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4.1 If ASTM Committee E13 has not specified an appropriate test procedure for a specific type of instrument, or if the sample specified by a Committee E13 procedure is incompatible with the intended instrument operation, then this practice can be used to develop practical performance tests.4.1.1 For instruments which are equipped with permanent or semi-permanent sampling accessories, the test sample specified in a Committee E13 practice may not be compatible with the instrument configuration. For example, for FT-MIR instruments equipped with transmittance or IRS flow cells, tests based on putting polystyrene films into the sample position are impractical. In such cases, this practice suggests means by which the recommended test procedures can be modified by changing the test material or the location of the recommended test material.4.1.2 For instruments used in process measurements, the choice of test materials may be limited due to process contamination and safety considerations. The practice suggests means of developing performance tests based on materials which are compatible with the intended use of the analyzer.4.2 Tests developed using the practice are intended to allow the user to compare the performance of an instrument on any given day with prior performance, and specifically to compare performance during calibration of the analyzer to performance during validation of the analyzer and during routine use of the analyzer. The tests are intended to uncover malfunctions or other changes in instrument operation, but they are not designed to diagnose or quantitatively assess the malfunction or change. The tests are not intended for the comparison of analyzers of different manufacture.4.3 Tests developed using this practice are also intended to allow the user to compare the performance of a primary analyzer used in development of a multivariate model to the performance of secondary analyzers used to apply that model for the analysis of process or product samples.1.1 This practice covers basic procedures that can be used to develop instrument performance tests for spectroscopic based online, at-line, laboratory and field analyzers. The practice is intended to be applicable to Raman spectrometers and to infrared spectrophotometers operating in the near-infrared and mid-infrared regions.1.2 This practice is not intended as a replacement for specific practices, such as Practices E275, E925, E932, E958, E1421, or E1683 that exist for measuring performance of specific types of laboratory spectroscopic instruments. Instead, this practice is intended to provide guidelines as to how similar practices should be developed when specific practices do not exist for a particular instrument type, or when specific practices are not applicable due to sampling or safety concerns. This practice can be used to develop instrument performance tests for on-line process spectroscopic-based analyzers.1.2.1 The performance tests described in this practice typically only evaluate the performance of the infrared spectrophotometer or Raman spectrometer part of the analyzer system, referred to herein as the instrument.1.2.2 Instrument performance tests do not typically evaluate performance of analyzer sampling systems.1.3 This practice describes univariate level zero and level one tests, and multivariate level A and level B tests which can be implemented to measure instrument performance. These tests are designed to be used as rapid, routine checks of instrument performance. They are designed to uncover malfunctions or other changes in instrument operation, but do not specifically diagnose or quantitatively assess the malfunction or change. The tests are not intended for the comparison of instruments or analyzers of different manufacture.1.4 The instrument performance tests described in this practice are used during the development of multivariate calibrations via Practice D8321 to establish the performance level at the time the calibration is developed. The same tests are used during validation of analyzers via Practice D6122 to qualify the working analyzer by demonstrating comparable performance.1.4.1 Instrument performance tests are used to requalify instruments after analyzer maintenance.1.4.2 Instrument performance tests are used to qualify instruments in secondary analyzers to which calibrations are being transferred after development on a primary analyzer.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Demonstration plans developed in accordance with this practice will include all necessary content and key considerations to support an effective flight demonstration program aimed at approval or certification of UAS by the FAA through D&R demonstration.4.2 This practice does not address planning requirements for UAS development testing. It is assumed that a manufacturer has completed all UAS design and development and is preparing demonstration programs to support compliance demonstration on a stable and controlled system configuration. Manufacturers who wish to prepare a detailed design and development program should review Specification F3298 for programmatic examples.4.3 This practice is intended to be used on low-risk UAS that meet the following