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5.1 This test method provides a method of measurement of distillation range of volatile organic liquids. The relative volatility of organic liquids can be used with other tests for identification and measurement of quality. Therefore, this test method provides a test procedure for assessing compliance with a specification.5.2 This test method also provides an empirical value of residue, solvent recovery capacity, and loss (or non-recovery) on heating. Organic liquids are used as solvents in many chemical processes. As the relative volatility, residual matter and recovery capability affect the efficiency of these processes, this test method is useful in manufacturing control.1.1 This test method covers the determination of the distillation range of liquids boiling between 30 and 350 °C, that are chemically stable during the distillation process, by manual or automatic distillation procedures.1.2 This test method is applicable to organic liquids such as hydrocarbons, oxygenated compounds, chemical intermediates, and blends thereof.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 For purposes of determining conformance of an observed or a calculated value using this test method to relevant specifications, test result(s) shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29.1.5 For hazard information and guidance, see the supplier's Material Safety Data Sheet.1.6 Warning—Mercury has been designated by EPA and many state agencies as a hazardous material that can cause central nervous system, kidney, and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable product Material Safety Data Sheet (MSDS) for details and EPA’s website (http://www.epa.gov/mercury/faq.htm) for additional information. Users should be aware that selling mercury or mercury-containing products, or both, in your state may be prohibited by state law.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in Section 7.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test method may be used for research and development. It also may be used for quality assurance, provided a standard has been agreed upon between a producer and a user.4.2 For identification purposes, melting range should be supplemented by measurements of a more specific physical and chemical property.4.3 This test method is not recommended for rubber chemicals that decompose at their melting ranges.4.4 The melting range as determined by Test Method A—Capillary Tube Melting Range is not recommended as a criterion of purity of a rubber chemical.1.1 These test methods cover the determination of the melting range of commercial rubber processing chemicals either by use of capillary melting point tubes or by differential scanning calorimetry (DSC).1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Fracture toughness is expressed in terms of an elastic-plastic stress intensity factor, KJc, that is derived from the J-integral calculated at fracture. 5.2 Ferritic steels are microscopically inhomogeneous with respect to the orientation of individual grains. Also, grain boundaries have properties distinct from those of the grains. Both contain carbides or nonmetallic inclusions that can act as nucleation sites for cleavage microcracks. The random location of such nucleation sites with respect to the position of the crack front manifests itself as variability of the associated fracture toughness (13). This results in a distribution of fracture toughness values that is amenable to characterization using the statistical methods in this test method. 5.3 The statistical methods in this test method assume that the data set represents a macroscopically homogeneous material, such that the test material has both the uniform tensile and toughness properties. The fracture toughness evaluation of nonuniform materials is not amenable to the statistical analysis procedures employed in this test method. For example, multi-pass weldments can create heat-affected and brittle zones with localized properties that are quite different from either the bulk or weld materials. Thick-section steels also often exhibit some variation in properties near the surfaces. Metallographic analysis can be used to identify possible nonuniform regions in a material. These regions can then be evaluated through mechanical testing such as hardness, microhardness, and tensile testing for comparison with the bulk material. It is also advisable to measure the toughness properties of these nonuniform regions distinctly from the bulk material. Section 10.6 provides a screening criterion to assess whether the data set may not be representative of a macroscopically homogeneous material, and therefore, may not be amenable to the statistical analysis procedures employed in this test method. If the data set fails the screening criterion in 10.6, the homogeneity of the material and its fracture toughness can be more accurately assessed using the analysis methods described in Appendix X5. 