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5.1 This test method is based on Test Method F903 for measuring resistance of chemical protective clothing materials to penetration by liquids. This test method is normally used to evaluate specimens from individual finished items of protective clothing and individual samples of materials that are candidates for items of protective clothing.5.1.1 Finished items of protective clothing include gloves, arm shields, aprons, gowns, coveralls, hoods, and boots.5.1.2 The phrase “specimens from finished items” encompasses seamed and other discontinuous regions as well as the usual continuous regions of protective clothing items.5.2 Medical protective clothing materials are intended to be a barrier to blood, body fluids, and other potentially infectious materials. Many factors can affect the wetting and penetration characteristics of body fluids, such as surface tension, viscosity, and polarity of the fluid, as well as the structure and relative hydrophilicity or hydrophobicity of the materials. The surface tension range for blood and body fluids (excluding saliva) is approximately 0.042 to 0.060 N/m (1) .7 To help simulate the wetting characteristics of blood and body fluids, the surface tension of the synthetic blood is adjusted to approximate the lower end of this surface tension range. The resulting surface tension of the synthetic blood is approximately 0.042 ± 0.002 N/m.5.3 The synthetic blood mixture is prepared with a red dye to aid in visual detection and a thickening agent to simulate the flow characteristics of blood.5.4 Part of the protocol in Procedures A and B in Table 1 for exposing the protective clothing material specimens with synthetic blood involves pressurization of the test cell to 13.8 kPa [2 psig]. This hydrostatic pressure has been documented to discriminate between protective clothing material performance and to correlate with visual penetration results that are obtained with a human factors validation (2). Some studies, however, suggest that mechanical pressures exceeding 345 kPa [50 psig] can occur during clinical use (3, 4). Therefore, it is important to understand that this test method does not simulate all the physical stresses and pressures that are exerted on protective clothing garments during actual use. This test method is offered to identify those protective clothing materials that warrant further evaluation with a microbiological challenge.5.5 Since this test method uses visual observation rather than analytical measurements for determination of penetration, use this test method as a preliminary evaluation for possible penetration of blood and other body fluids. Perform subsequent testing with a microbiological challenge and analytical technique using Test Method F1671.NOTE 1: No viral resistance claims can be made based on this test method, as materials can pass the test method and fail Test Method F1671.5.6 Testing without considering degradation by physical, chemical, and thermal stresses which could negatively impact the performance of the protective barrier could lead to a false sense of security. Consider tests which assess the impact of storage conditions and shelf life for disposable products, and the effects of laundering and sterilization for reusable products. The integrity of the protective barrier can also be compromised during use by such effects as flexing and abrasion (5) . It is also possible that prewetting by contaminating materials such as alcohol and perspiration can also compromise the integrity of the protective barrier. If these conditions are of concern, evaluate the performance of protective clothing materials for synthetic blood penetration following an appropriate preconditioning technique representative of the expected conditions of use.5.7 While this test method involves a qualitative determination of the protective clothing material resistance to penetration by synthetic blood under specific test conditions, it is possible to use this test method as a material quality control or assurance procedure.5.7.1 If this procedure is used for quality control, perform proper statistical design and analysis of the data when more than three specimens are tested. This type of analysis includes, but is not limited to, the number of individual specimens tested, the average percent passing or failing, or both, with a standard deviation. Data reported in this way helps to establish confidence limits concerning product performance. Examples of acceptable sampling plans are found in references such as MIL-STD-105, ANSI/ASQC Z1.4, and ISO 2859-1.1.1 This test method is used to evaluate the resistance of materials used in protective clothing to penetration by synthetic blood under conditions of continuous liquid contact. Protective clothing pass/fail determinations are based on visual detection of synthetic blood penetration.1.1.1 This test method is not always effective in testing protective clothing materials having thick, inner liners which readily absorb the synthetic blood.1.2 This test method is a means for selecting protective clothing materials for subsequent testing with a more sophisticated barrier test as described in Test Method F1671.1.3 This test method does not apply to all forms or conditions of blood-borne pathogen exposure. Users of the test method must review modes for work/clothing exposure and assess the appropriateness of this test method for their specific application.1.4 This test method addresses only the performance of materials or certain material constructions (for example, seams) used in protective clothing. This test method does not address the design, overall construction and components, or interfaces of garments, or other factors which may affect the overall protection offered by the protective clothing.1.5 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method evaluates puncture resistance of protective clothing materials which may include: plastics or elastomeric films, coated fabrics, flexible materials, laminates, leathers, or textile materials.5.1.1 This test method uses hypodermic needles with specified dimensions as puncture probes.5.1.2 This test method evaluates needle puncture resistance of protective clothing materials, perpendicular to the material’s surface and with no supporting structure under/behind the material specimen.5.1.3 Evaluation of puncture resistance for snag-type puncture should be performed in accordance with Test Method D2582.5.1.4 Evaluation of puncture resistance for non-cutting puncture should be performed in accordance with Test Method F1342/F1342M.AbstractThis test method is used for determining the force required to cause a hypodermic needle to penetrate through protective clothing material. It defines three common hypodermic needles - 21-, 25-, 28- gauge needles - to evaluate puncture resistance of protective clothing. This test method does not attempt to simulate all use conditions. A number of variables which impact puncture resistance, such as stiffness of backing materials, presence of lubricants, and tension on the specimen, are not addressed by this test method.1.1 This test method is used to determine the force required to cause a sharp-edged hypodermic needle to penetrate through protective clothing material. The standard describes three needles that may be used: 21-, 25-, or 28-gauge needles.