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AS 1463-1988 Polyethylene pipe extrusion compounds 现行 发布日期 :  1988-04-05 实施日期 : 

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1.1 This classification system covers requirements for cellulose acetate thermoplastic compounds plasticized with either diethyl phthalate or dimethyl phthalate and are suitable for injection molding and extrusion. These compounds have an acetyl content between 39 and 40 %. It does not include materials compounded for special application. Cellulosic plastic materials, being thermoplastic, are reprocessable and recyclable. This classification system allows for the use of those cellulosic materials, provided that all specific requirements of this classification system are met.1.2 The properties included in this classification system are those required to identify the compositions covered. Other requirements necessary to identify particular characteristics important to specialized applications are specified by using the suffixes as given in Section 5.1.3 This classification system and subsequent line call out (specification) are intended to provide a means of calling out plastic materials used in the fabrication of end items or parts. It is not intended for the selection of materials. Material selection can be made by those having expertise in the plastic field only after careful consideration of the design and performance required of the part, environment to which it will be exposed, fabrication process to be employed, costs involved, and inherent properties of the material other than those covered by this classification system.1.4 The values stated in SI units are to be regarded as standard.1.5 The following safety hazards caveat pertains only to the test method portion, Section 11, of this classification system. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.NOTE 1: There is no known ISO equivalent to this standard.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Manufacturers of carpet need to monitor emissions of VOCs to assess the environmental impact of their products indoors. These results are also used to demonstrate compliance with VOC emission limits for individual VOCs.5.2 These data are also used to understand which VOCs are emitted from a product or material and to measure the magnitude of those emissions.5.3 Emission data may be used to compare different lots of carpet of the same materials of construction, or carpets composed of different materials of construction, in order to develop products with lower emissions and lower potential environmental impact.5.4 This test method should be used in conjunction with practices/guidelines for emissions testing such as Guide D5116, Practice D7143, Practice D7706, ISO 16000-9, and ISO 16000-10. These detail how to select and prepare samples and how and when to carry out emissions tests such that the concentration and profile of vapors in the exhaust air of the emission chamber/cell are representative of the product under test. This test method covers the sampling and analysis of volatile organic compounds in the exhaust gas from the chamber/cell using thermal desorption—compatible sorbent tubes and will provide the necessary analytical consistency to ensure that reproducible data is obtained for the analysis of identical vapor samples by different laboratories.1.1 This test method describes an analytical procedure for identifying and quantifying the masses of individual volatile organic compounds (individual VOCs or IVOCs) that are emitted into a flow of air from carpet specimens and collected on sorbent sampling tubes during emissions testing.1.2 This test method will be used in conjunction with a standard practice for sampling and preparing carpet specimens for emissions testing. If a specific chamber practice is not available for the carpet specimens, this test method should be used in conjunction with approved standard practices for emissions testing and sample preparation.1.3 When used in conjunction with standard practices for carpet specimen preparation and collection of vapor-phase emissions , this test method will provide a standardized means of determining the levels of IVOC in the exhaust stream of the emissions test chamber/cell. If this test method is used with a reliable practice for emissions testing, these IVOC levels can be used to determine the emission rate from a unit quantity (usually surface area) of the sample material under test.1.4 VOCs in the exhaust stream of an emissions test device are collected on thermal desorption tubes packed with a specific combination of sorbents using active (pumped) sampling. (See Practice D6196 for a more general description of vapor collection using pumped sampling onto sorbent tubes.) The samples are analyzed by thermal desorption (TD) with gas chromatography and mass spectrometry detection (GC/MS) and/or flame ionization detection (FID) depending upon the requirements of the specific materials emissions testing/certification protocol.1.5 This test method can be used for the measurement of most GC-compatible organic vapors ranging from the approximate volatility from n-hexane to n-hexadecane (that is, compounds with vapor pressures ranging from 16 kPa to 4 × 10-4 kPa at 25°C). Properties other than a compound’s vapor pressure such as affinity for the sorbent may need to be taken into account. Compounds with vapor pressures outside this range may or may not be quantifiable by this test method. However, qualitative data concerning the identity of a compound(s), outside the stated volatility range for quantitation, may still be useful to the user. This test method can be applied to analytes over a wide concentration range—typically 1 μg/m3 to 1 mg/m3 concentration of vapor in the exhaust air from the emission cell or chamber.1.6 This test method is not capable of quantifying all compounds which are emitted from carpets. See the appropriate test practices/methods for determining