.1.2 This test method can be used to evaluate the comparative resistance of coated building products to accelerated mold growth. Ratings do not imply a specific time period that the coated building product will be free of fungal growth during installation in an interior environment.1.3 This test method is not intended for use in the evaluation of public health claims.1.4 The test method is intended for the accelerated evaluation of mold growth on a coated building product designed for interior use. This method is not intended for evaluation of surfaces designed for exterior applications or uncoated surfaces. Use of this test method for evaluating exterior performance has not been validated, nor have the limitations for such use been determined.1.5 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 The test gives an estimate of the ability of a rubber vulcanizate to resist crack growth of a pierced specimen when subjected to bending or flexing.4.2 No exact correlation between these test results and service is implied due to the varied nature of service conditions.1.1 This test method covers the determination of crack growth of vulcanized rubber when subjected to repeated bending strain or flexing. It is particularly applicable to tests of synthetic rubber compounds which resist the initiation of cracking due to flexing when tested by Method B of Test Methods D430. Cracking initiated in these materials by small cuts or tears in service, may rapidly increase in size and progress to complete failure even though the material is extremely resistant to the original flexing-fatigue cracking. Because of this characteristic of synthetic compounds, particularly those of the SBR type, this test method in which the specimens are first artificially punctured in the flex area should be used in evaluating the fatigue-cracking properties of this class of material.1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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