5.4 Distributions of KJc data from replicate tests can be used to predict distributions of KJc for different specimen sizes. Theoretical reasoning (9), confirmed by experimental data, suggests that a fixed Weibull slope of 4 applies to all data distributions and, as a consequence, standard deviation on data scatter can be calculated. Data distribution and specimen size effects are characterized using a Weibull function that is coupled with weakest-link statistics (14). An upper limit on constraint loss and a lower limit on test temperature are defined between which weakest-link statistics can be used. 5.5 The experimental results can be used to define a master curve that describes the shape and location of median KJc transition temperature fracture toughness for 1T specimens (15). The curve is positioned on the abscissa (temperature coordinate) by an experimentally determined reference temperature, T0. Shifts in reference temperature are a measure of transition temperature change caused, for example, by metallurgical damage mechanisms. 5.6 Tolerance bounds on KJc can be calculated based on theory and generic data. For added conservatism, an offset can be added to tolerance bounds to cover the uncertainty associated with estimating the reference temperature, T0, from a relatively small data set. From this it is possible to apply a margin adjustment to T0 in the form of a reference temperature shift. 5.7 For some materials, particularly those with low strain hardening, the value of T0 may be influenced by specimen size due to a partial loss of crack-tip constraint (5). When this occurs, the value of T0 may be lower than the value that would be obtained from a data set of KJc values derived using larger specimens. 5.8 As discussed in 1.3, there is an expected bias among T0 values as a function of the standard specimen type. The magnitude of the bias may increase inversely to the strain hardening ability of the test material at a given yield strength, as the average crack-tip constraint of the data set decreases (16). On average, T0 values obtained from C(T) specimens are higher than T0 values obtained from SE(B) specimens. Best estimate comparison indicates that the average difference between C(T) and SE(B)-derived T0 values is approximately 10 °C (2). However, individual C(T) and SE(B) datasets may show much larger T0 differences (3, 17, 18), or the SE(B) T0 values may be higher than the C(T) values (2) . On the other hand, comparisons of individual, small datasets may not necessarily reveal this average trend. Datasets which contain both C(T) and SE(B) specimens may generate T0 results which fall between the T0 values calculated using solely C(T) or SE(B) specimens. 1.1 This test method covers the determination of a reference temperature, T0, which characterizes the fracture toughness of ferritic steels that experience onset of cleavage cracking at elastic, or elastic-plastic KJc instabilities, or both. The specific types of ferritic steels (3.2.2) covered are those with yield strengths ranging from 275 MPa to 825 MPa (40 ksi to 120 ksi) and weld metals, after stress-relief annealing, that have 10 % or less strength mismatch relative to that of the base metal. 1.2 The specimens covered are fatigue precracked single-edge notched bend bars, SE(B), and standard or disk-shaped compact tension specimens, C(T) or DC(T). A range of specimen sizes with proportional dimensions is recommended. The dimension on which the proportionality is based is specimen thickness. 1.3 Median KJc values tend to vary with the specimen type at a given test temperature, presumably due to constraint differences among the allowable test specimens in 1.2. The degree of KJc variability among specimen types is analytically predicted to be a function of the material flow properties (1)2 and decreases with increasing strain hardening capacity for a given yield strength material. This KJc dependency ultimately leads to discrepancies in calculated T0 values as a function of specimen type for the same material. T0 values obtained from C(T) specimens are expected to be higher than T0 values obtained from SE(B) specimens. Best estimate comparisons of several materials indicate that the average difference between C(T) and SE(B)-derived T0 values is approximately 10°C (2). C(T) and SE(B) T0 differences up to 15 °C have also been recorded (3). However, comparisons of individual, small datasets may not necessarily reveal this average trend. Datasets which contain both C(T) and SE(B) specimens may generate T0 results which fall between the T0 values calculated using solely C(T) or SE(B) specimens. It is therefore strongly recommended that the specimen type be reported along with the derived T0 value in all reporting, analysis, and discussion of results. This recommended reporting is in addition to the requirements in 11.1.1. 1.4 Requirements are set on specimen size and the number of replicate tests that are needed to establish acceptable characterization of KJc data populations. 1.5 T0 is dependent on loading rate. T0 is evaluated for a quasi-static loading rate range with 0.1< dK/dt < 2 MPa√m/s. Slowly loaded specimens (dK/dt < 0.1 MPa√m) can be analyzed if environmental effects are known to be negligible. Provision is also made for higher loading rates (dK/dt > 2 MPa√m/s) in Annex A1. Note that this threshold loading rate for application of Annex A1 is a much lower threshold than is required in other fracture toughness test methods such as E399 and E1820. 1.6 The statistical effects of specimen size on KJc in the transition range are treated using the weakest-link theory (4) applied to a three-parameter Weibull distribution of fracture toughness values. A limit on KJc values, relative to the specimen size, is specified to ensure high constraint conditions along the crack front at fracture. For some materials, particularly those with low strain hardening, this limit may not be sufficient to ensure that a single-parameter (KJc) adequately describes the crack-front deformation state (5). 