This specification covers the classification, testing, and requirements of polyphthalamide (PPA) materials, both virgin and recycled, suitable for injection molding. This specification is intended to be a means of calling out plastics materials used in the fabrication of end items or parts, and not for the selection of materials. The materials are classified into groups according to crystallinity, and are further subdivided into classes and grades as specified. Materials shall be sampled, prepared, and conditioned appropriately for testing, for which specimens shall conform to specified values of the following requirements: inherent viscosity; melting temperature; glass transition; tensile strength; flexural strength and modulus; Izod impact strength; deflection temperature; and moisture.1.1 This classification system covers polyphthalamide (PPA) materials suitable for injection molding.1.2 The properties included in this classification system are those required to identify the compositions covered. Other requirements necessary to identify particular characteristics important to specialized applications are to be specified by using suffixes as given in Section 5.1.3 This classification system allows for the use of recycled materials provided that all specification requirements are met.1.4 This classification system is intended to be a means of calling out plastics materials used in the fabrication of end items or parts. It is not intended for the selection of materials. Material selection can be made by those having expertise in the plastics field only after careful consideration of the design and the performance required of the part, the environment to which it will be exposed, the fabrication process to be employed, the costs involved, and the inherent properties of the material other than those covered by this classification system.1.5 The values stated in SI units are to be regarded as the standard (see IEEE/ASTM SI-10). The values given in parentheses are for information only.1.6 The following precautionary caveat pertains only to the test methods portion, Section 11, of this classification system: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in 11.7.1.NOTE 1: There is no known ISO equivalent to this standard. ISO 16396-1/-2 for polyamides may also be used to describe and classify these PPA materials, but the technical content is significantly different.NOTE 2: ASTM Standard D6779 on polyamide materials also includes PPA materials in its coverage of various polyamide chemistries. This standard gives additional information for classification and specification for PPA compositions classified as Group 10 (PA6T/66), Group 12 (PA6T/6I/66) and Group 13 (PA6T/6I) in ASTM Standard D6779 and includes provisions for other PPA compositions to utilize the classification presented.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价： 590元 / 折扣价： 502 元 加购物车

4.1 With the need to calculate volatile organic content (VOC) of paints, and with acetone, p-chlorobenzotrifluoride, methyl acetate and t-butyl acetate4 considered as exempt volatile compounds, it is necessary to know the content of these analytes. This gas chromatographic test method provides a relatively simple and direct way to determine their content. However, because the detectors used in this test method are not selective, and because some coatings are very complex mixtures, compounds may be present in the sample that coelute with the analyte, giving a result that is erroneously high. Or a component may elute with the internal standard, giving a result that is erroneously low. It is therefore important to know the composition of the sample to ensure that there are no interferences, under the analysis conditions used. Test Method D6438 employs mass-spectral detection of analytes and may be used as an alternative method.1.1 This test method is for the determination of the total-concentration of acetone, p-chlorobenzotrifluoride, methyl acetate, or t-butyl acetate, or combination of any of the four, in solvent-reducible and water-reducible paints, coatings, resins, and raw materials. Because unknown compounds that co-elute with the analyte being measured or with the internal standard, will lead to erroneous results, this test method should only be used for materials of known composition so that the possibility of interferences can be eliminated. The established working range of this test method is from 1 % to 100 % for each analyte by weight.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价： 590元 / 折扣价： 502 元 加购物车

This specification covers the requirements and test methods for the material, dimensions, workmanship, and properties of extruded, compression molded, and injection molded acetal shapes such as sheet, plate, rod, and tubular bar. The specimens shall be a pure polyoxymethylene or may filled, lubricated, or reinforced with carbon and graphite fiber, glass, PTFE, graphite, silicone, molybdenum disulfide, mineral, combinations of reinforcements or fillers, or both. The products shall conform to the physical property requirements which include tensile strength, elongation at break, tensile modulus, dimensional stability, flexural modulus, Izod impact, and porosity level. Thickness tolerance, length camber, and width bow properties shall also comply with the dimensional requirements of the different acetal shapes.1.1 This specification covers requirements and test methods for the material, dimensions, and workmanship, and the properties of extruded, compression molded and injection molded polyoxymethylene (POM) sheet, plate, rod, and tubular bar shapes, excluding pipe and fittings.1.2 The properties included in this specification are those required for the compositions covered. Section 4 presents a classification system for defining requirements for particular characteristics important to specialized applications.1.3 This specification allows for the use of recycled plastics.1.4 The values stated in inch-pound units are to be regarded as the standard in all property and dimensional tables. For reference purposes, SI units are included in Table S-POM and Table 1 only.1.5 The following precautionary caveat pertains only to the test method portions, Section 11, of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.NOTE 1: There is no known ISO equivalent to this standard.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价： 590元 / 折扣价： 502 元 加购物车

