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5.1 This test method is useful for the determination of elemental concentrations in the range of approximately 0.1 µgg-1 to 10 percent (%) (See Table X1.1) in soda-lime glass samples (7 and 8). A standard test method can aid in the interchange of data between laboratories and in the creation and use of glass databases.5.2 The determination of elemental concentrations in glass provides high discriminating value in the forensic comparison of glass fragments.5.3 This test method produces minimal destruction of the sample. Microscopic craters of 50 µm to 100 µm in diameter by 80 µm to 150 µm deep are left in the glass fragment after analysis. The mass removed per replicate is approximately 0.4 µg to 3 µg (6).5.4 Appropriate sampling techniques shall be used to account for natural heterogeneity of the materials at a microscopic scale.5.5 The precision, bias, and limits of detection of the method (for each element measured) shall be established during validation of the method. The measurement uncertainty of any concentration value used for a comparison shall be recorded with the concentration.5.6 Acid digestion of glass followed by either Inductively Coupled Plasma-Optical Emission Spectrometry (ICP-OES) or Inductively Coupled Plasma-Mass Spectrometry (ICP-MS) can also be used for trace elemental analysis of glass, and offer similar detection levels and the ability for quantitative analysis. However, these methods are destructive, and require larger sample sizes and more sample preparation (Test Method E2330).5.7 Micro X-Ray Fluorescence (µ-XRF) uses comparable sample sizes to those used for LA-ICP-MS with the advantage of being non-destructive of the sample. Some of the drawbacks of µ-XRF include lower sensitivity and precision, and longer analysis time (Test Method E2926).5.8 Scanning Electron Microscopy with Energy Dispersive Spectrometry (SEM-EDS) is also available for elemental analysis, but it is of limited use for forensic glass source discrimination due to poor detection limits for higher atomic number elements present in glass at trace concentration levels. However, distinguishing between sources having similar RIs and densities is sometimes possible.1.1 This test method covers a procedure for the quantitative elemental analysis of the following seventeen elements: lithium (Li), magnesium (Mg), aluminum (Al), potassium (K), calcium (Ca), iron (Fe), titanium (Ti), manganese (Mn), rubidium (Rb), strontium (Sr), zirconium (Zr), barium (Ba), lanthanum (La), cerium (Ce), neodymium (Nd), hafnium (Hf) and lead (Pb) through the use of laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS) for the forensic comparison of glass fragments. The potential of these elements to provide the best discrimination among different sources of soda-lime glasses has been published elsewhere (1-5).2 Silicon (Si) is also monitored for use as a normalization standard. Additional elements may be added as needed, for example, tin (Sn) can be used to monitor the orientation of float glass fragments.1.2 The method only consumes approximately 0.4 µg to 3 µg of glass per replicate and is suitable for the analysis of full thickness samples as well as irregularly shaped fragments as small as 0.1 mm by 0.1 mm by 0.2 mm (6) in dimension. The concentrations of the elements listed above range from the low parts per million (µgg-1) to percent (%) levels in soda-lime glass, the most common type encountered in forensic cases. This standard method can be applied for the quantitative analysis of other glass types; however, some modifications in the reference standard glasses and the element menu may be required.1.3 This standard is intended for use by competent forensic science practitioners with the requisite formal education, discipline-specific training (see Practice E2917), and demonstrated proficiency to perform forensic casework.1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Overview: 4.1.1 Assurance of product quality is derived from careful attention to many factors but is not limited to raw material acceptance, software workflow definition, product and process design and control, printing and post processing, equipment and systems installation, maintenance, and in-process and end-product testing.4.1.2 By managing these factors, a manufacturer can establish confidence that all finished manufactured units from successive lots will be acceptable and meet lot release criteria.4.1.3 The basic principles of quality assurance (QA) have as their goal the production of articles that are fit for their intended use. These principles may be stated as:4.1.3.1 Quality, safety, and effectiveness shall be designed and built into the product as well as the production process.4.1.3.2 AM product characteristics all cannot currently be verified after the process without destructive testing and therefore requires validation. Suitable consideration should be designed into the product and controls should be applied to the process during process validation.4.1.3.3 Critical steps of the production process impacting quality shall be controlled to maximize the probability that the finished product meets all quality and design specifications.4.1.4 Process validation is a key element in ensuring that these QA goals are met. Routine end-product testing alone is often not sufficient to assure product quality. Some end-product tests have limited sensitivity. In some cases, destructive testing would be required to show that the manufacturing process is adequate, and in other situations, end-product testing does not reveal all variations that may occur in the product that may have an impact on device performance. However, successfully validating a process may reduce the dependence on intensive in-process and finished product testing. Note that, in most cases, end-product testing plays a major role in