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Workers who have the potential to be exposed to molten metal contact shall be permitted to wear protective clothing using materials that have been evaluated for heat transfer using this test method.5.2 This test method rates materials that are intended for primary protective clothing against potential molten substance contact for their thermal insulating properties and their reaction to the test exposure.5.3 The protective performance, as determined by this test method, will relate to the actual end-use performance only to the degree that the end-use exposure is identical to the exposure used in the test method.5.4 Visual inspection of the specimen subjectively notes the material's resistance to molten substance contact.1.1 This test method covers the evaluation of materials' thermal resistance to heat transfer when exposed to a molten substance pour.1.1.1 This test method was validated using molten substances of aluminum, brass, and iron. The test shall be permitted to be adapted for use with other substances.1.2 This test method is applicable to materials from which finished primary protective apparel articles are made.1.3 This test method does not measure the flammability of materials, nor is it intended for use in evaluating materials exposed to any other thermal exposure.1.4 Use this test method to measure and describe the properties of materials, products, or assemblies in response to molten substance pour under controlled laboratory conditions and shall not be used to describe or appraise the thermal hazard or fire risk of materials, products, or assemblies under actual conditions. However, it is acceptable to use results of this test as elements of a thermal risk assessment which takes into account all the factors that are pertinent to an assessment of the thermal hazard of a particular end use.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in Section 8.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method is based on Test Method F903 for measuring resistance of chemical protective clothing materials to penetration by liquids. This test method is normally used to evaluate specimens from individual finished items of protective clothing and individual samples of materials that are candidates for items of protective clothing.5.1.1 Finished items of protective clothing include gloves, arm shields, aprons, gowns, coveralls, hoods, and boots.5.1.2 The phrase “specimens from finished items” encompasses seamed and other discontinuous regions, as well as the usual continuous regions of protective clothing items.5.2 It is known that body fluids penetrating protective clothing materials are likely to carry microbiological contaminants; however, visual detection methods are not sensitive enough to detect minute amounts of liquid containing microorganisms (1-3).7 This test method uses media containing Phi-X174 Bacteriophage. The visual detection technique of this test method is supplemented with a biologically based assay capable of detecting virus under the specified test conditions.5.3 Test Method F1670/F1670M allows the screening of protective clothing materials for resistance to penetration with synthetic blood as a challenge liquid. Test Method F1670/F1670M uses the same penetration test cell and technique, but exposes material specimens to synthetic blood with visual detection of liquid penetration. Materials passing Test Method F1670/F1670M should then be tested against bacteriophage penetration using this test method to verify performance.5.4 This test method has been specifically designed for measuring penetration of a surrogate microbe for Hepatitis (B and C) and the Human Immunodeficiency Viruses. The surrogate, Phi-X174 Bacteriophage, used in this test method is similar to HCV in size and shape but also serves as a surrogate for HBV and HIV. Inferences about protection from other pathogens must be assessed on a case-by-case basis.5.5 Part of the protocol in Procedures A and B in Table 1 for exposing the protective clothing material specimens to the Phi-X174 Bacteriophage challenge suspension involves pressurization of the penetration cell to 13.8 kPa [2 psig]. This hydrostatic pressure has been documented to discriminate between protective clothing material performance and correlate with visual penetration results that are obtained with a human factors validation (4). Some studies, however, suggest that mechanical pressures exceeding 345 kPa [50 psig] can occur during actual clinical use (5, 6). Therefore, it is important to understand that this test method does not simulate all the physical stresses and pressures that might be exerted on protective clothing materials during actual use.5.6 Medical protective clothing materials are intended to be a barrier to blood, body fluids, and other potentially infectious materials. Many factors can affect the wetting and penetration characteristics of body fluids, such as surface tension, viscosity, and polarity of the fluids, as well as the structure and relative hydrophilicity or hydrophobicity of the materials. The surface tension range for blood and body fluids (excluding saliva) is approximately 0.042 to 0.060 N/m (7). To help simulate the wetting characteristics of blood and body fluids, the surface tension of the Phi-X174 Bacteriophage challenge suspension is adjusted to approximate the lower end of this surface tension range. This is accomplished by adding surfactant to the Phi-X174 Bacteriophage nutrient broth. The resulting surface tension of the Phi-X174 Bacteriophage challenge suspension is approximately 0.042 ± 0.002 N/m.5.7 Testing prior to degradation by physical, chemical, and thermal stresses which could negatively impact the performance of the protective material could lead to a false sense of security. Additional tests should be considered that assess the impact of storage conditions and shelf life on disposable products and the impact of laundering and sterilization on reusable products. The integrity of the protective barrier may also be compromised during use by such effects as flexing and abrasion (8). Prewetting agents, such as alcohol, and contaminating agents, such as perspiration, may also compromise the integrity of the protective barrier. If these conditions are of concern, the performance of protective clothing materials should be evaluated for Phi-X174 Bacteriophage penetration following an appropriate preconditioning technique representative of the expected conditions of use.5.8 This test method involves a sensitive assay procedure for determining protective clothing material