1.1 This test method can be used to determine small amounts of residual vinyl chloride monomer (VCM) in poly(vinyl chloride) (PVC) resins. It may be possible to use it for other resins or compounds containing vinyl chloride provided there are no other volatile components present with the same retention time as vinyl chloride monomer. 1.2 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For a specific hazard statement, see Section 9.

定价： 0元 / 折扣价： 0 元

4.1 This practice is to be used to help assess the biocompatibility of materials used in medical devices. It is an acute toxicological test designed to evaluate any irritation caused by device materials by gross assessment.4.2 This practice may not be appropriate for all types of implant applications. The user is cautioned to consider the appropriateness of this practice in view of the materials being tested, their potential applications, and the recommendations contained in Practice F748.NOTE 1: Some materials (e.g., absorbables) may result in an extract pH (e.g., ≤2.0 or ≥11.5) that cannot be used with this practice.4.3 The only applicable limitation is the extract preparation. Refer to Section 4.3 of Practice F619 for a description of this limitation.1.1 This practice is an intracutaneous reactivity test used to assess the potential of the material under test to produce irritation following intradermal injections of extracts of the material.1.2 The liquids injected into the rabbits are those obtained by Practice F619 where the extraction vehicles are saline, vegetable oil, or other liquids simulating human body fluids.1.3 This practice is one of several developed for the assessment of the biocompatibility of materials. Practice F748 may provide guidance for the selection of appropriate methods for testing materials for a specific application.1.4 The values stated in SI units, including units officially accepted for use with the SI, are to be regarded as standard. No other systems of measurement are included in this standard.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价： 515元 / 折扣价： 438 元 加购物车

This specification covers polypropylene materials suitable for injection molding and extrusion. Polymers consist of polypropylene homopolymers, polypropylene copolymers, and polypropylene-elastomer compounds produced with or without the addition of impact modifiers (ethylene-propylene rubber, polyisobutylene rubber, and butyl rubber, and so forth), colorants, stabilizers, lubricants, fillers, or reinforcements. Unreinforced polypropylene materials are classified into groups in accordance with basic composition. These groups are subdivided into classes and grades. The plastic composition shall be uniform and shall conform to the requirements specified. Tests shall be performed to determine the properties of the material in accordance with the following test methods: flow rate; tensile strength; flexural modulus; Charpy impact resistance; falling mass impact resistance; temperature of deflection under load; and multiaxial impact ductile-brittle transition temperature.1.1 This specification covers polypropylene materials suitable for injection molding and extrusion. Polymers consist of polypropylene homopolymers, polypropylene copolymers, and polypropylene-elastomer compounds produced with or without the addition of impact modifiers (ethylene-propylene rubber, polyisobutylene rubber, and butyl rubber, and so forth), colorants, stabilizers, lubricants, fillers, or reinforcements.1.2 This specification allows for the use of those polypropylene materials that can be recycled, reconstituted, and reground, provided that the following conditions are met:1.2.1 The requirements as stated in this specification and other ISO guidelines pertaining to these types of materials are met, and1.2.2 The material has not been modified in any way to alter its conformance to food contact regulations or similar requirements.1.3 The proportions of recycled, reconstituted, and regrind material used, as well as the nature and the amount of any contaminant, cannot be practically covered in this specification. It is the responsibility of the supplier and buyer of recycled, reconstituted, and regrind materials to ensure compliance.1.4 The properties included in this classification system are those required to identify the compositions covered. Other requirements necessary to identify particular characteristics important to specialized applications can be specified by using the suffixes as given in Section 5 and those in Classification System D4000.1.5 This classification system and specification are intended to provide a means of calling out polypropylene materials used in the fabrication of end items or parts. It is not intended for the selection of materials. Material selection can be made by those having expertise in the plastic field only after careful consideration of the design and the performance required of the part, the environment to which it will be exposed, the fabrication process to be employed, the costs involved, and the inherent properties of the material other than those covered by this specification.1.6 The values stated in SI units are to be regarded as the standard.1.7 The following precautionary caveat pertains only to the test methods portion, Section 13, of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.NOTE 1: This specification is similar to both ISO 1873-1 and ISO 1873-2, but to different degrees. This specification resembles ISO 1873-1 in title only. The content is significantly different. This specification and ISO 1873-2 differ in approach or detail; data obtained using either are technically equivalent.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价： 646元 / 折扣价： 550 元 加购物车