design criteria and operating limitations.4.3.1 The UAS has a command and control link that enables the pilot-in-command to take contingency action.4.3.2 The unmanned aircraft (UA) has a kinetic energy of ≤25 000 ft-lb calculated in accordance with methods specified within the MOC.4.3.3 The UA is operated ≤400 ft above ground level (AGL).4.3.4 No operations over open-air assemblies (operations over people are acceptable).4.3.5 No flight into known icing.4.3.6 Maximum of 20:1 aircraft to pilot ratio.4.3.7 The UA is electrically powered (excludes internal combustion engines and fuel cells).1.1 This standard practice is intended for low-risk UAS seeking type certification by the Federal Aviation Administration (FAA) under 14 CFR Part 21.17(b) in accordance with the FAA durability and reliability (D&R) means of compliance (MOC). The definition of “low-risk UAS” does not necessarily align with other definitions found within corresponding ASTM standards (F3442/F3442M) or other UAS-related standards. For the purposes of this practice, “low-risk” is defined as a UAS operated in accordance with the concept of operations (CONOPs), eligibility criteria, and kinetic energy threshold specified in the G-1 Issue Paper (which will be provided to the applicant by the FAA). See 4.3 for design criteria and operating limitations for low-risk UAS.1.2 This standard practice establishes a common methodology and key considerations for the development of minimum flight plans for low-risk UAS that demonstrate aircraft reliability as part of a D&R MOC.1.3 The scope of this standard practice encompasses D&R planning, data collection, and reporting.1.4 The values stated in SI units are to be regarded as standard. This is not intended to limit the systems of units used for design, development testing, or demonstration testing. However, the units of measurement used on pilot-facing placards and markings and manuals must be the same as those used on the corresponding equipment with recognition that international aviation utilizes feet for altitude and knots for airspeed as operational parameters.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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The purpose of this practice is to provide guidance to owners, mechanics, airports, regulatory officials, and aircraft and component manufacturers who may accomplish maintenance, repairs, and alterations on a light unmanned aircraft system (UAS). In addition, this practice covers the format and content of maintenance manuals and instructions for the maintenance, repair, and alteration of light UAS. The light UAS can be operated as a commercial aircraft or as a sport aircraft. This practice states the requirements for the maintenance of light commercial UAS. These same requirements may be used for the sport light UAS with the provisions shown. The maintenance requirements are divided between the aircraft and the ground equipment. The aircraft contains the air data terminal and the ground station controls the nearby ground data terminal. Therefore, the data link is not listed as a separate component, but has elements in the aircraft and near the ground station that is called the ground data terminal.1.1 This practice provides guidelines for the qualifications to accomplish the various levels of maintenance on certificated light unmanned aircraft system (UAS). In addition, it provides the content and structure of maintenance manuals for aircraft, ground control station, and data links that are operated as a light unmanned aircraft system (UAS).This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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4.1 The ASTM guidance manual, Form and Style for ASTM Standards,4 Section A21, requires a precision and bias statement in all ASTM test methods. Section A21.2.2 states:  Precision shall be estimated in accordance with the interlaboratory test program prescribed in Practice E691, Conducting an Interlaboratory Study to Determine the Precision of a Test Method, or by an interlaboratory test program that yields equivalent information, for example, a standard practice developed by an ASTM technical committee.4.2 Practice D2777, Section 1.1, states:  This practice establishes uniform standards for estimating and expressing the precision and bias of applicable test methods for Committee D19 on Water. Statements of precision and bias in test methods are required by the Form and Style for ASTM Standards, “Section A21. Precision and Bias (Mandatory).” In principle, all (ASTM Committee D19) test methods are covered by this practice.4.3 Practice D2777, Section 1.2, requires a task group proposing a new test method to carry out a collaborative study from which concentration limits, repeatability and reproducibility precision and bias statements are developed.4.3.1 This guide describes options for developing and optimizing chemical test methods for Committee D19, not implementation of a test method by a laboratory. Refer to Guide E2857 for procedures used in validating existing test methods for your laboratory.4.3.2 The collaborative study described in Practice D2777 is not the test method validation. The collaborative study verifies the new test method is reproducible among different