1.7 Statistical methods are employed to predict the transition toughness curve and specified tolerance bounds for 1T specimens of the material tested. The standard deviation of the data distribution is a function of Weibull slope and median KJc. The procedure for applying this information to the establishment of transition temperature shift determinations and the establishment of tolerance limits is prescribed. 1.8 The procedures described in this test method assume that the data set represents a macroscopically homogeneous material, such that the test material has uniform tensile and toughness properties. Application of this test method to an inhomogeneous material will result in an inaccurate estimate of the transition reference value T0 and nonconservative confidence bounds. For example, multi-pass weldments can create heat-affected and brittle zones with localized properties that are quite different from either the bulk or weld materials. Thick-section steels also often exhibit some variation in properties near the surfaces. Metallography and initial screening may be necessary to verify the applicability of these and similarly graded materials. Section 10.6 provides a screening criterion to assess whether the data set may not be representative of a macroscopically homogeneous material, and therefore, may not be amenable to the statistical analysis procedures employed in this test method. If the data set fails the screening criterion in 10.6, the homogeneity of the material and its fracture toughness can be more accurately assessed using the analysis methods described in Appendix X5. 1.9 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.10 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The boiling range distribution of medium and heavy petroleum distillate fractions provides an insight into the composition of feed stocks and products related to petroleum refining processes (for example, hydrocracking, hydrotreating, visbreaking, or deasphalting). The gas chromatographic simulation of this determination can be used to replace conventional distillation methods for control of refining operations. This test method can be used for product specification testing with the mutual agreement of interested parties.5.2 This test method extends the scope of boiling range determination by gas chromatography to include distillates (IBP > 100 °C) and heavy petroleum distillate fractions beyond the scope of Test Method D2887 (538 °C).5.3 Boiling range distributions obtained by this test method have not been analyzed for correlation to those obtained by low efficiency distillation, such as with Test Method D86 or D1160. This test method does not claim agreement between these physical distillations and simulated distillation. Efforts to resolve this question will continue. When successful resolutions of the questions are determined, this test method will be revised accordingly.1.1 This test method covers the determination of the boiling range distribution of petroleum products by capillary gas chromatography using flame ionization detection. This standard test method has been developed through the harmonization of two test methods, Test Method D6352 and IP 480. As both of these methods cover the same scope and include very similar operating conditions, it was agreed that a single standard method would benefit the global simulated distillation community.1.2 This test method is not applicable for the analysis of petroleum or petroleum products containing low molecular weight components (for example naphthas, reformates, gasolines, diesel). Components containing hetero atoms (for example alcohols, ethers, acids, or esters) or residue are not to be analyzed by this test method. See Test Methods D7096, D2887, or D7213 for possible applicability to analysis of these types of materials. This method is also not suitable for samples that will not elute completely from the gas chromatographic column, leaving residues. For such samples as crude oils and residues, see Test Methods D5307 and D7169.1.3 This test method is applicable to distillates with initial boiling points above 100 ºC and final boiling points below 735 ºC (carbon 110); for example, distillates (IBP > 100 °C), base oils and lubricating base stocks.1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D3132-84(1996) Standard Test Method for Solubility Range of Resins and Polymers (Withdrawn 2005) Withdrawn, No replacement 发布日期 :  1970-01-01 实施日期 : 

1.1 This test method covers determination of the solubility of resins and polymers in terms of the region of solubility parameter and hydrogen bonding of solvents in which complete solution occurs. In some cases dipole moment of the solvents may also be required to delineate more exactly the boundaries of solubility. 1.2 This test method is applicable only if the test solutions are of sufficient clarity and freedom from color to allow accurate visual judgement of complete solubility and of low enough viscosity for solution to take place. 1.3 This standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For a specific hazard statement see Note in 6.2.