5.1 The ID and DCN values determined by this test method can provide a measure of the ignition characteristics of diesel fuel oil in compression ignition engines.5.2 This test can be used by engine manufacturers, petroleum refiners and marketers, and in commerce as a specification aid to relate or match fuels and engines.5.3 The relationship of diesel fuel oil DCN determinations to the performance of full-scale, variable-speed, variable-load diesel engines is not completely understood.5.4 This test may be applied to non-conventional fuels. It is recognized that the performance of non-conventional fuels in full-scale engines is not completely understood. The user is therefore cautioned to investigate the suitability of ignition characteristic measurements for predicting performance in full-scale engines for these types of fuels.5.5 This test determines ignition characteristics and requires a sample of approximately 220 mL and a test time of approximately 20 min on a fit-for-use instrument.1.1 This test method covers the quantitative determination of the ignition characteristics of conventional diesel fuel oils, diesel fuel oils containing cetane number improver additives, and is applicable to products typical of Specification D975, Grades No. 1-D and 2-D regular and low-sulfur diesel fuel oils, European standard EN 590, and Canadian standards CAN/CGSB-3.517-2000 and CAN/CGSB 3.6-2000. The test method may also be applied to the quantitative determination of the ignition characteristics of blends of fuel oils containing biodiesel material, and diesel fuel oil blending components.1.2 This test method measures the ignition delay and utilizes a constant volume combustion chamber with direct fuel injection into heated, compressed air. An equation converts an ignition delay determination to a derived cetane number (DCN).1.3 This test method covers the ignition delay range from a minimum value of 35.0 DCN (ignition delay of 4.89 ms) to a maximum value of 59.6 DCN (ignition delay of 2.87 ms). The average DCN result for each sample in the ILS ranged from 37.29 (average ignition delay of 4.5894 ms) to 56.517 (average ignition delay of 3.0281 ms).1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

定价： 0元 / 折扣价： 0 元

5.1 The major organic constituents in industrial waste water need to be identified for support of effective in-plant or pollution control programs. Currently, the most practical means for tentatively identifying and measuring a range of volatile organic compounds is gas-liquid chromatography.1.1 This test method covers a wide range of alcohols with various structures and boiling points that can be separated and detected quantitatively in water and waste water at a minimum detection limit of approximately 1 mg/L by aqueous-injection gas-liquid chromatography.2 This test method can also be used to detect other volatile organic compounds qualitatively. Organic acids, amines, and high boiling, highly polar compounds are not readily detectable under this set of conditions. For analysis of organics with similar functionalities, refer to other test methods in Volumes 11.01 and 11.02 of the Annual Book of ASTM Standards.1.2 This test method utilizes the procedures and precautions as described in Practice D2908. Utilize the procedures and precautions as described therein.1.3 This test method has been used successfully with reagent grade Type II and natural chlorinated tap waters. It is the user's responsibility to assure the validity of this test method for any untested matrices.1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价： 590元 / 折扣价： 502 元 加购物车

5.1 Diesel fuel injection equipment has some reliance on lubricating properties of the diesel fuel. Shortened life of engine components, such as diesel fuel injection pumps and injectors, has sometimes been ascribed to lack of lubricity in a diesel fuel.5.2 Pump Lubricity Value (PLV) test results generally rank fuel effects on diesel injection system pump component distress due to wear in the same order as Bosch, Lucas, Stanadyne, and Cummins in-house rig tests.5 In these fuel/hardware tests, boundary lubrication is believed to be a factor in the operation of the component.5.3 The PLV is sensitive to contamination of the fluids and test materials and the temperature of the test. Lubricity evaluations are also sensitive to trace contaminants acquired during test fuel sampling and storage.5.4 Test Methods D6078 and D6079 are two methods for evaluating diesel fuel lubricity. No absolute correlation has been developed between these two test methods, or between either of these methods and the PLV.5.5 The PLV may be used to evaluate the relative effectiveness of a fluid for preventing wear under the prescribed test conditions.5.6 This test method is designed to evaluate boundary lubrication properties. While viscosity effects on lubricity are not totally eliminated, they are minimized.5.7 This test can indicate whether or not an additive will improve the lubricity of a poor lubricity fuel.1.1 This test method covers evaluating the lubricity of diesel fuels using a pump rig test and Stanadyne Model DB4427-4782 pumps.NOTE 1: Other pumps may be used if a correlation between pump performance factors and fuel lubricity has been developed.1.2 This test method is applicable to any fuel used in diesel engines, including those which may contain a lubricity enhancing additive.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific warning statements are given in Section 7.