laboratories, different instruments/apparatus, and different analysts.4.3.3 Practice D2777, Section 6.1, assumes the test method has already been optimized prior to conducting the collaborative study.4.4 Practice D2777, Section 4 (Summary of Practice), requires, a collaborative study only after the task group has assured itself that preliminary evaluation work is complete and the test method has been written in its final form.4.5 Practice D2777, Section 5.2 (), requires the collaborative test corroborates the test method write up (preliminary evaluation) within the limits of the test design.4.5.1 The assumption is that the collaborative study is a fair evaluation of the inter-laboratory variability when using the test method to analyze the matrices, and concentration ranges specified in the test method.4.6 Practice D2777, Section 6 (Preliminary Studies), requires considerable pilot work on a test method should precede the determination of precision and bias (collaborative study). This pilot work evaluates such variables as:4.6.1 Representative Sampling,4.6.2 Suitability of containers,4.6.3 Preservation requirements,4.6.4 Identification of interferences,4.6.5 Holding times (Practice D4841),4.6.6 Concentration range,4.6.7 Quantitation ranges,4.6.8 Concentration and preparation of reagents,4.6.9 Reagent standardization,4.6.10 Shelf life of reagents,4.6.11 Calibration,4.6.12 QC, and4.6.13 Sample size.4.7 Potentially significant factors are investigated in advance and are controlled in the written test method that is distributed for the collaborative test.4.8 Only after the proposed test method has been thoroughly tried and proved and reduced to unequivocal written form should a collaborative test be conducted.4.9 The Committee D19 test method is written in two steps:4.9.1 Step I—Single laboratory characterization or optimization (Practice D2777, Section 6.3.1.1).4.9.2 Step II—Collaborative study (Practice D2777, Section 6.3.1.2).4.10 This document is a guide to Committee D19 task groups developing chemical test methods.1.1 This guide identifies procedures for use in developing and optimizing new or modified Subcommitees D19.05 and D19.06 test methods intended for regulatory compliance reporting in EPA drinking water and wastewater programs. This guide may also be useful for developing test methods for emerging contaminants that may not yet have regulatory requirements.1.2 This guide also cites statistical procedures that are useful in the single laboratory characterization and optimization and in the inter-laboratory studies (ILSs).1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This guide offers an organized collection of information or a series of options and does not recommend a specific course of action. This document cannot replace education or experience and should be used in conjunction with professional judgment. Not all aspects of this guide may be applicable in all circumstances. This ASTM standard is not intended to represent or replace the standard of care by which the adequacy of a given professional service must be judged, nor should this document be applied without consideration of a project’s many unique aspects. The word “Standard” in the title of this document means only that the document has been approved through the ASTM consensus process.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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3.1 Trajectory models are used to predict the future movement and fate of oil (forecast mode) in contingency planning, in exercises and during real spill events. This information is used for planning purposes to position equipment and response personnel in order to optimize a spill response. Oil-spill trajectory models are used in the development of scenarios for training and exercises. The use of models allows the scenario designer to develop incidents and situations in a realistic manner.3.2 Oil-spill trajectory models can be used in a statistical manner (stochastic mode) to identify the areas that may be impacted by oil spills.3.3 In those cases where the degree of risk at various locations from an unknown source is needed, trajectory models can be used in an inverse mode to identify the sources of the pollution (hindcast mode).3.4 Models can also be used to examine habitats, shorelines, or areas to predict if they would be hit with oil from a given source (receptor mode).1.1 This practice describes the features and processes that should be included in an oil-spill trajectory and fate model.1.2 This practice applies only to oil-spill models and does not consider the broader need for models in other fields. This practice considers only computer-based models, and not physical modeling of oil-spill processes.1.3 This practice is applicable to all types of oil in oceans, lakes, and rivers under a variety of environmental and geographical conditions.1.4 This practice applies primarily to two-dimensional models. Consideration is given to three-dimensional models for complex flow regimes.