resistance to penetration by a surrogate microbe. Because of the length of time required to complete this method, it may not be suitable for use as a material or protective clothing quality control or quality assurance procedure.5.9 If this procedure is used for quality control or to support broad product claims concerning the viral-resistant properties of materials used in protective clothing, proper statistical design and analysis of larger data sets than those specified in this test method should be performed.8 Examples of acceptable sampling plans can be found in MIL-STD-105, ANSI/ASQ Z1.4, and ISO 2859-1.5.10 This test method requires a working knowledge of basic microbiological techniques (9).1.1 This test method is used to measure the resistance of materials used in protective clothing to penetration by blood-borne pathogens using a surrogate microbe under conditions of continuous liquid contact. Protective clothing material pass/fail determinations are based on the detection of viral penetration.1.1.1 This test method is not always effective in testing protective clothing materials having thick, inner liners which readily absorb the liquid assay fluid.1.2 This test method does not apply to all forms or conditions of blood-borne pathogen exposure. Users of the test method should review modes for worker/clothing exposure and assess the appropriateness of this test method for their specific applications.1.3 This test method has been specifically defined for modeling the viral penetration of Hepatitis (B and C) and Human Immunodeficiency Viruses transmitted in blood and other potentially infectious body fluids. Inferences for protection from other pathogens must be assessed on a case-by-case basis.1.4 This test method addresses only the performance of materials or certain material constructions (for example, seams) used in protective clothing and determined to be viral resistant. This test method does not address the design, overall construction and components, or interfaces of garments or other factors which may affect the overall protection offered by the protective clothing.1.5 The values stated in SI units or in other units shall be regarded separately as standard. The values stated in each system must be used independently of the other, without combining values in any way.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method determines the ignitability of materials in single or multiple layers.5.1.1 Material performance shall be determined from the ignitability of the specimen(s) and shall be reported as a probability of ignition at various incident energy levels.5.1.2 Materials which meet the flame resistance requirements of Specification F1506 do not require testing by this test method unless the mechanism of passing Specification F1506 involves melting and escape from the flame source (for example, coated fabrics, certain rainwear fabrics).5.2 This test method maintains the specimen in a static, vertical position and does not involve movement except that resulting from the exposure.5.3 This test method specifies a standard set of exposure conditions. Different exposure conditions may produce different results. In addition to the standard set of exposure conditions, other conditions representative of the expected hazard may be used.1.1 This test method is used to identify materials that are ignitable and that can continue to burn when exposed to an electric arc, and determines (a) the incident exposure energy that causes ignition, and (b) the probability of ignition.1.2 The specimens tested in this test method are materials fabricated in the form of shirts.1.3 This test method shall be used to measure and describe the properties of materials, products, or assemblies in response to convective and radiant energy generated by an electric arc under controlled laboratory conditions.1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.1.5 This standard shall not be used to describe or appraise the fire hazard or fire risk of materials, products, or assemblies under actual fire conditions. However, results of this test may be used as elements of a fire assessment which takes into account all of the factors which are pertinent to an assessment of the fire hazard of a particular end use.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.1.7 For specific precautions, see Section 7.

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5.1 This test method is intended for the determination of the arc rating of a material, or a combination of materials.5.1.1 Because of the variability of the arc exposure, different heat transmission values may be observed at individual sensors. Evaluate the results of each sensor in accordance with Section 12.5.2 This test method maintains the specimen in a static, vertical position and does not involve movement except that resulting from the exposure.5.3 This test method specifies a standard set of arc exposures performed under controlled laboratory conditions. Different exposure conditions have the potential to produce different results. In addition to the standard set of exposure conditions, other conditions representative of the expected hazard may be used and shall be documented in the reporting of the testing results.1.1 This test method is used to determine the arc rating of materials intended for use as flame resistant clothing for workers exposed to electric arcs that would generate heat flux rates of approximately 2100 kW/m2 [50 cal/cm2s] using an open air arc.1.2 This test method will determine the arc rating of materials which meet the following requirements: less than 150 mm [6 in.] char length and less than 2 s afterflame when tested in accordance with Test Method D6413.1.2.1 It is not the intent of this test method to evaluate non flame-resistant materials.1.3 The materials used in this test method are in the form of flat specimens.1.4 This test method shall be used to measure and describe the properties of materials, products, or assemblies in response to convective and radiant energy generated by an electric arc under controlled laboratory conditions.1.5 The values stated in SI units shall be regarded as standard except as noted. Within the text, alternate units are shown in brackets. The values stated in each system may not be exact equivalents therefore alternate systems must be used independently of the other. Combining values from the systems described in the text may result in nonconformance with the method.1.6 This test method does not apply to electrical contact or electrical shock hazards.1.7 This standard shall not be used to describe or appraise the fire hazard or fire risk of materials, products, or assemblies under actual fire conditions. However, results of this test may be used as elements of a fire assessment which takes into account all of the factors which are pertinent to an assessment of the fire hazard of a particular end use.1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific precautions, see Section 7.