other compounds that are not amenable to analysis by gas chromatography (that is, Test Method D5197 for the determination of aldehydes).1.7 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Purgeable organic compounds, including organohalides, have been identified as contaminants in raw and drinking water. These contaminants may be harmful to the environment and man. Dynamic headspace sampling is a generally applicable method for concentrating these components prior to gas chromatographic analysis (1-5).3 This test method can be used to quantitatively determine purgeable organic compounds in raw source water, drinking water, and treated effluent water.1.1 This test method covers the determination of most purgeable organic compounds that boil below 200°C and are less than 2 % soluble in water. It covers the low μg/L to low mg/L concentration range (see Section 15 and Appendix X1).1.2 This test method was developed for the analysis of drinking water. It is also applicable to many environmental and waste waters when validation, consisting of recovering known concentrations of compounds of interest added to representative matrices, is included.1.3 Volatile organic compounds in water at concentrations above 1000 μg/L may be determined by direct aqueous injection in accordance with Practice D2908.1.4 It is the user's responsibility to assure the validity of the test method for untested matrices.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in 8.5.5.1.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification covers the minimum requirements for bonding compounds used in adhering interior gypsum plasters to structurally sound surfaces. The bonding compound should be a tinted film-forming material suitable for application by brush, roller, and spray. It shall have a non-oxidizing, non-toxic, and non-flammable composition, and have a smooth, homogeneous, and flexible consistency with no settling of the solids. It shall also be free of foreign matter, and shall not be noticeably affected by mild acid or alkali. The apparatus needed for the preparation of the compound are moist cabinet, forced drift type oven, freezer, balance, timing device, tamper, steel straight edge, metal-bladed spatula, paint brush, briquet testing machine, briquet molds, divider, and clips. Specimens shall be sampled, tested, and conform accordingly to the following performance requirements: bonding capability; degradation; high temperature stability; freeze-thaw stability, and bond strength.1.1 This specification covers minimum requirements for bonding compounds for adhering interior gypsum plaster to structurally sound surfaces.1.2 This specification also covers test methods for determining performance requirements and physical properties.1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.4 The following safety hazards caveat pertains only to the test methods described in this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The logarithmic viscosity number provides information on the effect of compounding or processing of PVC.5.2 Exposure of PVC compositions to shear or to high temperatures can result in a change in the logarithmic viscosity number of the resin.1.1 This test method covers the determination of the logarithmic viscosity number of poly(vinyl chloride) (PVC) homopolymers after compounding or processing.1.2 It is the basic assumption of this technique that the formulation of the compounded resin is known and that any additives present can be separated from the resin by extraction with diethyl ether. This is necessary to permit adjustment of the amount of sample used in the test to give a resin concentration in cyclohexanone of 0.2 ± 0.002 g/100 mL.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in 7.3 and 8.4.1.NOTE 1: This test method and ISO 1628-2 are not equivalent.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification covers requirements for plasticized cellulose acetate butyrate thermoplastic compounds suitable for injection molding and extrusion. These compounds have a butyryl content less than 38 % and an acetyl content less than 15 % and may or may not contain dyes and pigments. This specification does not include special materials compounded for special applications. Cellulosic plastic materials, being thermoplastic, are reprocessable and recyclable. This specification allows for the use of those cellulosic materials, provided that all specific requirements of this specification are met. Test specimens of the thermoplastic compounds shall conform to the prescribed specific gravity, tensile stress at yield, flexural modulus, Izod impact strength, water absorption and weight loss on heating. The materials shall also be subject to color-visual, color-quantitative, and plasticizer content analysis.1.1 This classification system covers requirements for plasticized cellulose acetate butyrate thermoplastic compounds suitable for injection molding and extrusion. These compounds have a butyryl content less than 38 % and an acetyl content less than 15 % and can contain dyes and pigments. This classification system does not include special materials compounded for special applications. Cellulosic plastic materials, being thermoplastic, are reprocessable and recyclable. This classification system allows for the use of those cellulosic materials, provided that all specific requirements of this classification system are met.1.2 The properties included in this classification system are those required to identify the compositions covered. Other requirements necessary to identify particular characteristics important to specialized applications are specified by using the suffixes as given in Section 5.1.3 This classification system and subsequent line call out (specification) are intended to provide a means of calling out plastic materials used in the fabrication of end items or parts. It is not intended for the selection of materials. Material selection can be made by those having expertise in the plastic field only after careful consideration of the design and performance required of the part, environment to which it will be exposed, fabrication process to be employed, costs involved, and inherent properties of the material other than those covered by this classification system.1.4 The values stated in SI units are to be regarded as standard.1.5 The following safety hazards caveat pertains only to the test method portion, Section 12, of this classification system. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.NOTE 1: There is no known ISO equivalent to this standard.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Latex paints, alkyd paints, and primers are used as coatings for walls, wooden trim, and furnishings in occupied buildings. Paint may be applied to large surface areas and may be applied repeatedly during the lifetime of a building. VOCs are emitted from paint after application to surfaces.5.2 Many other types of architectural coatings may be used in large quantities indoors in buildings. In particular, many different types of coatings are used for floors including wood floor stains and finishes and concrete sealers, hardeners, and stains. Two component finishes are often mixed on site and are applied to floors and other surfaces to create a finished surface.5.3 There is a need for standardized procedures for measuring the emissions of VOCs from paint and coating samples that can be reproduced by different laboratories and that can used for the assessment of the acceptability of VOC emissions from paints and coatings that are intended for use indoors in occupied spaces. This practice describes standardized procedures that can be incorporated into test methods used for the purpose of estimating the impacts of cured paints and coatings on indoor air quality. Different procedures are required for the estimation of VOC exposures to workers applying such products.1.1 This practice describes procedures for testing the emissions of volatile organic compounds (VOCs), formaldehyde, and other carbonyl compounds, from alkyd paint, latex paint, primer, and other architectural coating samples using a small-scale environmental chamber test facility.1.2 This practice describes the requirements for the chamber test facility, the small-scale test chamber, the clean air supply system, the environmental controls, the environmental monitoring and data acquisition system, and the chamber air sampling system.1.3 This practice describes procedures for documenting the paint and coating samples and for the handling and storage of these samples including splitting of samples into smaller containers for storage and subsequent testing.1.4 This practice identifies appropriate substrates to be used for the preparation of test specimens of paints and coatings, as well as procedures for preparing substrates for use.1.5 This practice provides detailed procedures for preparing test specimens of paint and coating samples.1.6 This practice generally describes chamber test procedures and chamber air sampling procedures. The details of these procedures are dependent upon the objectives of the test.1.7 This practice does not recommend specific methods for sampling and analysis of VOCs, formaldehyde, and other carbonyl compounds. The appropriate methods are dependent upon the objectives of the test.1.8 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.9 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.10 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This practice provides a general procedure for the solvent extraction of volatile and semi-volatile organic compounds from a water matrix. Solvent extraction is used as the initial step in the solvent extraction of organic constituents for the purpose of quantifying extractable organic compounds.4.2 Typical detection limits that can be achieved using micro-extraction techniques with gas chromatography (GC) with flame ionization detector (FID), electron capture detector (ECD), or with a mass spectrometer (GC/MS) range from milligrams per litre (mg/L) to nanograms per litre (ng/L). The detection limit, linear concentration range, and sensitivity of the test method for a specific organic compound will depend upon the sample clean-up, injection volume, solvent to sample ratio, solvent concentration methods used, and the determinative technique employed.4.3 Micro-extraction has the advantage of speed, simple extraction devices, and the use of small amounts of sample and solvents.4.3.1 Selectivity can be improved by the choice of solvent (usually hexane or pentane) or mixed solvents, extraction time and temperature, and ionic strength of the solution.4.3.2 Extraction devices can vary from the sample container itself to commercial devices specifically designed for micro-extraction. See 7.1 and 7.2.4.3.3 A list of chlorinated organic compounds that can be determined by this practice includes both high and low boiling compounds or chemicals (see Table 1).(A) Based on the injection of chlorinated compounds in pentane solution, taking into consideration the 100:1 concentration of a water sample by the microextraction technique.1.1 This practice covers standard procedures for extraction of volatile and semi-volatile organic compounds from water using small volumes of solvents.1.2 The compounds of interest must have a greater solubility in the organic solvent than the water phase.1.3 Not all of the solvents that can be used in micro extraction are addressed in this practice. The applicability of a solvent to extract the compound(s) of interest must be demonstrated before use.1.4 This practice provides sample extracts suitable for any technique amenable to solvent injection such as gas chromatography or high performance liquid chromatography (HPLC).1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 91.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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