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5.1 This guide is intended for the developers or sponsors of new aviation gasolines or additives to describe the data requirements necessary to support the development of specifications for these new products by ASTM members. The ultimate goal of the data generated in accordance with this guide is to provide an understanding of the performance of the new fuel or additive within the property constraints and compositional bounds of the proposed specification criteria.5.2 This guide is not an approval process. It is intended to describe test and analysis requirements necessary to generate data to support specification development. This guide does not address the approval process for ASTM International standards.5.3 This guide will reduce the uncertainty and risk to developers or sponsors of new aviation gasolines or additives by describing the test and analysis requirements necessary to proceed with the development of an ASTM International specification for aviation gasoline or specification revision for an aviation gasoline additive. There are certain sections within this guide that do not specify an exact number of data points required. For example, 6.2.4.3 requires viscosity to be measured from freezing point to room temperature; 6.2.4.4, 6.2.4.5, and 6.3.2.3 require measurements over the operating temperature range; 6.3.2.4 and 6.3.2.5 require measurements versus temperature. In these cases, the developers or sponsors of new aviation gasolines or additives should attempt to generate data close to the upper and lower boundaries indicated. If no boundary is specified (for example, generate data versus temperature), then data at the widest practical test limits should be generated. A minimum of three data points is required in all cases (for example, upper, middle, lower), while five or more data points are preferred.5.4 This guide does not purport to specify an all-inclusive listing of test and analysis requirements to achieve ASTM International approval of a specification or specification revision. The final requirements will be dependent upon the specific formulation and performance of the candidate fuel and be determined by the ASTM International task forces and committees charged with overseeing the specification development.5.5 This guide is intended to describe data to be used to make a determination of the suitability of the proposed fuel or additive for use in existing or future aircraft and engines, but not necessarily for use in all existing or future aircraft and engines.5.6 This guide does not describe data requirements of other approving authorities, such as national aviation regulatory authorities, or of other organizations or industry associations. However, the data generated in the conduct of the procedure may be useful for other purposes or other organizations.5.7 Over 200 000 piston-engine aircraft rely on Specification D910 lead-containing aviation gasoline (avgas) for safe operation. There has been an increase in the research and development of alternatives to Specification D910 gasolines as a result of environmental and economic concerns.1.1 This guide provides procedures to develop data for use in research reports for new aviation gasolines or new aviation gasoline additives.1.2 This data is intended to be used by the ASTM subcommittee to make a determination of the suitability of the fuel for use as an aviation fuel in either a fleet-wide or limited capacity, and to make a determination that the proposed properties and criteria in the associated standard specification provide the necessary controls to ensure this fuel maintains this suitability during high-volume production.1.3 These research reports are intended to support the development and issuance of new specifications or specification revisions for these products. Guidance to develop ASTM International standard specifications for aviation gasoline is provided in Subcommittee J on Aviation Fuels Operating Procedures, Annex A6, “Guidelines for the Development and Acceptance of a New Aviation Fuel Specification for Spark-Ignition Reciprocating Engines.”1.4 The procedures, tests, selection of materials, engines, and aircraft detailed in this guide are based on industry expertise to give appropriate data for review. Because of the diversity of aviation hardware and potential variation in fuel/additive formulations, not every aspect may be encompassed and further work may be required. Therefore, additional data beyond that described in this guide may be requested by the ASTM task force, Subcommittee J, or Committee D02 upon review of the specific composition, performance, or other characteristics of the candidate fuel or additive.1.5 While it is beyond the scope of this guide, investigation of the future health and environmental impacts of the new aviation gasoline or new aviation gasoline additive and the requirements of environmental agencies is recommended.1.6 The values stated in SI units are to be regarded as standard.1.6.1 Exception—Some industry standard methodologies utilize imperial units as their primary system (permeability; Table A2.2).1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Nuclear grade graphite is a composite material made from petroleum or a coal-tar-based coke and a pitch binder. Manufacturing graphite is an iterative process of baking and pitch impregnation of a formed billet prior to final graphitization, which occurs at temperatures greater than 2500 °C. The impregnation and rebake step is repeated several times until the desired product density is obtained. Integral to this process is the use of isotropic cokes and a forming process (that is, isostatically molded, vibrationally molded, or extruded) that is intended to obtain an isotropic or near isotropic material. However, the source, size, and blend of the starting materials as well as the forming process of the