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method evaluates puncture resistance of protective clothing materials which may include plastics or elastomeric films, coated fabrics, flexible materials, laminates, or textile materials.5.2 This test method is not intended to measure puncture resistance of all types of punctures encountered using protective clothing material. This test method involves a procedure where a puncture probe of specified dimensions is used for puncturing specimens.5.3 This test method evaluates puncture resistance of protective clothing materials, specifically for puncture forced on specimens perpendicular to material surface. There is no supporting structure under the material specimen.5.4 Evaluation of puncture resistance for snag-type puncture should be performed in accordance with Test Method D2582.1.1 This test method determines the puncture resistance of a protective clothing material specimen by measuring the force required to cause a pointed puncture probe to penetrate through the specimen. This test method describes three protocols that may be used: Method A, Method B, and Method C.1.1.1 Method A requires the use of Probe A only. The probe used for testing shall be recorded in the test report.1.1.1.1 Probe A may be used to measure puncture resistance for the following types of materials:(1) Elastomeric materials,(2) Textiles, and(3) Coated materials.1.1.2 Method B requires the use of Probe B. The probe used for testing shall be recorded in the test report.1.1.2.1 Probe B may be used to measure puncture resistance for the following types of materials:(1) Textiles.(2) Coated materials.NOTE 1: Probe B is not suited for measuring the puncture resistance of unsupported elastomeric materials.1.2 The values stated in SI units are to be regarded as the standard. The values in inch-pound units in brackets are for information purposes only. The values stated in each system may not be exact equivalents; therefore, each system must be used independently of the other, without combining values in any way.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Use this test method to measure the thermal protection provided by different materials, garments, clothing ensembles, and systems when exposed to a specified fire (see 3.2.2, 3.2.3, 4.1, and 10.4).5.1.1 This test method does not simulate high radiant exposures, for example, those found in electric arc flash exposures, some types of fire exposures where liquid or solid fuels are involved, nor exposure to nuclear explosions.5.2 This test method provides a measurement of garment and clothing ensemble performance on a stationary upright manikin of specified dimensions. This test method is used to provide predicted skin burn injury for a specific garment or protective clothing ensemble when exposed to a laboratory simulation of a fire. It does not establish a pass/fail for material performance.5.2.1 This test method is not intended to be a quality assurance test. The results do not constitute a material’s performance specification.5.2.2 The effects of body position and movement are not addressed in this test method.5.3 The measurement of the thermal protection provided by clothing is complex and dependent on the apparatus and techniques used. It is not practical in a test method of this scope to establish details sufficient to cover all contingencies. Departures from the instructions in this test method have the potential to lead to significantly different test results. Technical knowledge concerning the theory of heat transfer and testing practices is needed to evaluate if, and which departures from the instructions given in this test method are significant. Standardization of the test method reduces, but does not eliminate, the need for such technical knowledge. Report any departures along with the results.1.1 This test method is used to provide predicted human skin burn injury for single-layer garments or protective clothing ensembles mounted on a stationary upright instrumented manikin which are then exposed in a laboratory to a simulated fire environment having controlled heat flux, flame distribution, and duration. The average exposure heat flux is 84 kW/m2 (2 cal/s·cm2), with durations up to 20 s.1.2 The visual and physical changes to the single-layer garment or protective clothing ensemble are recorded to aid in understanding the overall performance of the garment or protective clothing ensemble and how the predicted human skin burn injury results can be interpreted.1.3 The skin burn injury prediction is based on a limited number of experiments where the forearms of human subjects were exposed to elevated thermal conditions. This forearm information for skin burn injury is applied uniformly to the entire body of the manikin, except the hands and feet. The hands and feet are not included in the skin burn injury prediction.1.4 The measurements obtained and observations noted can only apply to the particular garment(s) or ensemble(s) tested using the specified heat flux, flame distribution, and duration.1.5 This standard is used to measure and describe the response of materials, products, or assemblies to heat and flame under controlled conditions, but does not by itself incorporate all factors required for fire hazard or fire risk assessment of the materials, products, or assemblies under actual fire conditions.1.6 This method is not a fire test response test method.1.7 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units or other units commonly used for thermal testing. If appropriate, round the non-SI units for convenience.1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.9 Fire testing is inherently hazardous. Adequate safeguards for personnel and property shall be employed in conducting these tests.1.10 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method is normally used to evaluate the barrier effectiveness against penetration of liquids through materials, seams, closures, or other planar assemblies used in protective clothing and specimens from finished items of protective clothing.5.1.1 Finished items of protective clothing include gloves, arm protectors, aprons, coveralls, suits, hoods, boots, and similar items.5.1.2 The phrase “specimens from finished items” is permitted to include continuous regions of protective clothing items as well as seamed or other discontinuous regions of protective clothing.5.1.3 The types of specimens are limited to those that are relatively flat (planar) that are capable of being sealed in the test cell specified in this test method without peripheral leakage.5.2 A substitute challenge liquid (for example, water or isopropanol) is appropriate in some cases to generalize material penetration resistance to liquids. However, it is possible that differences in chemical and molecular properties (for example, surface tension) may lead to different results.5.3 In addition to the failure mode where a liquid finds a pathway for penetration through a void, imperfection, or