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5.1 The boiling range distribution of light and medium petroleum distillate fractions provides an insight into the composition of feed stocks and products related to petroleum refining process, This gas chromatographic determination of boiling range can be used to replace conventional distillation methods for control of refining operations. This test method can be used for product specification testing with the mutual agreement of interested parties.5.2 This test method extends the scope of boiling range determination by gas chromatography to include light and medium petroleum distillate fractions beyond the scope of Test Method D2887 (538 °C) and below Test Method D6352 (700 °C).5.3 Boiling range distributions obtained by this test method are theoretically equivalent to those obtained by true boiling point (TBP) distillation (see Test Method D2892). They are not equivalent to results from low efficiency distillation such as those obtained with Test Method D86 or D1160.1.1 This test method covers the determination of the boiling range distribution of petroleum products. This test method is applicable to petroleum distillates having an initial boiling point greater than 100 °C and a final boiling point less than 615 °C at atmospheric pressure as measured by this test method.1.2 The test method is not applicable for analysis of petroleum distillates containing low molecular weight components (for example, naphthas, reformates, gasolines, crude oils). Materials containing heterogeneous components (for example, alcohols, ethers, acids or esters) or residue are not to be analyzed by this test method. See Test Methods D7096, D2887, D6352, or D7169.1.3 This test method uses the principles of simulated distillation methodology.1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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1.1 In these tables, body measurements of adult female plus women’s figure type sizes 14W–40W are listed. Although these are body measurements, they can be used as a baseline in designing apparel for plus women in this size range when considering such factors as fabric type ease for body movement, styling, and fit.1.2 These tables list body measurements for the complete range of plus women sizing.1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The boiling range distribution of petroleum distillate fractions provides an insight into the composition of feed stocks and products related to petroleum refining processes. A major advantage of the fast analysis time obtained by this test method is increasing product through put and reduced lab testing time by a minimum factor of 3. This gas chromatographic determination of boiling range may be used to replace conventional distillation methods for control of refining operations and for product specification testing with the mutual agreement of interested parties.5.2 Boiling range distributions obtained by this test method are essentially equivalent to those obtained by true boiling point (TBP) distillation (see Test Method D2892). They are not equivalent to results from low efficiency distillations such as those obtained with Test Method D86 or D1160.1.1 This test method covers the determination of the boiling range distribution of petroleum products and biodiesel formulations, B5, B10, and B20. It is applicable to petroleum distillates having a final boiling point not greater than 538 °C or lower at atmospheric pressure as measured by this test method. The difference between the initial boiling point and the final boiling point shall be greater than 55 °C.1.2 The test method is not applicable for analysis of petroleum distillates containing low molecular weight components (for example naphthas, reformates, gasolines, full range crude oils). Materials containing heterogeneous mixtures (for example, alcohols, ethers, acids or esters, except biodiesels) or residue are not to be analyzed by this test method. See Test Methods D3710, D7096, D6352, or D7169.1.3 This test method uses the principles of simulated distillation methodology. This test method uses gas chromatographic components that allow the entire analysis from sample to sample to occur in 5 min or less. In these instruments the column is heated directly at rates 10 to 15 times that of a conventional gas chromatograph and thus the analysis time is reduced from sample to sample.1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4.1 Exception—Appendix X1 includes temperatures in Fahrenheit for information only.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method provides an accurate and reliable procedure to measure the total heating value of a fuel gas, on a continuous basis, which is used for regulatory compliance, custody transfer, and process control.5.2 Some instruments which conform to the requirements set forth in this test method can have response times on the order of 1 min or less and can be used for on-line measurement and control.5.3 The method is sensitive to the presence of oxygen and nonparaffin fuels. For components not listed and composition ranges that fall outside those in Table 1 and Table 2, modifications in the method and changes to the calibration gas or gasses being used may be required to obtain correct results.1.1 This test method covers the determination of the heating value of natural gases and similar gaseous mixtures within the range of composition shown in Table 1, and Table 2 that covers flare components but is not intended to limit the components to be measured in flare gases.1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification describes a medium access control (MAC) and physical layer (PHY) specification for wireless connectivity using dedicated short-range communications (DSRC) services. This standard is based on and refers to IEEE Standards 802.11, Wireless LAN Medium Access Control and Physical Layer Specifications, and 802.11a, Wireless LAN Medium Access