定价： 0元 / 折扣价： 0 元

5.1 This test method evaluates the ability of an automotive engine to mitigate preignition in the combustion chambers in turbocharged, direct injection, gasoline engines under low-speed and high-load operating conditions.5.2 Varying quality reference oils, with known preignition tendencies, were used in developing the operating conditions of the test procedure.5.3 The test method has applicability in gasoline-engine-oil specifications and is expected to be used in specifications and classifications of engine lubricating oils, such as the following:5.3.1 Specification D4485.5.3.2 ILSAC GF-6.5.3.3 SAE Classification J183.1.1 This laboratory engine test evaluates the ability of an automotive engine to mitigate preignition in the combustion chambers in gasoline, turbocharged, direct-injection (GTDI) engines under low-speed and high-load operating conditions. This test method is commonly known as the Ford low-speed, preignition (LSPI) test.1.1.1 In vehicles, equipped with relatively small GTDI spark-ignition engines, preignition has occasionally occurred when the vehicles are operated under low-speed and high-load conditions. Uncontrolled, preignition may cause destructive engine damage.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.2.1 Exceptions—Where there is no direct SI equivalent such as screw threads, national pipe threads/diameters, tubing size, wire gauge, or specified single source equipment.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价： 1058元 / 折扣价： 900 元 加购物车

4.1 This practice is subject to the definition of injection molding given in 3.1.2 with the further provision that with in-line screw injection the plastic compound, heated in a chamber by conduction and friction, is fluxed by the action of a reciprocating screw and then is forced into a hot mold where it solidifies. Hereafter, in-line screw-injection molding will be referred to simply as injection molding.4.2 The mold referenced in this section (see Fig. 1) is generally useful, and describes what have been the most common specimens required for the testing of thermosets. ISO specimens and testing are gaining favor, however. Practice D3641 and ISO 10724 describe the layout and practice for injection molding the multi-purpose specimens in accordance with ISO 3167.FIG. 1 Five-Cavity Transfer Mold for Thermosetting Plastic Test Specimens (Steam Cores Not Shown)NOTE 1: Thermometer wells shall be 8 mm (5/16 in.) in diameter to permit use of a readily available thermometer.4.3 Typically, injection-molded test specimens are made with shorter cycles than those used for similar moldings made by compression, and the cycle is equal to or faster than that for transfer molding.4.4 Breathing of the mold is not usually required to release trapped volatile material as the gas is free to flow from the vent end of the mold. This is particularly advantageous for heat-resistant compounds and reduces the tendency for molded specimens to blister at high exposure temperatures.4.5 Injection molding is intended for low-viscosity compounds. One set of processing parameters cannot be specified for all types of thermosetting materials, nor for samples of the same material having different plasticities.4.6 Materials containing fibrous fillers such as glass roving, chopped cloth, or cellulosic fibers can be injection molded, but their properties will be affected depending upon how much fiber breakdown occurs as the compound is worked by the screw and as it passes through the system of runners and gates. The orientation of the fibers in the molded specimen will also affect injection-molded properties.4.7 Flow and knit lines in a molded piece are often sites of mechanical or electrical weakness. The fluxed material passing through the gate wrinkles and folds as it proceeds into the mold cavity. Knit lines are found to some degree throughout the molded piece; and can affect test results. Fibers and other reinforcements in the molding compound align with the flow pattern and, generally, are perpendicular to the axis of the bar at its center and parallel at its surface.4.7.1 Placement and size of gates and vents can be used to minimize flow and knit lines, for example, side gating of bars will minimize the tendency of the material to fold onto itself as the material front proceeds through the length of the mold.4.8 The Izod impact strength of injection-molded specimens containing short fibers will generally be lower than the values obtained using compression molding methods. The impact strength can also vary along the axis of the bar due to molding parameters, flow patterns, and fiber orientation.4.9 The flexural and tensile strength of injection-molded specimens of molding compounds containing short fibers will generally be higher than the values obtained using compression-molding methods. Flexural tests are particularly sensitive to injection molding due to the thin resin skin formed at the surface of the bar during final filling of the cavity and pressure buildup.4.10 At constant mold temperature the following parameters are known to cause an underfilled condition at the vented end of the cavity: incorrect plasticity, too low an injection pressure, insufficient material, too long an injection time, blocked vents, high stock temperature, or incorrect die temperature.1.1 This practice covers the general principles to be followed when injection molding test specimens of thermosetting materials. It is to be used to obtain uniformity in methods of describing the various steps of the injection molding process and in the reporting of those conditions. The exact molding conditions will vary from material to material, and if not incorporated in the material specification, shall be agreed upon between the purchaser and the supplier or determined by previous experience with the particular type of material being used and its plasticity.NOTE 1: The utility of this practice has been demonstrated for the molding of thermosetting molding compounds exhibiting lower-viscosity non-Newtonian flow.1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This practice assumes the use of reciprocating screw injection molding machines.NOTE 2: This standard and ISO 10724 address the same subject matter, but differ in technical content.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价： 515元 / 折扣价： 438 元 加购物车