defect in material or clothing subassembly, some selected chemicals cause degradation of barrier material, film, or coating, leading to penetration over extended periods of contact.75.4 Five different procedures for how the specimen is exposed to the liquid are provided in Table 1. In this test method, all procedures involve liquid exposure that is continuous over the duration of the test. These procedures entail different hydrostatic pressures and durations of liquid exposure.5.4.1 Procedures A, B, and C apply a set pressure (6.9 or 13.8 kPa [1 or 2 psig]) for a specified period of time (1 or 10 min) over a 15- or 60-min liquid exposure time.5.4.2 Procedures A and B represent the originally established methods of liquid contact developed by the National Institute for Occupational Safety and Health, where Procedure A involves the application of a test pressure (13.8 kPa [2 psig]) that has been found to discriminate the liquid barrier performance of materials, while a lower pressure (6.9 kPa [1 psig]) is used for Procedure B to accommodate materials that exhibit ballooning or extension when the 13.8 kPa (2 psig) pressure is applied.8,9 Both procedures entail exposure of the specimen for 5 min at ambient pressure followed by 10 min of exposure of the specimen to the test pressure.5.4.3 Procedure C was developed to account for potentially longer exposures where failure may also occur as the result of material or assembly degradation. Procedure C uses a 13.8 kPa (2 psig) test pressure for a portion of the test where the specimen is first exposed to the liquid at ambient pressure for 5 min, followed by 1 min at 13.8 kPa (2 psig), and continuing for 54 additional minutes at ambient pressure.5.4.4 Procedure D involves the sequential increase of pressure from ambient (0 kPa [0 psig]) to 68.9 kPa (10 psig) in increments of 3.5 kPa (0.5 psig) in 1-min intervals until liquid penetration is observed at a specific test pressure. The time interval between changes in pressure is set at 1 min to coincide with the time of applied pressure in Procedure C.5.4.5 Procedure E permits the test method user to specify the pressures and duration of the specimen’s exposure to the liquid.5.5 Different results are reported by the different procedures.5.5.1 Procedures A, B, and C results are reported as “pass” or “fail” for each replicate. Passing results indicate that no liquid penetration was observed over the duration of the test exposure.5.5.2 Procedure D results are reported as the test pressure at which liquid penetration was observed for each replicate.5.6 The choice of pressure/time sequence and type of test result are dependent on the objectives of the testing.5.6.1 Procedure C is specified in several different National Fire Protection Association standards for establishing the minimum barrier performance of protective clothing materials, seams, and closures of first responder protective clothing.5.6.2 Procedure D may be used when the pressure where penetration occurs is sought without a set pressure pass/fail criterion. Procedure D also has utility for assessing the robustness of protective clothing materials and assemblies as part of quality systems. It is also possible to use Procedure D to supplement the pass/fail results provided by Procedures A, B, and C.5.6.3 Procedure E permits setting a specific sequence of pressure/time exposures based on the specific needs for the testing.5.6.4 In this test method, a hydrostatic pressure is applied but does not necessarily correlate with a mechanical pressure against a semi-rigid or rigid surface.5.6.5 It is recommended that a human factors investigation, hazard/risk exposure assessment, or similar study be conducted to determine the most suitable procedure for relating the choice of a specific procedure for measuring protective clothing material liquid penetration resistance to the intended protective performance of the clothing material.5.7 This test method permits the use of a retaining screen for preventing the overextension of a specimen as pressure is applied. However, it is important that the selected retaining screen does not interfere with the observation of liquid penetration or affect the sealing of the specimen in the test cell.5.8 A critical feature of the test is how the specimen is sealed in the test cell. Inadequate sealing of the specimen can lead to a false result (observed liquid penetration that is due to the method of sealing rather than penetration through the specimen). It is recommended that any special means used to seal specimens in the test cell be validated for providing sufficient integrity of the specimen in the test cell, not contribute to specimen damage, and not interfere with the observation of liquid penetration. Special means used to seal specimens in the test cell should be documented in the report.5.9 A minimum number of three test specimens is established for this test method. However, it is also appropriate to establish sampling plans based on a specific acceptable quality limit using a larger number of specimens, depending on the application of the test method. Potential sampling plans for this approach are found in MIL-STD-105E, ANSI/ASQC Z1.4, and ISO 2859-1.5.10 This test method does not address the liquid penetration of full protective clothing or ensembles. Use Test Method F1359 to provide a complete evaluation of the liquid integrity of protective clothing or ensembles, particularly areas of the clothing or ensembles that cannot be directly assessed by this test method, such as interface areas between different items of clothing and equipment.1.1 This test method is used to test specimens of protective clothing materials, assemblies such as seams and closures, or interfaces used in the construction of protective clothing. The resistance to visible penetration of the test liquid is determined with the liquid in continuous contact with the normally outside (exterior) surface of the test specimen.1.2 This test method includes different procedures for maintaining the liquid in contact with the test specimen in terms of the length of exposure and the pressure applied. Suggestions are provided for how to select an appropriate procedure for liquid contact.1.3 In some cases, significant amounts of hazardous materials will permeate specimens that pass the penetration tests. For more sensitive analyses, use either Test Method F739 or F1383 to determine permeation.1.4 This test method does not address penetration of vapors through protective clothing materials.1.5 This test method is not applicable to non-planar protective clothing materials, interfaces, or assemblies such as the fingertips or crotch areas of gloves, which are possible failure points.1.6 This test method does not address the liquid penetration resistance of full protective clothing items or ensembles. Use Test Method F1359 for this purpose.1.7 The values as stated in inch-pound units are to be regarded as the standard. The values in parentheses are for information only.1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazards are given in Section 7.