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AS 1896-1976 Method of test for ignition temperature of gases and vapours 现行 发布日期 :  1976-07-01 实施日期 : 

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5.1 Benzene is a compound that endangers health, and the concentration is limited by environmental protection agencies to produce a less toxic gasoline.5.2 This test method is fast, simple to run, and inexpensive.5.3 This test method is applicable for quality control in the production and distribution of spark-ignition engine fuels.1.1 This test method covers the determination of the percentage of benzene in spark-ignition engine fuels. It is applicable to concentrations from 0.1 % to 5 % by volume.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification covers requirements for fuel grade ethyl tertiary-butyl ether (ETBE) that may be used for blending with fuels for aviation spark-ignition engines where permissible. The requirements for ETBE that may be used for blending with fuels for aviation spark-ignition engines are given. The ETBE shall be visually free of undissolved water, sediment, and suspended matter that could render the material unacceptable for the intended application.1.1 This specification covers requirements for fuel grade ethyl tertiary-butyl ether (ETBE) that may be used for blending with fuels for aviation spark-ignition engines where permissible. Other ETBE grades available in the marketplace that do not comply with the requirements of this specification, are not suitable for blending with aviation fuels.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 During operation of electrical equipment, including wires, resistors, and other conductors, it is possible for overheating to occur, under certain conditions of operation or when malfunctions occur. When this happens, a possible result is ignition of the insulation material.5.2 This test method assesses the relative resistance of electrical insulating materials to ignition by the effect of hot wire sources.5.3 This test method determines the average time, in seconds, required for material specimens to ignite under the specified conditions of test.5.4 This method is suitable to characterize materials, subject to the appropriate limitations of an expected precision of ±15 %, to categorize materials.5.5 In this procedure the specimens are subjected to one or more specific sets of laboratory conditions. If different test conditions are substituted or the end-use conditions are changed, it is not always possible by or from this test to predict changes in the fire-test-response characteristics measured. Therefore, the results are valid only for the fire test exposure conditions described in this procedure.1.1 This test method is intended to differentiate, in a preliminary fashion, among materials with respect to their resistance to ignition because of their proximity to electrically-heated wires and other heat sources.21.2 This test method applies to molded or sheet materials available in thicknesses up to and including 13.0 mm (0.51 in.).1.3 This test method applies to materials that are rigid or flexible at normal room temperatures. It is important to minimize deformation during preparation, especially during the wire-wrapping step described in 10.1, by following the method outlined under Clause 10, Sample Preparation. Examples of deformation include bowing, in either a transverse or a longitudinal direction, twisting of the specimen, and indentation of the wire into the specimen during the wire-wrapping step, to a degree visible to the eye.1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard. (See SI10 for further details.)1.5 This test method measures and describes the response of materials, products, or assemblies to heat and flame under controlled conditions, but does not by itself incorporate all factors required for fire hazard or fire risk assessment of the materials, products, or assemblies under actual fire conditions.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 Fire testing is inherently hazardous. Adequate safeguards for personnel and property shall be employed in conducting these tests.NOTE 1: Although this test method and IEC TS 60695-2-20 (withdrawn) differ in approach and in detail, data obtained using either are technically equivalent.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification covers two types of metal ignition crucibles, nickel or platinum, complete with covers, for laboratory use. Two types of crucibles shall be classified according to their capacities: Type I is nickel with capacities of 100 mL and 250 mL and Type II is platinum with capacity of 20 mL. Type I are crucibles and covers which shall be made from 99.4% nickel, spun and hardened and Type II are crucibles and covers which shall be made from 99.9% platinum plus iridium, with the iridium content of not more than 0.4%. The crucibles shall have a standard shape with a flat base to give a firm and stable resting surface. The side wall shall form a sloping and convex surface extending up to the brim. Crucibles shall be of one-piece construction. Covers shall be flat, sunken in the center, and shall have an extension to serve as a handle. The sunken area in the center shall fit inside the crucible.1.1 This specification covers two types of metal ignition crucibles, nickel or platinum, complete with covers, for laboratory use.