supporting QA goals, that is, validation and end-product testing are not mutually exclusive.4.1.5 Key process variables should be monitored and documented using statistical process control where applicable. Analysis of the data collected from monitoring should establish the potential variability of process parameters for individual production runs to ensure that a process is within acceptable control limits and the equipment can consistently produce the product within specification.4.2 Preliminary Considerations: 4.2.1 A manufacturer should evaluate all factors that affect product quality through appropriate documented process characterization.4.2.2 Risk management and an analysis file shall be created in line with ISO 14971. These factors may vary considerably among different products, manufacturing technologies, and facilities. No single approach to process validation will be appropriate and complete in all cases; however, the following quality steps should be undertaken.4.2.3 All pertinent aspects of the production processes that have an impact on device design (product’s end use) should be considered during process validation. These aspects include, but are not necessarily limited to, performance, reliability, and stability. Performance limits and variation should be established for each characteristic acceptance criteria and expressed in readily measurable terms. Once a product specification is defined it is important that any changes to it be made in accordance with documented change control procedures and the device history file.1.1 This practice provides an overview of how to perform process validation for medical devices manufactured using PBF/LB/M. The topics that will be covered include machine qualifications, software used in the manufacturing process, the importance of design specification and verification on process validation, and raw materials.1.2 This practice also provides recommendations for process characterization, risk management, additive manufacturing (AM) facility qualification, and process control as a prerequisite for qualification activity, including installation qualification/operational qualification/performance qualification (IQ/OQ/PQ).1.3 The practice is primarily focused on non-device-specific AM system(s) validation. Additional information may be needed in reference to the performance of the actual device.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The presence and concentration of total oil and grease as well as total petroleum hydrocoarbons, in domestic and industrial wastewater is of concern to the public because of its deleterious aesthetic effect and its impact on aquatic life.5.2 Regulations and standards have been established that require monitoring of total oil and grease as well as total petroleum hydrocarbons in water and wastewater.1.1 This test method covers the determination of total oil and grease (TOG) and total petroleum hydrocarbons (TPH) in water and waste water that are extractable by this test method from an acidified sample with a cyclic aliphatic hydrocarbon (for example cyclohexane, cyclopentane) and measured by IR absorption in the region from 1370 cm–1 to 1380 cm–1 (7.25 μm to 7.30 μm) using a mid-IR laser spectrometer. Polar substances are removed by clean-up with Florisil.21.2 This test method also considers the volatile fraction of petroleum hydrocarbons, which is lost by gravimetric methods that require solvent evaporation prior to weighing, as well as by solvent-less IR methods that require drying of the employed solid phase material prior to measurement. Similarly, a more complete fraction of extracted petroleum hydrocarbons are accessible by this test method as compared to GC methods that use a time window for quantification, as petroleum hydrocarbons eluting outside these windows are quantified too.1.3 This test method covers the range of 0.1 mg/L to 1000 mg/L and may be extended to a lower or higher level by extraction of a larger or smaller sample volume collected separately.1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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General Utility—The molecular mass (MM) and molecular mass distribution (MMD) are fundamental characteristics of a synthetic polymer that result from the polymerization process. The MM and MMD is useful for a wide variety of correlations for fundamental studies, processing and product applications. For example, it is possible to compare the observed MMD to predictions from an assumed kinetic or mechanistic model for the polymerization reaction. Differences between the values will allow alteration of the model or experimental design. Similarly, it is possible the strength, the melt flow rate, and other properties of a polymer are dependent on the MM and MMD. Determination of the MM and MMD are used for quality control of polymers and as specification in the commerce of polymers.Limitations—If the MMD is too wide, it is possible that the assumption of the constancy of the intensity scale calibration is in serious error.1.1 This test method covers the determination of molecular mass (MM) averages and the distribution of molecular masses for linear atactic polystyrene of narrow molecular mass distribution (MMD) ranging in molecular masses from 2000 g/mol to 35 000 g/mol by matrix assisted laser desorption/ionization time-of-flight mass spectrometry (MALDI-TOF-MS). This test method is not absolute and requires the use of biopolymers for the calibration of the mass axis. The relative calibration of the intensity axis is assumed to be constant for a narrow MMD. Generally, this is viewed as correct if the measured polydispersity is less than 1.2 for the molecular mass range given above.1.2 The values stated in SI units are to be regarded as the standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.Note 1—There is no known ISO equivalent to this standard.