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method is intended for the determination of the radiant heat resistance value of a material, a combination of materials, or a comparison of different materials used in flame-resistant clothing for workers exposed to radiant thermal hazards.5.2 This test method evaluates a material's heat transfer properties when exposed to a continuous and constant radiant heat source. Air movement at the face of the specimen and around the calorimeter can affect the measured heat transferred due to forced convective heat losses. Minimizing the air movement around the specimen and test apparatus will aid in the repeatability of the results.5.3 This test method maintains the specimen in a static, vertical position and does not involve movement, except that resulting from the exposure.5.4 This test method specifies two standard sets of exposure conditions: 21 kW/m2 (0.5 cal/cm2s) and 84 kW/m2 (2.0 cal/cm2s). Either can be used.5.4.1 If a different set of exposure conditions is used, it is likely that different results will be obtained.5.4.2 The optional use of other conditions representative of the expected hazard, in addition to the standard set of exposure conditions, is permitted. However, the exposure conditions used must be reported with the results along with a determination of the exposure energy level stability.5.5 This test method does not predict skin burn injury from the standardized radiant heat exposure.NOTE 4: See Appendix X4 for additional information regarding this test method and predicted skin burn injury.1.1 This test method rates the non-steady state thermal resistance or insulating characteristics of flame resistant clothing materials subjected to a continuous, standardized radiant heat exposure.1.1.1 This test method is not applicable to clothing materials that are not flame resistant.NOTE 1: The determination of a clothing material's flame resistance shall be made prior to testing and done in accordance with the applicable performance standard, specification standard, or both, for the clothing material's end use.1.1.2 This test method does not predict skin burn injury from the standardized radiant heat exposure, as it does not account for the thermal energy contained in the test specimen after the exposure has ceased.NOTE 2: See Appendix X4 for additional information regarding this test method and predicted skin burn injury.1.2 This test method is used to measure and describe the response of materials, products, or assemblies to heat under controlled conditions, but does not by itself incorporate all factors required for fire hazard or fire risk assessment of the materials, products, or assemblies under actual fire conditions.1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound or other units that are commonly used for thermal testing.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method is intended to determine the ignition resistance and burning characteristics of materials used in protective clothing where flame resistance is not the primary form of protection designated.5.1.1 Flame resistance is a distinctive property of clothing items designated for isolating parts of the body from anticipated flame hazards. It is possible that protective clothing designated for isolation from other hazards, such as those for chemical or biological protection, neither have flame resistance nor isolate the wearer from flame hazards. This test method can be used to evaluate the effects of flame impingement on protective clothing where flame resistance is not the primary objective of protection.5.1.2 When flame resistance is the primary protection offered by the protective clothing, alternative test methods can be used. A test method that is useful for evaluating flame resistance of textiles is Test Method D6413/D6413M. Classification Index D4723 contains descriptions and guidance on other flammability test methods for textiles.5.1.3 This test method is useful to determine the ignition resistance and burning characteristics of materials used in protective clothing not designated for flame resistance when the outer material surface is exposed to the flame. As such, it is particularly suited to protective clothing materials that are composed of different layers such as coated fabrics, laminates, or multilayer clothing systems.5.2 Alternative procedures for conducting either a 3-s or 12-s exposure are provided where one or the other flame application exposure times are applied. The choice of either the shorter or longer single exposure time is provided to permit an assessment of the effects for flame impingement on materials under short-term and long-term flame exposure conditions.5.3 Correlation of data from this test method with the ignition resistance and burning characteristics of protective clothing (not designated for flame resistance) under actual use conditions is not implied.1.1 This test method establishes a small-scale laboratory screening procedure for comparing the ignition resistance and burning characteristics of materials used in protective clothing where flame resistance is not the primary form of protection provided by the clothing.1.1.1 This test method shall not be used in applications where flame resistance is the primary form of protection offered by the protective clothing. Other flammability test methods are more appropriate for those materials.1.1.2 This test method provides a means for comparing ease of ignition and burning behavior of materials which include plastic or elastomeric films, coated fabrics, flexible laminates, multilayer material systems, or other protective clothing materials that are not designated for offering flame resistance as their primary form of protection.1.2 This test method is used to measure and describe the response of materials, products, or assemblies to heat and flame under controlled conditions, but does not by itself incorporate all factors required for fire hazard or fire risk assessment of the materials, products, or assemblies under actual fire conditions.1.3 Fire testing is inherently hazardous. Adequate safeguards for personnel and property shall be employed in conducting these tests.1.4 The values stated in SI units or other units shall be regarded separately as standard. The values stated in each system are not exact equivalents; therefore, each system must be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method evaluates the ability of the construction and configuration of protective clothing or protective ensembles to resist liquid penetration. In most cases, the conditions used in this test method will not represent actual end-use conditions.5.2 Two different spray configurations are used for exposing the protective clothing or protective ensemble on a manikin.5.2.1 Procedure A involves five shower nozzles, with one nozzle directly above the clothed manikin and two nozzles