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Composite materials consist by definition of a reinforcement phase in a matrix phase. In addition, carbon-carbon composites often contain measurable porosity which interacts with the reinforcement and matrix. The composition and structure of the C-C composite are commonly tailored for a specific application with detailed performance requirements. The tailoring involves the selection of the reinforcement fibers (composition, properties, morphology, etc), the matrix (composition, properties, and morphology), the composite structure (component fractions, reinforcement architecture, porosity structure, microstructure, etc.), and the fabrication conditions (forming, assembly, forming, densification, finishing, etc.). The final engineering properties (physical, mechanical, thermal, electrical, etc.) can be tailored across a broad range with major directional anisotropy in the properties.4.2 Specifications for specific C-C composite components covering materials, material processing, and fabrication procedures are developed to provide a basis for fabricating reproducible and reliable structures. Designer/users/producers have to write C-C composite specifications for specific applications with well-defined composition, structure, properties and processing requirements. But with the extensive breadth of selection in composition, structure, and properties in C-C composites, it is virtually impossible to write a "generic" composite specification applicable to any and all C-C composite applications that has the same type of structure and details of the commonly-used specifications for metal alloys. This guide is written to assist the designer/user/producer in developing a comprehensive and detailed material specification for a specific CMC application/component with a particular focus on nuclear applications.4.3 The purpose of this guide is to provide guidance on how to specify the constituents, the structure, the desired engineering properties (physical, chemical, mechanical, durability, etc), methods of testing, manufacturing process requirements, the quality assurance requirements, and traceability for C-C composites for nuclear reactor applications. The resulting specification may be used for the design, production, evaluation, and qualification of C-C composites for structures in nuclear reactors.4.4 The guide is applicable to C-C composites with flat plate, rectangular bar, round rod, and round tube geometries.4.5 This guide may also be applicable to the development of specifications for C-C composites used for other structural applications, discounting the nuclear-specific chemical purity and irradiation behavior requirements.1.1 This document is a guide to preparing material specifications for fiber reinforced carbon-carbon (C-C) composite structures (flat plates, rectangular bars, round rods, and tubes) manufactured specifically for structural components in nuclear reactor core applications. The carbon-carbon composites consist of carbon/graphite fibers (from PAN, pitch, or rayon precursors) in a carbon/graphite matrix produced by liquid infiltration/pyrolysis and/or by chemical vapor infiltration.1.2 This guide provides direction and guidance for the development of a material specification for a specific C-C composite component or product for nuclear reactor applications. The guide considers composite constituents and structure, physical and chemical properties, mechanical properties, thermal properties, performance durability, methods of testing, materials and fabrication processing, and quality assurance. The C-C composite materials considered here would be suitable for nuclear reactor core applications where neutron irradiation-induced damage and dimensional changes are a significant design consideration. (1-4)21.3 The component specification is to be developed by the designer/purchaser/user. The designer/purchaser/user shall define and specify in detail any and all application-specific requirements for necessary design, manufacturing, and performance factors of the ceramic composite component. This guide for material specifications does not directly address component/product-specific issues, such as geometric tolerances, permeability, bonding, sealing, attachment, and system integration.1.4 This guide is specifically focused on C-C composite components and structures with flat panel, solid rectangular bar, solid round rod, or tubular geometries.1.5 This specification may also be applicable to C-C composites used for other structural applications discounting the nuclear-specific chemical purity and irradiation behavior factors.1.6 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This guide for development and implementation of a pollution prevention program is applicable to any organization or facility that releases materials to any of the three environmental media (air, water, or land) and that wishes to reduce those releases, without using treatment or transferring them to one of the other two media primarily for the purpose of disposal. Incentives for applying this standard of practice include concern for the environment, conservation of natural resources, economic considerations, and current and future regulatory compliance. Effective pollution prevention can also increase the efficiency of operations and use of resources, employee morale, and profitability while reducing liability.A successful pollution prevention program can save money by reducing waste management