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5.1 This guide describes the use of torque and angle-of-twist data as a preliminary acceptance criteria for a production run utilizing a previously qualified AM process through periodical or continuous evaluation. A torsion device (for example, torque wrench, instrumented lathe with torque readout) is used to break strategically placed torque specimens within the build volume in the as-built state to provide evidence of build health. If a round of tests from a production run is determined to fall outside of some criteria (for example: 3 standard deviations from the mean or other user defined criteria), additional qualification procedures should be performed to ensure the AM machine or process health are acceptable.NOTE 1: It is advantageous to locate the specimen at the same build height and near-critical locations of the part or component being fabricated for the evaluation to be representative of the specific region.5.2 This guide is not intended to replace rigorous qualification procedures and should only be considered as a preliminary acceptance criterion to increase confidence that an AM machine or process has not been significantly compromised.1.1 This guide illustrates a test specimen geometry and testing protocol that can be used to assess the quality of a metal powder bed fusion build cycle as it could be affected by major system errors (for example, corrupted calibration, disrupted inert gas flow, laser wear) severely affecting the quality of materials fabricated by laser beam powder bed fusion (PBF-LB).1.2 This method is designed to interrupt the manufacturing process if poor material quality is identified through go/no-go torque/angle of twist measurements of witness coupons after each fabrication.1.3 Units—The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this guide.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method is useful for the analysis of total uranium in water following wet-ashing, as required, due to impurities or suspended materials in the water.1.1 This test method covers the determination of total uranium, by mass concentration, in water within the calibrated range of the instrument, 0.1 μg/L or greater. Samples with uranium mass concentrations above the laser phosphorimeter dynamic range are diluted to bring the concentration to a measurable level.1.2 This test method was used successfully with reagent water. It is the user’s responsibility to ensure the validity of this test method for waters of untested matrices.1.3 The values stated in SI units are to be regarded as the standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 All S/H systems change with time and use. Therefore, a calibration procedure for evaluating the operation of an S/H system is desirable. This calibration procedure provides a method of obtaining an optimized interferometric image pattern associated with a given size anomaly.5.2 The use of straining blocks as calibration devices provides a means for ensuring the continued optimal performance of the S/H system. Straining blocks can also be used to compare performance of S/H systems in different facilities.5.3 At not greater than a three (3) month interval the S/H system shall be calibrated following the procedures described in this practice. When necessary, adjustments, repairs, or modifications shall be made to the S/H system until it is able to observe, in the same image, all anomalies of size within the range of interest contained in the straining blocks.1.1 This practice describes the construction and use of a calibration device for demonstrating the anomaly detection capability of interferometric laser imaging nondestructive tire inspection system. A common practice within the industry is to refer to these systems as shearographic/holographic (S/H) systems.1.2 This standard practice applies to S/H systems that are used for evaluating the structural integrity of pneumatic tires, (for example, presence or absence of anomalies within the tire).1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 H2S measurements in natural gas are performed to ensure concentrations satisfy gas purchase contract criteria and to prevent pipeline and associated component corrosion.5.2 Using TDLAS for the measurement of H2S in natural gas enables a high degree of selectivity with minimal interference from common constituents in natural gas streams. The TDLAS analyzer can detect changes in concentration with a relatively rapid response compared to other methods so that operators may take swift action when designated H2S concentrations are exceeded.5.3 Primary applications covered in this test method are listed in 5.3.1 and 5.3.2. Each application may have differing requirements and methods for gas sampling. Additionally, different natural gas applications may require unique spectroscopic considerations.5.3.1 Raw natural gas is found in production, gathering sites, and inlets to gas-processing plants characterized by potentially high levels of water (H2O), carbon dioxide (CO2), H2S, and heavy hydrocarbons. Gas-conditioning plants and skids are normally used to remove H2O, CO2, H2S, and other contaminants.5.3.2 High-quality “sales gas” is found in transportation pipelines, natural gas distribution (utilities), and natural gas power plant inlets. The gas is characterized by a very high percentage of methane (90 to 100 %) with small quantities of other hydrocarbons and trace levels of contaminants.1.1 This test method is for the online determination of hydrogen sulfide (H2S) in natural gas using tunable diode laser absorption spectroscopy (TDLAS) analyzers also known as a “TDL analyzers.” The particular wavelength for H2S measurement varies by manufacturer, typically between 1000 and 10 000 nm with an individual laser having a tunable range of less than 10 nm. The H2S concentration ranges can be anywhere from 0-5  ppm(v) to 0-90 % by volume.1.2 Units—The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard. TDLAS analyzers inherently output concentrations in unitless molar ratios such as ppm(v).NOTE 1: Weight-per-volume units such as milligrams or grains of H2S per cubic foot or cubic meter can be derived from ppm(v) at “standard conditions” or standard temperature and pressure.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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1.1 Scope IEC 60825-1 is applicable to safety of laser products. For convenience it is divided into three separate sections: Section One (General) and the annexes; Section Two (Manufacturing requirements); and Section Three (User's guide ). A laser