Control and Physical Layer Specifications High-Speed Physical Layer in the 5 GHz Band, with permission from the IEEE society. This specification is meant to be an extension of IEEE 802.11 technology into the high-speed vehicle environment. The difference between IEEE 802.11 and IEEE 802.11a operating parameters required to implement a mostly high-speed data transfer service in the 5.9-GHz Intelligent Transportation Systems Radio Service (ITS-RS) Band is explained. Potential operations within the Unlicensed National Information Infrastructure (UNII) Band are also addressed, as appropriate.1.1 This specification2 describes a medium access control (MAC) and physical layer (PHY) specification for wireless connectivity using dedicated short-range communications (DSRC) services. This standard is based on and refers to IEEE Standards 802.11, “Wireless LAN Medium Access Control and Physical Layer Specifications,” and 802.11a, “Wireless LAN Medium Access Control and Physical Layer Specifications High-Speed Physical Layer in the 5 GHz Band,” with permission from the IEEE Society. This specification is meant to be an extension of IEEE 802.11 technology into the high-speed vehicle environment. As presented here, this specification contains just enough information to explain the difference between IEEE 802.11 and IEEE 802.11a operating parameters required to implement a mostly high-speed data transfer service in the 5.9-GHz Intelligent Transportation Systems Radio Service (ITS-RS) band. Potential operations within the Unlicensed National Information Infrastructure (UNII) band are also addressed, as appropriate.1.2 Purpose—The purpose of this specification is to provide wireless communications over short distances between information sources and transactions stations on the roadside and mobile radio units, between mobile units, and between portable units and mobile units. The communications generally occur over line-of-sight distances of less than 1000 m between roadside units and mostly high-speed, but occasionally stopped and slow-moving, vehicles or between high-speed vehicles. This specification also offers regulatory bodies a means of standardizing access to the 5.9-GHz frequency band for the purpose of interoperable communications to and between vehicles at line-of-sight distances on the roadway.1.3 Specifically, this specification accomplishes the following:1.3.1 Describes the functions and services required by a DSRC and IEEE 802.11-compliant device to operate in a high-speed mobile environment.1.3.2 Refers to IEEE 802.11 MAC procedures.1.3.3 Defines the 5.9-GHz DSRC signaling technique and interface functions that are controlled by the IEEE 802.11 MAC.1.3.4 Permits the operation of a DSRC-conformant device within a DSRC communications zone that may coexist with multiple overlapping DSRC communication zones.1.3.5 Describes the requirements and procedures to provide privacy of user information being transferred over the wireless medium and authentication of the DSRC or IEEE 802.11-conformant devices.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 The use of the body measurement information in Tables 1 and 2 will assist manufacturers in developing patterns and garments that are consistent with the current anthropometric characteristics of the population of interest. This practice should, in turn, reduce or minimize consumer confusion and dissatisfaction related to apparel sizing. (Also refer to ISO 3635.)4.2 Three-dimensional avatars depicting each of the big men sizes on certain measurements were created by Alvanon, Inc. and included in these tables to assist manufacturers in visualizing the posture, shape, and proportions generated by the measurements charts in Figs. 1-3.FIG. 1 Mature Big MenFIG. 2 Mature Big MenFIG. 3 Mature Big Men1.1 These tables list body measurements of mature big men figure type sizes 46–64. Although these are body measurements, they can be used as a baseline in designing apparel for big men in this size range when considering such factors as fabric type ease for body movement, styling, and fit.1.2 These tables list body measurements for the complete range of big men sizing.1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The boiling range distribution of light and medium petroleum distillate fractions provides an insight into the composition of feed stocks and products related to petroleum refining processes. This gas chromatographic determination of boiling range can be used to replace conventional distillation methods for control of refining operations. This test method can be used for product specification testing with the mutual agreement of interested parties.5.2 This test method extends the scope of Test Method D2887 (538 °C) boiling range determination by gas chromatography to include sulfur boiling range distribution in the petroleum distillate fractions. Knowledge of the amount of sulfur and its distribution in hydrocarbons is economically important in determining product value and in determining how best to process or refine intermediate products. Sulfur compounds are known to affect numerous properties of petroleum and petrochemical products. The corrosion of metals and poisoning of catalysts is of particular concern. In addition, the content of sulfur in various refined products may be subject to governmental regulations. Test Methods, such as, D2622, D3120, D5504 and D5623, are available to determine total sulfur content or content of individual sulfur compounds in petroleum and petroleum products. Test Methods, such as, D86, D1160, D2887, D3710, and D2892, are also available to determine the hydrocarbon boiling ranges of such samples. The gas chromatographic determination of the sulfur boiling range assists in process development, in treatment and control of refining operations and is useful for assessing product quality. This determination produces detailed information about the sulfur distribution in a sample that cannot be obtained by