green billet will impart unique material properties as well as variations within the final product. There will be density variations from the billet surface inward and different physical properties with and transverse to the grain direction. Material variations are expected within individual billets as well as billet-to-billet and lot-to-lot. Other manufacturing defects of interest include large pores, inclusions, and cracks. In addition to the material variation inherent to the manufacturing process, graphite will experience changes in volume, mechanical strength, and thermal properties while in service in a nuclear reactor along with the possibility of cracking due to stress and oxidation resulting from constituents in the gas coolant or oxygen ingress. Therefore, there is the recognized need to be able to nondestructively characterize a variety of material attributes such as uniformity, isotropy, and porosity distributions as a means to assure consistent stock material. This need also includes the ability to detect isolated defects such as cracks, large pores and inclusions, or distributed material damage such as material loss due to oxidation. The use of this guide is to acquire a basic understanding of the unique attributes of nuclear grade graphite and its application that either permits or hinders the use of conventional eddy current, ultrasonic, or X-ray inspection technologies.1.1 This guide provides general tutorial information regarding the application of conventional nondestructive evaluation technologies (NDE) to nuclear grade graphite. An introduction will be provided to the characteristics of graphite that defines the inspection technologies that can be applied and the limitations imposed by the microstructure. This guide does not provide specific techniques or acceptance criteria for end-user examinations but is intended to provide information that will assist in identifying and developing suitable approaches.1.2 The values stated in SI units are to be regarded as the standard.1.2.1 Exception—Alternative units provided in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method provides quick and accurate ratings for the sensory heat in low heat chilies ranging from 200 to 2500 Scoville heat units.5.2 Sensory results from this test method correlate highly (r2 = 0.94) with results from high-pressure liquid chromatography; making the two methods substitutable.61.1 This test method describes standardized procedures for the sensory evaluation of heat in low heat chili peppers ranging from 200 to 2500 Scoville heat units.1.2 This test method is intended as an alternative to the Scoville heat test (see ASTA Method 21.0 and ISO 3513), but results can be expressed in Scoville heat units (S.H.U.).1.3 This test method does not apply for ground red pepper or oleoresin capsicums.1.4 The values stated in SI units are to be regarded as the standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 8.

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5.1 Field, in-place repetitive static plate load tests are used for the evaluation and design of pavement structures. Repetitive static plate load tests are performed on soils and unbound base and subbase materials to determine strain modulus or a measure of the shear strength of pavement components.1.1 This test method covers the apparatus and procedure for making repetitive static plate load tests on subgrade soils and compacted pavement components, in either the compacted condition or the natural state, and is to provide data for use in the evaluation and design of rigid and flexible-type airport and highway pavements.1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method assesses the performance of an engine oil with respect to control of piston deposits and maintenance of oil consumption under heavy-duty operating conditions selected to accelerate deposit formation in a turbocharged, intercooled four-stroke-cycle diesel engine equipped with a combustion system that minimizes federally controlled exhaust gas emissions.5.2 The results from this test method may be compared against specification requirements to ascertain acceptance.5.3 The design of the test engine used in this test method is representative of many, but not all, diesel engines. This factor, along with the accelerated operating conditions, needs to be considered when comparing test results against specification requirements.1.1 The test method covers a heavy-duty engine test procedure under high output conditions to evaluate engine oil performance with regard to piston deposit formation, piston ring sticking and oil consumption control in a combustion environment designed to minimize exhaust emissions. This test method is commonly referred to as the Caterpillar C13 Heavy-Duty Engine Oil Test.31.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.2.1 Exceptions—Where there are no SI equivalent such as screw threads, National Pipe Treads (NPT), and tubing sizes.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. See Annex A1 for general safety precautions.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method provides quick and accurate ratings for the sensory heat in oleoresin capsicums ranging from 100 000 to 1 000 000 Scoville heat units.5.2 Sensory results from this test method correlate highly (r2 = 0.94) with results from high pressure liquid chromatography; making the two methods substitutable.61.1 This test method describes standardized procedures for the sensory evaluation of heat in oleoresin capsicums ranging from 100 000 to 1 000 000 Scoville heat units (S.H.U.).1.2 This test method is intended as an alternative to the Scoville heat test, but results can be expressed in Scoville heat units (see ASTA Method 21.0 and ISO 3513).1.3 This test method does not apply for ground red pepper, low heat chili peppers, or chili powder.1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 8.