costs and raw material purchases, reduce potential emissions and disposal liabilities, protect public health and worker health and safety, and protect the environment. It will also position an organization to compete domestically and internationally through both long-term cost reductions and participation in green marketing opportunities.1.1 This guide covers guidance on a logical progression of tasks and procedures to be followed in a pollution prevention program to reduce or eliminate the generation of waste, the loss of natural resources, and process emissions through source reduction, reuse, recycling, and reclamation.1.2 Summary—The basic components of a pollution prevention program should include the following seven activities:1.2.1 Develop an organizational commitment to pollution prevention (see Section 4).1.2.2 Establish goals, objectives, and an implementation schedule (see Section 5).1.2.3 Generate baseline information (see Section 6).1.2.4 Develop a resource, emissions, and waste measurement and tracking system (see Section 7).1.2.5 Analyze pollution prevention opportunities (see Section 8).1.2.6 Prioritize pollution prevention opportunities (see Section 9).1.2.7 Implement and maintain the progress of a pollution prevention program (see Section 10).1.3 Organization of Text—This guide is organized based on the activities previously enumerated. Each section of the guide describes the manner in which the specified activity may be conducted to implement a program of pollution prevention at a facility.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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4.1 The test method enables strength values for wood and other materials bonded with an adhesive under a range of controlled bonding temperature, time, and pressure conditions to be evaluated. Bond formation and subsequent testing is affected in a coordinated fashion, and this enables transient strength values of sets of similar bond types to be explored with diverse parameters as independent variables. Principal among these variables is the temperature at which bonds are formed and the time that selected temperatures are maintained prior to testing. The use of controlled methods of adhesive application, the rapid attainment of stable bond formation conditions, and the rapid transition to the bond testing mode enables snapshots of bond strength to be attained as bonds progress from limited strength (or initial tack) to maximum strength. Derived data may be used to evaluate and compare the strength development characteristics of diverse types and formulations of adhesive. The method may thus be used to aid in tailoring and matching adhesives to the manufacture of diverse bonded products that involve heating.4.2 The method may also be used to evaluate the co-dependent effect of temperature and time on the degradation of sample bonds. Pressing temperatures up to 265°C (509°F) may be necessary for such investigations of thermal degradation. Specimens are pressed for a range of times and temperatures and very shortly thereafter tested either at elevated temperature or immediately following rapid forced air cooling. Alternatively, thermal damage of pre-formed bond samples may be evaluated by subjecting them to controlled temperature and time sequences prior to testing.4.3 The method may also be used to evaluate the effect of wood type and variability, or of non-wood materials, on bond strength development.4.4 By hermetically sealing the overlap region of sample bonds during their formation, the method may also be used to evaluate the effect of moisture and other resident volatile fluids on bond strength development.4.5 The method may also be used to evaluate the effect that the temperature at which variously formed bonds are tested has on their strength. Controlled rapid forced air cooling immediately after bond formation but before testing is necessary for such investigations. This approach may be employed to explore the thermoplastic characteristic of thermosetting adhesives and also the strength of hot melt adhesives as a function of pressing and testing temperatures.1.1 This test method concerns bonding and testing of wood adhesives and related adhesives using small scale tensile lap-shear samples in a manner that emphasizes transient cohesive strength as a function of bonding time and temperature.1.2 Use of thin adherends enables bondlines to be rapidly heated to elevated temperatures and maintained at those temperatures for a range of times at a controlled pressure before testing.1.3 Optional rapid forced air cooling of bonds after pressing and immediately before testing enables the effect of testing temperature on transient strength to be evaluated.1.4 Bond overlap distance is specified to ensure that failure occurs in the bondline rather than in unbonded portions of adherend strips, and also to minimize the effect of shear stress non-uniformity along the overlap during tensile testing.1.5 Standard wood or alternative non-standard materials must be of specified high quality and uniformity of structure and dimension to minimize variability of bonding and maximize stress transfer into the bonds during testing.1.6 The effect of wood variability and type, or of the properties of alternative non-wood materials, on bond strength development may be explored using the method.1.7 Optional hermetic sealing of bond overlaps during their heated pressing enables the effect of moisture on bonding to be evaluated.1.8 Thermal damage, either of pre-formed bonds or by prolonging bond forming times, may be evaluated as a function of time and elevated temperature using this test method.1.9 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.10 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Some specific hazards statements are given in Section 10 on Hazards.1.11 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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S408-1981 (R2001) Guidelines for the Development of Limit States Design 现行 发布日期 :  1970-01-01 实施日期 : 