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5.1 This guide provides a means of using an LD instrument to obtain a droplet size distribution from a spray in gas co-flow that approximates a flux-sensitive sample.45.2 In many sprays, the experimenter shall account for spatial segregation of droplets by size. This guide provides a means of spatial averaging the droplet distribution.5.3 The results obtained will be statistical in nature and refer to the time average of droplet size distribution of the entire spray.5.4 This guide is used to calibrate a spray generation device to produce a desired droplet size distribution under prespecified environmental and co-flow conditions or characterize an unknown spray while minimizing the uncertainty in the measurement.1.1 The purpose of this guide is to define a test procedure for applying the laser diffraction (LD) method to estimate an average droplet size distribution that characterizes the flux of liquid droplets produced by a specified spray generation device under specified gas co-flow conditions using a specified liquid. The intended scope is limited to artificially generated sprays with high speed co-flow. The droplets are assumed to be in the size range of 1 to 2000 µm in diameter and occur in sprays that are contained within a volume as small as a few cubic centimetres or as large as a cubic metre. The droplet sizes are assumed to be distributed non-uniformly within the spray volume.1.2 This guide is intended primarily to guide measurement of performance of nozzles and atomizers using LD instruments.1.3 Non-uniform sprays require measurements across the entire spray cross section or through several chords providing a representative sample of the overall spray cross section. The aim of multiple-chord measurements is to obtain a single droplet size distribution that characterizes the whole spray rather than values from a single chordal measurement.1.4 Use of this guide requires that the instrument does not interfere with spray production and does not significantly impinge upon or disturb the co-flow of gas and the spray. This technique is, therefore, considered non-intrusive.1.5 The computation of droplet size distributions from the light-scattering distributions is done using Mie scattering theory or Fraunhofer diffraction approximation. The use of Mie theory accounts for light refracted through the droplet and there is a specific requirement for knowledge of both real (refractive) and imaginary (absorptive) components of the complex index of refraction. Mie theory also relies on an assumption of droplet homogeneity. The Fraunhofer diffraction approximation does not account for light refracted through the droplet and does not require knowledge of the index of refraction.1.6 The instruments shall include data-processing capabilities to convert the LD scattering intensities into droplet size distribution parameters in accordance with Practice E799 and Test Method E1260.1.7 The spray is visible and accessible to the collimated beam produced by the transmitter optics of the LD instrument. The shape and size of the spray shall be contained within the working distance of the LD system optics as specified by the instrument manufacturer.1.8 The size range of the LD optic should be appropriate to the spray generation device under study. For example, the upper bound of the smallest droplet size class reported by the instrument shall be not more than 1/4 the size of DV0.1.1.9 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.10 This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.11 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test method permits a user to compare the performance of an instrument to the tolerance limit specifications stated by a manufacturer and to verify that an instrument is suitable for continued routine use. It also provides for generation of calibration data on a periodic basis, forming a database from which any changes in the performance of the instrument will be evident.4.2 This test method for the calibration verification of laser diffraction particle sizing instruments is suitable for acceptance testing of laser diffraction instruments so long as current estimates of the bias (see Section 11) and the between-laboratory precision of the test method (see Section 10) are acceptably small relative to typical laser diffraction instrument accuracy specifications; see Practice D3244.1.1 This test method describes a procedure necessary to permit a user to easily verify that a laser diffraction particle sizing instrument is operating within tolerance limit specifications, for example, such that the instrument accuracy is as stated by the manufacturer. The recommended calibration verification method provides a decisive indication of the overall performance of the instrument at the calibration point or points, but it is specifically not to be inferred that all factors in instrument performance are verified. In effect, use of this test method will verify the instrument performance for applications involving spherical particles of known refractive