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5.1 LOI refers to the mass loss of a combustion residue whenever it is heated in an air or oxygen atmosphere to high temperatures. In the cement industry, use of the term LOI normally refers to a mass loss in a sample heated to 950 °C. To combustion engineers, the term LOI normally refers to mass losses in samples heated to temperatures normally less than 950 °C. These test methods establish a procedure for determining LOI values for combustion residues heated to 750 °C or 950 °C. LOI values from these test methods can be used by industries that utilize combustion residues in various processes and products.5.2 If the solid combustion residue is heated to estimate the combustible or unburned carbon in the sample, it has been shown that LOI and estimation of unburned carbon do not necessarily agree well with each other and that LOI should not be used as an estimate of unburned carbon in all combustion residues.4 Direct determination of unburned (combustible) carbon can be carried out using Test Method D6316.5.3 If the solid combustion residue is heated to prepare an ash for the determination of the mass fractions of major and minor elements, use the heating procedure described in Test Methods D3682, D4326, and D6349, or the procedures for the 750 °C LOI determination described in these test methods (Method A).5.4 If the solid combustion residue is heated to prepare an ash for the determination of the mass fractions of trace elements, use the heating procedure described in Test Methods D3683 and D6357.NOTE 1: Combustion residues produced in furnace operations or other combustion systems can differ from the ash yield, as determined in Test Methods D3174 and D7582, because combustion conditions influence the chemistry and amount of ash. Combustion causes an expulsion of all water, the loss of carbon dioxide from carbonates, the conversion of metal sulfides into metal oxides, metal sulfates and sulfur oxides, and other chemical reactions. Likewise, the “ash” obtained after igniting combustion residues can differ in composition and amount from Test Methods D3174 and D7582 ash yields because of different heating procedures, combustion of unburned carbon, and decomposition of materials in the residue.1.1 These test methods cover the determination of the mass loss from solid combustion residues upon heating in an air or oxygen atmosphere to a prescribed temperature. The mass loss can be due to the loss of moisture, carbon, sulfur, and so forth, from the decomposition or combustion of the residue.1.2 Units—The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This guide describes the requirements for igniting oil for the purpose of in-situ burning. It is intended to aid decision-makers and spill-responders in contingency planning, spill response, and training, and to aid manufacturers in developing effective ignition devices.4.2 This guide describes criteria for the design and selection of ignition devices for in-situ burning applications.4.3 This guide is not intended as a detailed operational manual for the ignition and burning of spilled oil.1.1 This guide relates to the use of in-situ burning of spilled oil. The focus of the guide is in-situ burning of oil on water, but the ignition techniques and devices described in the guide are generally applicable to in-situ burning of oil spilled on land as well.1.2 The purpose of this guide is to provide information that will enable oil-spill responders to select the appropriate techniques and devices to successfully ignite oil spilled on water.1.3 This guide is one of four related to in-situ burning of oil spills. Guide F1788 addresses environmental and operational considerations. Guide F2152 addresses fire-resistant booms, and Guide F2230 addresses burning in ice conditions.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. In particular, the storage, transport, and use of ignition devices may be subject to regulations that will vary according to the jurisdiction. While guidance of a general nature is provided herein, users of this guide should determine regulations that apply to their situation.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Test Method—It was determined through field testing that intake valve deposits could adversely affect the driveability of certain automobiles.7 Southwest Research Institute and BMW of North America (BMW NA) jointly conducted testing to develop this test method to determine an unleaded automotive spark-ignition engine fuel's propensity to form intake valve deposits. This testing concluded that if an automotive spark-ignition engine fuel could keep intake valve deposits at or below a certain average weight per valve at the end of mileage accumulation, then that automotive spark-ignition engine fuel could be used in the BMW vehicle-engine combination for a specified period without intake valve deposits causing driveability degradation. Minimizing intake valve deposits may be necessary to maintain vehicle driveability and tailpipe emissions control.5.1.1 State and Federal Legislative and Regulatory Action—Legislative activity and rulemaking primarily by California Air Resources Board8 and the Environmental Protection Agency9 necessitate the acceptance of a standardized test method to evaluate the intake system deposit forming tendency of an automotive spark-ignition engine fuel.5.1.2 Relevance of Results—The operating conditions and design of the engine and vehicle used in this test method are not representative of all modern automobiles. These factors shall be considered