each to upper and lower sides of the manikin that are all positioned in the same vertical plane. This spray configuration is intended to provide a full exposure of the entire protective clothing or protective ensemble system.5.2.2 Procedure B involves three shower nozzles that are positioned at different heights on a vertical line that is parallel to the manikin with the locations and direction of each nozzle set with respect to targets on the manikin. This spray configuration is intended to provide a direct assessment of garment features such as the front closure.5.3 The selected duration of the test is not intended to simulate user exposure to splashes of liquid substances but rather to provide sufficient time for enough liquid to penetrate to make visual detection easier. The default liquid exposure time for Procedure A is 20 min. The default liquid exposure time for Procedure B is 10 min.5.3.1 It is permissible to specify shorter test durations. It is recommended that the duration of exposure be the same in each manikin orientation.5.3.2 The choice of different test duration is partly based on the number of layers in the specimen being tested, some of which serve to absorb the surfactant-treated test liquid and result in attenuating the severity of the liquid challenge to the specimen.5.4 A nontoxic, non-foaming surfactant is added to water for this test method to simulate liquids of lower surface tensions. Liquids of specific interest can be simulated by treating water to achieve an equivalent surface tension.5.5 For protective clothing with water-repellent surfaces, the lower surface tension liquid will aid in the evaluation of the construction and configuration of the garment because it is less likely to be repelled and more likely to wet the protective clothing. This is especially useful for reusable garments whose water-repellent surface interferes with the evaluation of their construction and configuration when new, but is diminished after wearing and washing.5.6 Fluorescent or colored dyes are permitted to be added to the water to enhance detection of liquid penetration into the protective clothing or protective ensemble.5.7 This test method can be used by both manufacturers and end users to assess liquid penetration resistance. Manufacturers can use this test method to evaluate quality of construction and effectiveness of clothing and ensemble configurations.5.8 The clothing or ensemble is sized to fit the manikin. It is important that the clothing be selected to fit the manikin well since detection of liquid penetration requires as much contact as possible between the clothing or ensemble and the inner liquid-absorptive garment.5.9 Results on a mismatched size of clothing or ensemble shall not be used to generalize about a particular construction or configuration. Manikin fit potentially affects liquid penetration resistance determinations.5.10 There are no known restrictions to the types of protective clothing or protective ensembles that can be evaluated with this test method.5.11 In some cases protective clothing or protective ensembles that show no liquid penetration during this test method will still fail to protect wearers against specific liquids due to the material degradation, penetration, or permeation or the effects associated with the vapors of liquid chemicals.5.12 In some cases protective clothing or protective ensembles that show no liquid penetration during this test method will fail to protect wearers in specific circumstances as, for example, deluge or immersion.1.1 This test method measures the ability of protective clothing or protective ensembles to resist liquid penetration in the form of a shower spray with surfactant-treated water.1.2 This test method measures the liquid penetration resistance of the construction and configuration of the overall protective clothing or protective ensemble, but especially of seams, closures, and interfaces with other components such as gloves, boots, hoods, and respiratory protective equipment. It is intended that this test method be used to assess the liquid penetration resistance of protective clothing and protective ensembles as received from the manufacturer and worn in accordance with their instructions.1.3 Resistance of materials used in protective clothing to permeation or penetration can be determined in accordance with Test Method F739 (or Test Method F1383 or F1407) and Test Method F903, respectively. Alternatively, resistance of materials used in protective clothing to penetration by synthetic blood or liquids containing virus can be determined in accordance with Test Methods F1670/F1670M and F1671/F1671M.1.4 The integrity of vapor protective ensembles is measured by its ability to maintain positive internal pressure with Test Method F1052.1.5 The values in SI units or in other units shall be regarded separately as standard. The values stated in each system must be used independently of the other, without combining values in any way.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method is used to evaluate the heat resistance of materials, clothing, and equipment when exposed to heat in a hot air circulating oven. The principal findings of this test method are observations of the specimen response to the heat exposure.5.1.1 The majority of procedures specified in this test method apply to the evaluation of flat material specimens.5.1.2 When evaluating non-flat materials, alternative procedures are required for mounting specimens and interpreting the effects of the heat exposure.5.2 If specified, this test method is used for the measurement of material dimensional change following a convective heat exposure in a hot air circulating oven.5.3 This test method is not intended to simulate the actual exposure of material, clothing, or equipment in high-heat conditions such as a fire environment.1.1 This test method covers quantitative measurements and subjective observations that characterize the performance for evaluating the heat resistance of materials, protective clothing, and equipment when exposed in a hot air circulating oven.1.2 This test method is intended to evaluate physical changes in materials, protective clothing, and equipment at a specified heat exposure.1.2.1 The specified heat exposure in the hot air circulating oven is a combination of convective heat and radiant heat.1.3 Materials, protective clothing, and equipment are evaluated for visible changes or subjected to a material property measurement following a specified heat exposure.1.3.1 This test method is not to be used for the evaluation of sticking. An acceptable method for evaluating sticking of fabrics is described in NFPA 1975, Sections 7.2.1 and 8.3. The NFPA 1975 test method evaluates the thermal stability of specimens by assessing the blocking of folded specimens placed between glass plates, under a specified weight, inside an oven meeting the same characteristics of the oven used in this test method.1.4 This test method enables the quantitative measurement of dimensional change that occurs as a result of a specified heat exposure in a hot air circulating oven.1.5 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to other units that are commonly used for thermal testing.