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5.1 Results from this accelerated corrosion test shall not be considered as an indicator of the useful life of the metal equipment. Many factors need consideration for applicability to specific circumstances. Refer to Guide C1696 and Practice G31 for additional information.5.2 Corrosion associated with insulation is an important concern for insulation manufacturers, specification writers, designers, contractors, users and operators of the equipment. Some material specifications contain test methods (or reference test methods contained in other material specifications), for use in evaluating the insulation with regard to the corrosion of steel, copper, and aluminum. In some cases these tests are not applicable or effective and have not been evaluated for precision and bias.5.3 A properly selected, installed, and maintained insulation system will reduce the corrosion that often occurs on an un-insulated structure. However, when the protective weather-resistant covering of an insulation system fails, the conditions for the aqueous environment necessary for corrosion under insulation (CUI) often develop. It is possible the insulation contains, collects, or concentrates corrosive agents, or a combination thereof, often found in industrial and coastal environments. If water is not present, these electrolytes cannot migrate to the metal surface. The electrochemical reaction resulting in the aqueous corrosion of metal surfaces cannot take place in the absence of water and electrolytes. Additional environmental factors contributing to increased corrosion rates are oxygen, and elevated-temperature (near boiling point).5.4 Chlorides and other corrosive ions are common to many environments. The primary corrosion preventative is to protect insulation and metal from contamination and moisture. Insulation covers, jackets, and metal coating of various kinds are often used to prevent water infiltration and contact with the metal.5.5 This procedure can be used to evaluate all types of thermal insulation and fireproofing materials (industrial, commercial, residential, cryogenic, fire-resistive, insulating cement) manufactured using inorganic or organic materials, faced or unfaced, for which a filtered extraction solution can be obtained.5.6 This procedure can be used with all metal types for which a coupon can be prepared such as mild steel, stainless steel, copper, or aluminum. Other metals (copper, aluminum) will need different times, reference solutions and cleaning practices. It shall not be interpreted that the steel procedures work for everything. When procedures are developed for other metals they will be balloted for inclusion in the document.5.7 This procedure can also be applicable to insulation accessories including jacketing, covers, adhesives, cements, and binders associated with insulation and insulation products.5.8 Heat treatment of the insulation (as recommended by the manufacturer up to the maximum potential exposure temperature) can be used to simulate possible conditions of use.5.9 Adhesives can be tested by first drying followed by water extraction or by applying a known quantity of the test adhesive to a test piece of insulation and then extracting.5.10 Insulating cements can be tested by casting a slab, drying, and extracting or by using the uncured insulating cement powder for extraction.5.11 Reference tests prepared with various concentrations of solutions that are conducive to the corrosion of the tested metal serve as comparative criteria. Solutions containing chloride, sodium hydroxide, various acids (sulfuric, hydrochloric, nitric, and citric acid), as well as “blank” tests using only de-ionized water and tap water are used.5.12 Research can be done on insulation that has been specially formulated to inhibit corrosion in the presence of corrosive ions through modifications in basic composition or incorporation of certain chemical additives. Corrosive ions can also be added to the insulation extraction solutions to determine the effectiveness of any inhibitors present.5.13 Protective surface treatments and coatings of different types and thickness can be applied to the metal coupons and compared using various corrosive liquids.5.14 Several sets of tests are recommended because of the number of factors that affect corrosion. An average of the tests and the standard deviation between the test results are used on the data. Much of the corrosion literature recommends a minimum of three specimens for every test. Consult Guide G16 for additional statistical methods to apply to the corrosion data.1.1 This practice covers procedures for a quantitative accelerated laboratory evaluation of the influence of extraction solutions containing ions leached from thermal insulation on the aqueous corrosion of metals. The primary intent of the practice is for use with thermal insulation and associated materials that contribute to, or alternatively inhibit, the aqueous corrosion of different types and grades of metals due to soluble ions that are leached by water from within the insulation. The quantitative evaluation criteria are Mass Loss Corrosion Rate (MLCR) expressed in mils per year determined from the weight loss due to corrosion of exposed metal coupons after they are cleaned.1.2 This practice cannot cover all possible field