5.1 Control over the residue content as specified in Specification D1835 is of considerable importance in end-use applications of LPG. Oily residue in LPG is contamination which can occur during production, transportation, or storage.5.2 This test method is quicker and much more sensitive than manual methods, such as Test Method D2158, which is based on evaporation of large sample volumes followed by visual or gravimetric estimation of residue content.5.3 This test method provides enhanced sensitivity in measurements of heavier (oily) residues, with a quantification limit of 10 mg/kg total residue.5.4 This test method gives both quantitative results and information about contaminant composition such as boiling point range and fingerprint, which can be very useful in tracing the source of a particular contaminant.1.1 This test method covers the determination, by gas chromatography, of soluble hydrocarbon materials, sometimes called “oily residue,” which can be present in liquefied petroleum (LP) gases and which are substantially less volatile than the LPG product.1.2 This test method quantifies, in the range of 10 mg/kg to 600 mg/kg (ppm mass), the residue with a boiling point between 174 °C and 522 °C (C10 to C40) in LPG. Higher boiling materials, or materials that adhere permanently to the chromatographic column, will not be detected.1.3 Appendix X3, Appendix X4, and Appendix X6 describe additional applications which could be performed based on the hardware and procedures described in this test method. Appendix X3 describes a test procedure for expanding the analysis range to benzene, Appendix X4 describes a test procedure for the analysis of diisopropanolamine, and Appendix X6 describes a test procedure for the analysis of heavy residues or contaminants from C40 to about C60 in LPG.1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价： 777元 / 折扣价： 661 元 加购物车

The test methods in this standard may be used to measure the concentrations of 99Tc, 230Th, and 234U in soil samples. The test methods are applicable to soils that have been contaminated by nuclear-related activities such as uranium ore processing and uranium enrichment. The FI concentration step reduces detection limits by approximately a factor of ten compared to ICP-MS with conventional sample introduction. Approximate IDLs are listed in Table 1.1.1 This test method covers a procedure for measuring 99Tc and a procedure for measuring 230Th and 234U in soils. It is applicable to background soils and soils that have been contaminated by nuclear processes. It is intended as an alternative to radiochemical methods because it is faster, requires less labor, and produces less waste than many radiochemical methods.1.2 Samples are dried, ground, dissolved by fusion, and analyzed by inductively coupled plasma-mass spectrometry (ICP-MS). A sequential flow injection (FI) technique is used to provide lower detection limits than those obtained with direct aspiration into an ICP-MS, and, in the case of 99Tc, provides separation from interferences.1.3 The 230Th and 234U procedure also would work for 232Th, 235U, and 238U, but the FI preconcentration usually is not required to measure these isotopes at the concentrations typically found in soils.1.4 This test method is guided by quality control procedures derived from U.S. EPA procedures for inorganic analysis reported in SW-846 and the Contract Laboratory Program Statement of Work. The required level of quality control may vary between laboratories and projects. Laboratory statistical quality control procedures are required to ensure that this test method is reliable.1.5 Becquerel (Bq) is the acceptable metric unit for radionuclide activity. However, picocurie (pCi) frequently is the unit used to express regulatory limits for radioactivity. The values stated in either of these units shall be regarded as standard. The values stated in each system may not be exact equivalents; therefore, each system must be used independently of the other, without combining values in any way.1.6 Refer to Practice C 998 for information on soil sample collection.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