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.NOTE 1: Flame-resistant and heat-resistant materials are described in a range of different standards and meet a range of different requirements. For materials tested in accordance with this test method, the applicable standard shall be used to establish preconditioning, conditioning, and testing conditions and requirements.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method establishes a standard procedure for rapidly (in 1 h or less) determining the chemical resistance of specimens of protective clothing materials. This test method can be used to rank materials as to their suitability for use with liquids of known or unknown composition.5.2 The breakthrough detection time, permeation rate, or cumulative permeation can be used to identify protective clothing materials that are more likely to limit potential exposures to chemicals. Longer breakthrough detection times and lower cumulative amounts permeated and permeation rates are characteristics of materials that are better barriers to the test chemical.5.3 In general this test method is less sensitive than Test Method F739 coupled with sensitive analytical procedures. In cases where the chemical of concern is highly toxic and contact of even a very small amount with the skin may be detrimental to health, the permeation cup method is not recommended. Use Test Method F739.5.4 Upon permeating the clothing material, the chemical must evaporate in order for a weight loss to occur and permeation to be detected. Consequently, the test method may not be applicable for chemicals having low volatility (that is, vapor pressure). The vapor pressure below which this test method is not applicable has not been determined.5.4.1 A procedure for assessing volatility is described in Section 10.5.5 The results of this test method are highly dependent on the test temperature. If the objective is to compare different clothing materials, all tests shall be conducted at the same temperature (±3 °C).1.1 This test method measures the barrier effectiveness of a specimen of protective clothing upon continuous contact with a liquid.1.1.1 Procedure A—For use when a value for the cumulative amount of chemical permeated in 1 h is desired.1.1.2 Procedure B—For use when breakthrough detection time and permeation rate values are desired.1.2 Although not addressed herein, the effect of the test chemical on the clothing material can be determined by comparing the weight or other physical properties of the specimen before and after the permeation test.1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 7.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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1.1 This specification provides minimum requirements for labeling protective clothing offering heat, flame, and melting resistance for applications where the potential exists for incidental exposure to open flame, radiant heat sources, or hot surfaces which could melt or ignite materials.1.1.1 Examples of possible applications for this specification include safety apparel, including high-visibility safety apparel, in situations where the possibility exists for accidental contact with hot surfaces, radiant heat sources, or an open flame; clothing worn by individuals for chemical, liquid, or particle protection where the possibility exists for clothing to similarly contact a burner or similar low-intensity flame source; or other clothing worn by individuals that comes in contact with torch flames, hot piping, or other surfaces that melt, degrade, or ignite clothing materials by proximity or contact.1.1.2 This specification is not to be used for separate claims for flame resistance (“FR”), heat resistance, or protection against the transfer of thermal energy. Instead, clothing materials are required to be evaluated for the combination of flame and heat resistance tests.1.1.3 This specification does not include a test for establishing protection levels against specific hazards where clothing insulation is needed such as from flash fires, exposure to high-energy electrical arc, or extended duration fires. This specification does not replace and shall not be used in lieu of existing standards where well-defined criteria are established for protection of workers from known characterized intense thermal hazards such as flash fires (NFPA 2112), high-energy electrical arc (Specification F1506), or wildland firefighting (NFPA 1977). See Appendix X1 for a list of standards for heat and flame-resistant protective clothing.1.1.4 This specification includes requirements that define resistance to melting and combustion of materials used in personal protective clothing in a manner to limit the contribution of the clothing for causing injury to the wearer when exposed to low levels of heat or flame. The primary mechanisms by which a garment can contribute to injury are by the garment igniting and supporting combustion, and if the garment melts onto the wearer’s skin.1.1.5 This specification is applicable to all materials used in the construction of the protective clothing, including lining materials and materials that contact the skin or underclothing of the wearer. Exclusions are permitted for some materials such as labels and small components that do not come in contact with the wearer’s skin or underclothing.1.1.6 This specification does not include testing for the evaluation of the entire clothing item.1.1.7 This specification does not include procedures for testing of gloves or footwear.1.1.8 This specification is applicable to hoods, balaclavas, shrouds, neck gaiters, barrier face coverings, and other items of apparel that are primarily worn on the individual wearer’s head.1.2 This specification does not apply to protective clothing that is addressed in other standards for specific applications including electrical arc flash, flash fire, and various types of firefighting or emergency response. See Appendix X1 for a list of standards for heat and flame-resistant protective clothing.1.3 The values stated in SI units or in other units shall be regarded separately as standard. The values stated in each system must be used independently of the other, without combining values in any way.1.4 This standard measures and describes the response of materials, products, or assemblies to heat and flame under controlled conditions, but does not by itself incorporate all factors required for fire hazard or fire risk assessment of the materials, products, or assemblies under actual fire conditions.1.5 The following precautionary caveat pertains only to the test methods portion, Section 8, of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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