when interpreting test results.5.2 Test Validity: 5.2.1 Procedural Compliance—The test results are not considered valid unless the test is completed in compliance with all requirements of this test method. Deviations from the parameter limits presented in Sections 10 and 11 will result in an invalid test. Engineering judgment shall be applied during conduct of the test method when assessing any anomalies to ensure validity of the test results.5.2.2 Vehicle Compliance—A test is not considered valid unless the vehicle met the quality control inspection requirements as described in Section 10.1.1 This test method covers a vehicle test procedure for evaluation of intake valve deposit formation of unleaded spark-ignition engine fuels. This test method uses a 1985 model BMW 318i2 vehicle. Mileage is accumulated following a specified driving schedule on either public road or test track. This test method is adapted from the original BMW of North America/Southwest Research Institute Intake Valve Deposit test and maintains as much commonality as possible with the original test. Chassis dynamometers shall not be used for this test procedure as the BMW NA/SwRI IVD Test was not intended to be applicable to chassis dynamometers and no correlation between road operation and chassis dynamometers has been established.NOTE 1: If there is any doubt as to the latest edition of Test Method D5500, contact ASTM International.1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific statements on hazards are given throughout this test method.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D2533-99 Standard Test Method for Vapor-Liquid Ratio of Spark-Ignition Engine Fuels (Withdrawn 2008) Withdrawn, No replacement 发布日期 :  1970-01-01 实施日期 : 

The tendency of a fuel to vaporize in common automobile fuel systems is indicated by the vapor-liquid ratio of that fuel at conditions approximating those in critical parts of the fuel systems.1.1 This test method covers a procedure for measuring the volume of vapor formed at atmospheric pressure from a given volume of gasoline. The ratio of these volumes is expressed as the vapor-liquid (V/L) ratio of the gasoline at the temperature of the test. 1.2 Dry glycerol can be used as the containing liquid for nonoxygenated fuels. 1.3 Mercury can be used as the containing liquid with both oxygenated and nonoxygenated fuels. Because oxygenates in fuels may be partially soluble in glycerol, gasoline-oxygenate blends must be tested using mercury as the containing fluid. Note 1-Test Method D4815 can be used to determine the presence of oxygenates in fuels. 1.4 The values stated in both inch-pound and SI units are to be regarded separately as the standard. The units given in parentheses are for information only. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 7 and Note 10.

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A knowledge of spark-ignition engine fuel composition is useful for regulatory compliance, process control, and quality assurance.The quantitative determination of olefins and other hydrocarbon types in spark-ignition engine fuels is required to comply with government regulations.This test method is not applicable to M85 and E85 fuels, which contain 85 % methanol and ethanol, respectively.1.1 This test method provides for the quantitative determination of oxygenates, paraffins, olefins, naphthenes, and aromatics in low-olefin spark-ignition engine fuels by multidimensional gas chromatography. Each hydrocarbon type can be reported either by carbon number (see ) or as a total through C10, except for olefins, which can only be reported through C9. Higher boiling hydrocarbons cannot be reported by type and are reported as a composite group. The lower limit of detection for a single hydrocarbon component or carbon number type is 0.05 mass %.Note 1—There can be an overlap between the C9 and C10 aromatics; however, the total is accurate. Isopropyl benzene is resolved from the C8 aromatics and is included with the other C9 aromatics. Naphthalene is determined with the C11+ components.1.2 This test method is applicable for total olefins in the range from 0.05 to 13 mass %. The test method can quantitatively determine olefins in samples where the olefin concentration does not exceed 0.6 % C4 or 4.0 % C5 or 4.5 % of the combined C4 and C5. Although the precision for benzene was determined in the range from 0.3 to 1.0 mass %, this test method can be used to determine benzene concentrations up to 5.0 mass %.1.3 This test method is not intended to determine individual hydrocarbon components except for those hydrocarbon types for which there is only one component within a carbon number. Individually determined hydrocarbons are benzene, toluene, cyclopentane, propane, propylene, and cyclopentene.1.4 Precision data has only been obtained on samples containing MTBE. Application of this test method to determine other oxygenates shall be verified in the user's laboratory. Methanol cannot be determined and shall be quantitated by an appropriate oxygenate method such as Test Method D 4815 or D 5599. Methanol is fully resolved and does not interfere with the determination of other components or groups.1.5 Although specifically written for spark-ignition engine fuels containing oxygenates, this test method can also be applied to other hydrocarbon streams having similar boiling ranges, such as naphthas and reformates.1.6 The values stated in SI units are to be regarded as the standard.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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