This PDF includes Update #1 1. Scope 1.1 This Publication sets forth a recommended common basis for codes and standards for the design and evaluation of civil engineering structures, such as building and industrial structures, bridges, earth and wa

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5.1 A colorant sometimes fails to disperse completely in a base paint due to poor compatibility, which can be the fault of the colorant, the paint, or both. This will result in poor color development, which is readily manifested by the common procedure of applying the paint with a doctor blade and subjecting the drawdown to high shear stress by finger-rubbing a small area of the partially dry film. This tends to disperse undeveloped colorant, if any, and produces a color variation between the unsheared and sheared areas of the paint film. The variation can be measured colorimetrically to give a numerical color difference value that is a measure of the color development of the original paint, the smaller the difference the better the color development and vice versa. Color difference values obtained by finger-rubbing were found to vary widely for the same as well as among different operators. This test method establishes a controlled shear-stress procedure analogous to the finger rub-up test, but with far better reproducibility.5.2 Poor color development can be a problem in the production of paints, and in their performance in the field. In production it causes a loss of colorant monetary value, and unpredictable tinting results. In field performance it results in color variations in the applied paint film due to the varying shear forces to which the paint is subjected at different stages or by different modes of application.5.3 Although poor color development is primarily and most often related to the colorant portion of a tinted paint, the white pigment in the base paint can also be poorly developed due to flocculation or other causes. In the latter case, shear dispersion can make the paint film lighter and less colorful, rather than the reverse. Then too, the colorant and the white might both be poorly developed, and the color change due to shear stress would then be the combined effect of both.5.4 In any case, color development is an important paint property, for the measurement of which this test method is intended to provide a generally accepted and reproducible test method.1.1 This test method covers a procedure for measuring color development in tinted latex paints, for the purpose of determining the efficiency of colorants, the tintability of base paints and the potential for poor color uniformity of applied paint films.1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard. The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Composite materials consist by definition of a reinforcement phase in a matrix phase. In addition, ceramic matrix composites (CMCs) often contain measurable porosity which interacts with the reinforcement and matrix. And SiC-SiC composites often use a fiber interface coating which has an important mechanical function. The composition and structure of these different constituents in the CMC are commonly tailored for a specific application with detailed performance requirements. The tailoring involves the selection of the reinforcement fibers (composition, properties, morphology, etc.), the matrix (composition, properties, and morphology), the composite structure (component fractions, reinforcement architecture, interface coatings, porosity structure, microstructure, etc.), and the fabrication conditions (forming, assembly, forming, densification, finishing, etc.). The final engineering properties (physical, mechanical, thermal, electrical, etc.) can be tailored across a broad range with major directional anisotropy in the properties.4.2 Specifications for specific CMC components covering materials, material processing, and fabrication procedures are developed to provide a basis for fabricating reproducible and reliable structures. Designer/users/producers have to write CMC specifications for specific applications with well-defined composition, structure, properties and processing requirements. But with the extensive breadth of selection in composition, structure, and properties in CMCs, it is virtually impossible to write a "generic" CMC specification applicable to any and all CMC applications that has the same type of structure and details of the commonly-used specifications