定价： 0元 / 折扣价： 0 元

This specification is intended to provide a callout system for thermoplastic polyester (TPES) injection and extrusion materials, both virgin and recycled, based on ISO test methods. However, the proportions of recycled material used, and the nature and amount of any contaminant, as well as the selection of materials cannot be covered practically in this specification. Materials are classified into groups according to their composition, and are further subdivided into classes and grades as specified. Individual groups shall be identified in accordance to performance properties as to tensile strength, tensile modulus, Charpy impact strength, deflection temperature, melt flow rate, and density.1.1 This classification system covers thermoplastic polyester materials suitable for molding or extrusion.1.2 This classification system allows for the use of recycled thermoplastic polyester materials provided that the requirements as stated in this classification system and subsequent line callout (specification) are met. The proportions of recycled material used, as well as the nature and amount of any contaminant, however, cannot be covered practically in this specification.1.3 The properties included in this standard are those required to identify the compositions covered. Other requirements necessary to identify particular characteristics important to specialized applications are to be specified by using the suffixes as given in Section 5.1.4 This classification system and subsequent line callout (specification) are intended to provide a means of calling out plastic materials used in the fabrication of end items or parts. It is not intended for the selection of materials. Material selection can be made by those having expertise in the plastic field only after careful consideration of the design and performance required of the part, the environment to which it will be exposed, the fabrication process to be used, the costs involved, and the inherent properties of the material other than those covered by this specification.1.5 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.6 The following hazards caveat pertains only to the test methods portion, Section 11, of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.NOTE 1: This standard and ISO 7792-1:2012 and ISO 7792-2:2012 address the same subject matter, but differ in technical content.

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5.1 Cyanide and hydrogen cyanide are highly toxic. Regulations have been established to require the monitoring of cyanide in industrial and domestic wastes and surface waters.45.2 It is useful to determine the aquatic free cyanide to establish an index of toxicity when a wastewater is introduced into the natural environment at a given pH and temperature.5.3 This test method is applicable for natural water, saline waters, and wastewater effluent.5.4 Free cyanide measured using this test method is applicable for implementation of the International Cyanide Code Guidance in accordance with Guide D7728.1.1 This test method is used to establish the concentration of free cyanide in an aqueous wastewater, effluent and in-stream free cyanide concentrations after mixing treated water with receiving water. The test conditions of this test method are used to measure free cyanide (HCN and CN–) and cyanide bound in the metal-cyanide complexes that are easily dissociated into free cyanide ions at the pH of 6. Free cyanide is determined at pH 6 at room temperature. The aquatic free cyanide can be determined by matching the pH to the water in the receiving environment in the range of pH 6 to 8. The extent of HCN formation is less dependent on temperature than the pH; however, the temperature can be regulated if deemed necessary for aquatic free cyanide to further simulate the actual aquatic environment.1.2 The free cyanide test method is based on the same instrumentation and technology that is described in Test Method D6888, but employs milder conditions (pH 6–8 buffer versus HCl or H2SO4 in the reagent stream), and does not utilize ligand displacement reagents.1.3 The aquatic free cyanide measured by this procedure should be similar to actual levels of HCN in the original aquatic environment. This in turn may give a reliable index of toxicity to aquatic organisms.1.4 This procedure is applicable over a range of approximately 5 to 500 μg/L (parts per billion) free cyanide. Sample dilution may increase cyanide recoveries depending on the cyanide speciation; therefore, it is not recommended to dilute samples. Higher concentrations can be analyzed by increasing the range of calibration standards or with a lower injection volume. In accordance with Guide E1763 and Practice D6512 the lower scope limit was determined to be 9 μg/L for chlorinated gold leaching barren effluent water and the IQE10 % is 12 µg/L in the gold processing detoxified reverse osmosis permeate waste water sample matrix.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This test method is not recommended for samples that contain reduced sulfur compounds such as sulfides.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in 8.6 and Section 9.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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