conditions that contribute to aqueous corrosion. The intent is to provide an accelerated means to obtain a non-subjective numeric value for judging the potential contribution to the corrosion of metals that can come from ions contained in thermal insulation materials or other experimental solutions. The calculated numeric value is the mass loss corrosion rate. This calculation is based on general corrosion spread equally over the test duration and the exposed area of the experimental cells created for the test. Corrosion found in field situations and this accelerated test also involves pitting and edge effects and the rate changes over time.1.3 The insulation extraction solutions prepared for use in the test can be altered by the addition of corrosive ions to the solutions to simulate contamination from an external source. Ions expected to provide corrosion inhibition can be added to investigate their inhibitory effect.1.4 Prepared laboratory ionic solutions are used as reference solutions and controls, to provide a means of calibration and comparison.21.5 Other liquids can be tested for their potential corrosiveness including cooling tower water, boiler feed, and chemical stocks. Added chemical inhibitors or protective coatings applied to the metal can also be evaluated using the general guidelines of the practice.1.6 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Field, in-place nonrepetitive static plate load tests are used for the evaluation and design of pavement structures. Nonrepetitive static plate load tests are performed on soils and unbound base and subbase materials to determine the modulus of subgrade reaction or a measure of the shear strength of pavement components.1.1 This test method covers the apparatus and procedure for making nonrepetitive static plate load tests on subgrade soils and compacted pavement components, in either the compacted condition or the natural state, and is to provide data for use in the evaluation and design of rigid and flexible-type airport and highway pavements.1.2 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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3.1 A number of laboratory procedures are used to evaluate the effectiveness of fire-retardant and fire-resistant treatments and coatings. In general, these methods measure the three stages of fire development: (1) ignition; (2) flame spread (rate of growth of the fire); and (3) conflagration extent. While all three are of extreme importance, flame spread has been recognized as the main factor associated with testing fire-retardant coatings.3.2 Flame spread ratings based upon Test Method E84 have acquired common acceptance by regulatory agencies, but such large-scale tests are seldom practical during the development or modification of a fire-retardant coating.3.3 This test method provides the relative flame spread of experimental coatings using small test specimens under the conditions established in the 2-foot tunnel. By experimentally calibrating the 2-foot tunnel with similar Test Method E84-rated fire-retardant paint, results obtained by this test method can be used to screen coatings for suitability for testing in the Test Method E84 tunnel.3.3.1 This test method is intended as an experimental tool in evaluating experimental coatings for further development. No direct correlation of results from this test method and the Test Method E84 tunnel have been made or are implied.3.3.2 The results obtained by this test method do not in themselves act as an accurate predictor of performance in Test Method E84 and shall not be used for the purpose of certification to any class of flame spread performance.1.1 This test method determines the protection a coating affords its substrate, and the comparative burning characteristics of coatings by evaluating the flame spread over the surface when ignited under controlled conditions in a small tunnel. This establishes a basis for comparing surface-burning characteristics of different coatings without specific consideration of all the end-use parameters that might affect surface-burning characteristics under actual fire conditions.1.2 In addition to the experimental flame spread rate, the weight of panel consumed, time of afterflaming and afterglow, char dimensions and index, and height of intumescence can be measured in this test. However, a relationship should not be presumed among these measurements.1.3 This standard is used to determine certain fire-test responses of materials, products, or assemblies to heat and flame under controlled conditions by using results obtained from fire-test response standards. The results obtained from using this standard do not by themselves constitute measures of fire hazard or fire risk.1.4 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.5 This standard is used to measure and describe the response of materials, products, or assemblies to heat and flame under controlled conditions, but does not by itself incorporate all factors required for fire hazard or fire risk assessment of the materials, products, or assemblies under actual fire conditions.1.6  Fire testing is inherently hazardous. Adequate safeguards for personnel and property shall be employed in conducting these tests.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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