index where the near-forward light scattering properties are accurately modeled by the instrument data processing and data reduction software. The precision and bias limits presented herein are, therefore, estimates of the instrument performance under ideal conditions. Nonideal factors that could be present in actual applications and that could significantly increase the bias errors of laser diffraction instruments include vignetting4 (that is, where light scattered at large angles by particles far away from the receiving lens does not pass through the receiving lens and therefore does not reach the detector plane), the presence of nonspherical particles, the presence of particles of unknown refractive index, and multiple scattering.1.2 This test method shall be used as a significant test of the instrument performance. While the procedure is not designed for extensive calibration adjustment of an instrument, it shall be used to verify quantitative performance on an ongoing basis, to compare one instrument performance with that of another, and to provide error limits for instruments tested.1.3 This test method provides an indirect measurement of some of the important parameters controlling the results in particle sizing by laser diffraction. A determination of all parameters affecting instrument performance would come under a calibration adjustment procedure.1.4 This test method shall be performed on a periodic and regular basis, the frequency of which depends on the physical environment in which the instrumentation is used. Thus, units handled roughly or used under adverse conditions (for example, exposed to dust, chemical vapors, vibration, or combinations thereof) shall undergo a calibration verification more frequently than those not exposed to such conditions. This procedure shall be performed after any significant repairs are made on an instrument, such as those involving the optics, detector, or electronics.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Leaks in blister packs may affect product quality and such defects can arise from imperfections in the packaging material or bond between the sealed surfaces.5.2 This method of leak testing is a useful tool as it allows non-destructive and non-subjective leak testing of blister packs. It allows the operator to evaluate how different packaging materials and packaging machine conditions affect the integrity of the packaging. It can also provide indication of unwanted changes in the packaging conditions.5.3 This type of testing is typically used in pharmaceutical packaging production, during stability trials and for package research and development operations because of its non-destructive nature, cleanliness, and speed.1.1 Test Packages—This test method can be applied to non-porous blister packs sealed with flexible films such as those used in pharmaceutical packaging. Such blister packs typically consist of thermoformed polymer or cold formed aluminum trays that contain a number of individual blister pockets into which tablets or capsules are placed. The trays are then sealed with a polymer, paper-backed or foil-based flexible laminate lidding material.1.2 Leaks Detected—This test method detects leaks in blister packs by measuring the deflection of the blister pack surface in response to an applied vacuum. This deflection of the blister pack surface results from the difference in pressure between the gas inside the blister pack and the applied vacuum. Air loss from within a blister pocket as a result of a leak will alter this pressure differential causing a measureable variation in blister pocket deflection. This test method requires that the blister packs are held in appropriate tooling inside a suitable test chamber.1.3 Test Results—Test results are reported qualitatively (pass/fail). Appropriate acceptance criteria for deflection, height, and collapse values are established by comparing non-leaking packs with those containing defects of a known size. Suitably sized defects in the laminate, tray material, and seal can be detected using this test method. The sensitivity of this test method depends upon a range of factors including blister pocket headspace, blister pocket size, lidding material type, lidding material thickness, lidding material tension, printing, surface texture, test conditions, and the values selected for the pass/fail acceptance criteria. The ability of the test to detect 15 µm, 50 µm, and catastrophic sized holes in four blister pack designs was demonstrated in a study.1.4 The values stated in SI units are to be regarded as standard and no other units of measurement are included in this test method.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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5.1 The present and growing international governmental requirements to add FAME (biodiesel, as specified in standards such as Specification D6751 and EN 14214) to diesel fuel has had the side effect of leading to potential FAME contamination of jet turbine fuel in multifuel transport facilities such as cargo tankers and pipelines. FAME has been added as an identified incident material to Table 3 of Specification D1655 in which a permitted level of contamination is specified.5.2 This test method has been developed for use in the supply chain by nonspecialized personnel to detect all kinds of FAME covering the range of 10 mg/kg to 400 mg/kg.NOTE 3: This test method can be used to screen for unconverted esters from lipid co-hydroprocessed hydrocarbon synthetic kerosene in aviation turbine fuel. This application is detailed in X1.2.1.1 This test method covers the quantification of the fatty acid methyl esters (FAME) content in aviation turbine fuel in the range of 10 mg/kg to 400 mg/kg by measuring infrared (IR) transmission before, during, and after FAME is converted to molecules that absorb