for metal alloys. This guide is written to assist the designer/user/producer in developing a comprehensive and detailed material specification for a specific CMC application/component with a specific focus on nuclear applications.4.3 The purpose of this guide is to provide guidance on how to specify the constituents, the structure, the desired engineering properties (physical, chemical, mechanical, durability, etc), methods of testing, manufacturing process requirements, the quality assurance requirements, and traceability for SiC-SiC composites for nuclear reactor applications. The resulting specification may be used for the design, production, evaluation, and qualification of SiC-SiC composites for structures in nuclear reactors.4.4 The guide is applicable to SiC-SiC composites with flat plate, rectangular bar, round rod, and round tube geometries.4.5 This guide may also be applicable to the development of specifications for SiC-SiC composites used for other structural applications, discounting the nuclear-specific chemical purity and irradiation behavior requirements.1.1 This document is a guide to preparing material specifications for silicon carbide fiber/silicon carbide matrix (SiC-SiC) composite structures (flat plates, rectangular bars, round rods, and tubes) manufactured specifically for structural components and for fuel cladding in nuclear reactor core applications. The SiC-SiC composites consist of silicon carbide fibers in a silicon carbide matrix produced by liquid infiltration/pyrolysis and/or by chemical vapor infiltration.1.2 This guide provides direction and guidance for the development of a material specification for a specific SiC-SiC composite component or product for nuclear reactor applications. The guide considers composite constituents and structure, physical and chemical properties, mechanical properties, thermal properties, performance durability, methods of testing, materials and fabrication processing, and quality assurance. The SiC-SiC composite materials considered here would be suitable for nuclear reactor core applications where neutron irradiation-induced damage and dimensional changes are significant design considerations. (1-8)21.3 The component material specification is to be developed by the designer/purchaser/user. The designer/purchaser/user shall define and specify in detail any and all application-specific requirements for design, manufacturing, performance, and quality assurance of the ceramic composite component. Additional specification items for a specific component, beyond those listed in this guide, may be required based on intended use, such as geometric tolerances, permeability, bonding, sealing, attachment, and system integration.1.4 This guide is specifically focused on SiC-SiC composite components and structures with flat plate, solid rectangular bar, solid round rod, and tubular geometries.1.5 This guide may also be applicable to the development of specifications for SiC-SiC composites used for other structural applications, discounting the nuclear-specific chemical purity and irradiation behavior factors.1.6 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The objective of this practice is to provide guidelines for the preparation of samples for use in collaborative tests, to evaluate methods during their development, and for the evaluation of the precision and bias of proposed test methods.5.2 Statements of the precision and bias are a mandatory part of ASTM test methods. Such an evaluation is necessary to provide guidance to the user as to the reliability of measurements that can be expected by its use. The statements are developed on the basis of user experience (ordinarily collaborative tests) with the test method.5.3 The availability of test samples is a key requirement for collaborative evaluation of test methods.1.1 This practice establishes uniform general procedures for the development (preparation) and use of samples in the collaborative testing of methods for chemical analysis of sediments and similar materials.1.2 The principles of this practice are applicable to aqueous samples with suitable technical modifications.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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3.1 In this guide, the planning, conduct, and completion of the independent verification, and other related details are addressed.3.2 The ITPV is intended to assist manufacturers, users, and regulating authorities in ensuring the accuracy of a reference material with a high level of confidence.1.1 This guide covers the significance and use, planning, conduct and completion of an independent third-party verification of reference materials.1.2 In this guide, independent third-party verification (ITPV) is defined as the evaluation of the conceptual and technical soundness a design or outcome being reviewed by one or more independent third party (ITPV) qualified by their education, training, and experience in the same discipline, or closely related field of science, to judge the worthiness of the design or assess the design’s likelihood of achieving the intended objectives and anticipated outcomes.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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