either total sulfur analysis or analysis of sulfur in discreet distillation cuts.5.2.1 The hydrocarbon boiling range distributions obtained by Test Method D2887 are theoretically equivalent to those obtained by true boiling point (TBP) distillation (see Test Method D2892). They are not equivalent to results from low efficiency distillation such as those obtained with Test Method D86 or D1160.1.1 This test method covers the determination of the boiling range distribution of petroleum products. The test method is applicable to petroleum products and fractions having a final boiling point of 538 °C (1000 °F) or lower at atmospheric pressure as measured by this test method. This test method is limited to samples having a boiling range greater than 55 °C (100 °F), and having a vapor pressure sufficiently low to permit sampling at ambient temperature.1.1.1 The applicable sulfur concentration range will vary to some extent depending on the boiling point distribution of the sample and the instrumentation used; however, in most cases, the test method is applicable to samples containing levels of sulfur above 10 mg/kg.1.2 This test method requires the use of both FID and SCD for detection. The hydrocarbon simulated distillation data obtained from the FID signal should be performed according to Test Method D2887 Procedure B.1.3 The test method is not applicable for analysis of petroleum distillates containing low molecular weight components (for example, naphthas, reformates, gasolines, crude oils). Materials containing heterogeneous components (for example, alcohols, ethers, acids, or esters) or residue are not to be analyzed by this test method. See Test Methods D3710, D7096, D5307, D7169, or D7500.1.4 This test method does not purport to identify all sulfur species in a sample. The detector response to sulfur is equimolar for all sulfur compounds within the scope (1.1) of this test method. Thus, unidentified sulfur compounds are determined with equal precision to that of identified substances. Total sulfur content is determined from the total area of the sulfur detector.1.4.1 This test method uses the principles of simulated distillation methodology.1.5 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价: 646元 / 折扣价: 550 加购物车

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5.1 Cooking can be one of the most polluting activities commonly and regularly occurring in residential environments. Capturing airborne cooking contaminants before they can mix with the indoor air is a critical indoor air quality control method.5.2 Range hoods are used in homes to remove cooking-generated contaminants above cooking surfaces before they mix with air in the rest of the house. This test method is used to measure the capture efficiency under specific conditions that permit comparisons and ratings of range hoods.5.3 Range hoods may be manufactured and intended to operate at different flow rates or using different inserts such as filters. This test method may be used to determine capture efficiency over the range of rated air flows and operating configurations of a range hood. The rated air flows shall be listed and shall be tested in accordance with HVI Test Procedure 916, IEC 61591, ASHRAE 51/AMCA 210, or equivalent. The maximum air flow allowed for this test method is 200 L/s.1.1 This test method measures the capture efficiency of wall-mounted domestic range hoods under controlled conditions in a test chamber.1.2 This test method applies to range hoods that exhaust air to outside and does not apply to recirculating range hoods.1.3 This test method only applies to range hood air flows up to 200 L/s and widths up to 0.91 m (36 in.).1.4 This test method is intended to quantify the capture efficiency of range hoods under controlled laboratory conditions suitable for rating.1.5 The values stated in SI units are to be regarded as standard. If a value for measurement is followed by a value in other units in parentheses, the second value may be approximate. The first stated value is the requirement.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价: 590元 / 折扣价: 502 加购物车

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Safe operation of the unmanned aircraft is of the primary importance to the unmanned aircraft industry and for successful integration of unmanned aircraft with manned aircraft in civil airspace. Operators and pilots-in-command of unmanned aircraft systems shall comply with applicable Federal Aviation Regulations (14 CFR Part 43, 14 CFR Part 71, 14 CFR Part 73, 14 CFR Part 91, 14 CFR Part 93, and 14 CFR Part 99). This standard includes the minimum additional methods that should be followed by unmanned aircraft system operators, including pilots-in-command, on every visual range flight to ensure the safe operation of the aircraft and safety of people and property in the air and on the ground. This visual range flight operation standard shall be used in conjunction with appropriate unmanned aircraft system airworthiness and pilot qualification standards.1.1 This practice prescribes guidelines that govern the visual flight operation of unmanned aircraft systems in civil airspace in order to provide for the safe integration of unmanned aircraft flight operations with manned aircraft flight operations.1.2 This practice applies to those operations conducted for civil purposes other than sport or recreation that remain within the visual range of the pilot in command (see Terminology F 2395 for a definition of "visual range").1.3 This practice complies with the known rules, regulations, and public law available at the time of its publication. Should any conflict with a rule, regulation, or public law arise, the user must comply with rule and should notify ASTM of the conflict.This practice only prescribes accepted methods for visual range flight operation of unmanned aircraft systems.This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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