in a different spectral region than FAME using a selective chemical reaction facilitated by a suitable catalyst.NOTE 1: This test method detects all FAME components with peak IR absorbance at approximately 1749 cm-1 and C8 to C22 carbon chain length. The accuracy of this test method is based on the molecular weight of C16 to C18 FAME species. The presence of other FAME species with different molecular weights could affect the accuracy.NOTE 2: Additives such as antistatic agents, antioxidants, and corrosion inhibitors are measured with the FAME by mid IR absorption. However, these additives do not contribute to the differential absorption spectrum used to quantify FAME, as they do not take part in the selective reaction.1.2 This test method has interim repeatability precision only, see Section 15 for more information.1.3 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific warning statements are given in Section 8.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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1.1 This specification covers additive manufacturing of parts manufactured via laser beam powder bed fusion (PBF-LB) processing of niobium-hafnium alloy used in spaceflight applications. Parts made using this processing method are typically used in applications that require mechanical properties like wrought products. Products built to this specification may require additional post-processing in the form of machining, polishing etc. to meet necessary surface finish and dimensional tolerances.1.2 This specification is intended for the use of purchasers or producers, or both, of PBF-LB R04295 parts for defining the requirements based on classification methodology. These requirements shall be agreed upon by the part supplier and purchaser.1.3 Users are advised to use this specification as a basis for obtaining parts that will meet the minimum acceptance requirements established and revised by consensus of committee members.1.4 User requirements considered more stringent may be met by the addition to the purchase order.1.5 Units—The values stated in SI units are to be regarded as the standard. Other units are included only for informational purposes.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价: 590元 / 折扣价: 502 加购物车

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This specification covers laser-fused stainless steel bars, plates, and shapes of structural quality for use in bolted or welded structural applications. The butt-welded test pieces are welded using laser fusion and then machined into tensile test bars and root-bend test specimens. The term laser fusion is used in this specification to refer to a joining process that is able to produce a coalescence of material using the heat obtained from the application of a concentrated coherent light beam impinging on the surface of a weld joint.1.1 This specification covers laser and laser hybrid welded stainless steel bars, plates, sharp-cornered profile (SCP), and built-up shapes of structural quality for use in bolted or welded structural applications. SCP and built-up shapes are used in, but not limited to, the following applications: industrial and general structural applications like buildings, including architecturally exposed steel structures (AESS); architectural steel profiles, such as curtain wall and staircases.NOTE 1: The term laser fusion is also used to describe laser welding.1.1.1 Supplementary requirements of an optional nature are provided. They shall apply only when specified by the purchaser.NOTE 2: Since the product covered by this specification is manufactured in small lots on dedicated production lines, minimum product quality requirements are ensured by requiring welding process specification and operator qualification at each manufacturing facility in accordance with AWS, ASME, or ISO requirements. If required, the purchaser can specify higher levels of weld inspection; supplementary requirements for mechanical and corrosion testing; and other requirements.NOTE 3: Because of the varying requirements of the end-use applications, different length tolerance and weld inspection levels may be specified.1.2 Shapes covered in this specification include those defined in Article 3.1.2 of Specification A6/A6M, square and rectangular hollow sections, and additional shapes, including customized, that are made from two or more shapes, plates, bar, sheet, or strip.1.3 This specification establishes the minimum requirements for manufacturing of laser and laser hybrid welded stainless steel shapes and requires the welds to, at a minimum, match the tensile and yield strength of the base metal. If base metals of different strengths are used, the lower strength base metal shall be matched.1.4 This specification refers to Specifications A240/A240M, A276/A276M, or A479/A479M for chemical requirements, but the mechanical test requirements are determined by the mechanical properties section of this standard. This standard includes four strength grades. The default strength grade 1 is determined by the base metal standard. Grades 2 through 4 are for specification of higher strength levels.1.5 The text of this specification contains notes and footnotes that provide explanatory material. Such notes and footnotes, excluding those in tables and figures, do not contain any mandatory requirements.1.6 Units—This specification is expressed in both inch-pound units and in SI units; however, unless the purchase order or contract specifies the applicable M specification designation (SI units), the inch-pound units shall apply. The values stated in either inch-pound units or SI units are to be regarded separately as standard. Within the text, the SI units are shown in brackets. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价: 590元 / 折扣价: 502 加购物车

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